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    • 1. 发明专利
    • DE69401772T2
    • 1997-09-11
    • DE69401772
    • 1994-10-24
    • TAKAHASHI YASUNORI
    • TAKAHASHI YASUNORI
    • B22F1/02B22F1/00C22C1/04H01F1/057H01F1/08H01F41/02
    • It is an object of the present invention to provide a method of producing sintered- or bond- rare earth element.iron.boron magnets obtainable easily and superior in magnetic properties with stable performance. The method of producing sintered rare earth element.iron. boron magnets according to the present invention is characterized by that it comprises steps of mixing in a scheduled ratio an acicular iron powder coated with a coating material, a rare earth element powder coated with a coating material and a boron powder coated with a coating material, and subjecting the mixture to compression molding followed by sintering of the molded mixture in the presence of a magnetic field. The method of producing bond rare earth element.iron. boron magnets according to the present invention is characterized by that it comprises steps of preparing a magnet powder by hydrogen-disintegration of the above-mentioned sintered magnet wherein a hydrogen-occluded sintered magnet resulted from heating the magnet under hydrogen atmosphere is subjected to hydrogen emission under substantial vacuum to cause disintegration of the hydrogen-occluded sintered magnet, coating the magnet powder with a coating material, mixing the coated magnet powder with a binder, and compression molding the mixture under heating in the presence of a magnetic field.
    • 2. 发明专利
    • DE69403059T2
    • 1997-08-28
    • DE69403059
    • 1994-10-24
    • TAKAHASHI YASUNORI
    • TAKAHASHI YASUNORI
    • B22F1/02C22C33/02C23C26/00H01F1/057H01F1/059H01F1/06H01F1/08
    • The material for permanent magnet according to the present invention comprises an acicular iron powder having successively on the surface (1) a coated layer of aluminum phosphate, (2) a diffused layer of rare earth element or a diffused layer of rare earth element.boron or a diffused layer of rare earth element.boron.nitrogen, and (3) a coated layer of aluminum phosphate. The material for permanent magnet can be produced by (a) a step of mixing and covering an acicular goethite (FeOOH) crystal with aluminum phosphate, (b) a step of preparing an acicular iron powder coated with a layer of aluminum phosphate by reducing under hydrogen atmosphere at 300-500 DEG C the acicular goethite (FeOOH) crystal covered by the aluminum phosphate, (c) a step of diffusing a rare earth element or a rare earth element and boron into the surface layer of aluminum phosphate by heating under argon atmosphere at 650-1000 DEG C the acicular iron powder coated with a layer of aluminum phosphate in the presence of the rare earth element or the rare earth element and boron, (d) a step of mixing and covering the rare earth element diffused powder or rare earth element and boron diffused powder with aluminum phosphate, and (e) a step of coating the rare earth element diffused powder or rare earth element and boron diffused powder with aluminum phosphate by heating under argon atmosphere at 300-500 DEG C the rare earth element diffused powder or rare earth element and boron diffused powder covered by the aluminum phosphate.
    • 9. 发明专利
    • DE69401772D1
    • 1997-03-27
    • DE69401772
    • 1994-10-24
    • TAKAHASHI YASUNORI
    • TAKAHASHI YASUNORI
    • B22F1/02B22F1/00C22C1/04H01F1/057H01F1/08H01F41/02
    • It is an object of the present invention to provide a method of producing sintered- or bond- rare earth element.iron.boron magnets obtainable easily and superior in magnetic properties with stable performance. The method of producing sintered rare earth element.iron. boron magnets according to the present invention is characterized by that it comprises steps of mixing in a scheduled ratio an acicular iron powder coated with a coating material, a rare earth element powder coated with a coating material and a boron powder coated with a coating material, and subjecting the mixture to compression molding followed by sintering of the molded mixture in the presence of a magnetic field. The method of producing bond rare earth element.iron. boron magnets according to the present invention is characterized by that it comprises steps of preparing a magnet powder by hydrogen-disintegration of the above-mentioned sintered magnet wherein a hydrogen-occluded sintered magnet resulted from heating the magnet under hydrogen atmosphere is subjected to hydrogen emission under substantial vacuum to cause disintegration of the hydrogen-occluded sintered magnet, coating the magnet powder with a coating material, mixing the coated magnet powder with a binder, and compression molding the mixture under heating in the presence of a magnetic field.
    • 10. 发明专利
    • AT149065T
    • 1997-03-15
    • AT94116750
    • 1994-10-24
    • TAKAHASHI YASUNORI
    • TAKAHASHI YASUNORI
    • B22F1/02B22F1/00C22C1/04H01F1/057H01F1/08H01F41/02
    • It is an object of the present invention to provide a method of producing sintered- or bond- rare earth element.iron.boron magnets obtainable easily and superior in magnetic properties with stable performance. The method of producing sintered rare earth element.iron. boron magnets according to the present invention is characterized by that it comprises steps of mixing in a scheduled ratio an acicular iron powder coated with a coating material, a rare earth element powder coated with a coating material and a boron powder coated with a coating material, and subjecting the mixture to compression molding followed by sintering of the molded mixture in the presence of a magnetic field. The method of producing bond rare earth element.iron. boron magnets according to the present invention is characterized by that it comprises steps of preparing a magnet powder by hydrogen-disintegration of the above-mentioned sintered magnet wherein a hydrogen-occluded sintered magnet resulted from heating the magnet under hydrogen atmosphere is subjected to hydrogen emission under substantial vacuum to cause disintegration of the hydrogen-occluded sintered magnet, coating the magnet powder with a coating material, mixing the coated magnet powder with a binder, and compression molding the mixture under heating in the presence of a magnetic field.