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1. 发明授权

US09943832B2 Bulk catalyst composition comprising bulk metal oxide particles 有权
公开(公告)号：US09943832B2
公开(公告)日：2018-04-17
申请号：US12743153
申请日：2008-12-04
申请人： Sona Eijsbouts-Spickova , Robertus Gerardus Leliveld , Paul Joseph Maria Lebens , Frans Lodewijk Plantenga , Bob Gerardus Oogjen , Henk Jan Tromp , Stuart Leon Soled , Sabato Miseo
发明人： Sona Eijsbouts-Spickova , Robertus Gerardus Leliveld , Paul Joseph Maria Lebens , Frans Lodewijk Plantenga , Bob Gerardus Oogjen , Henk Jan Tromp , Stuart Leon Soled , Sabato Miseo
IPC分类号： B01J23/888 , B01J23/85 , B01J37/03 , B01J37/20 , C10G49/04 , B01J21/16 , B01J35/00 , B01J37/00
CPC分类号： B01J23/8885 , B01J21/16 , B01J23/85 , B01J23/888 , B01J35/002 , B01J37/0009 , B01J37/03 , B01J37/20 , C10G49/04
摘要： The invention relates to a process for preparing bulk metal oxide particles comprising the steps of combining in a reaction mixture (i) dispersible nanoparticles having a dimension of less than about 1 μm upon being dispersed in a liquid, (ii) at least one Group VIII non-noble metal compound, (iii) at least one Group VIB metal compound, and (iv) a protic liquid; and reacting the at least one Group VIII non-noble metal compound and the at least one Group VIB metal in the presence of the nanoparticles. It also relates to bulk metal hydroprocessing catalysts obtainable by such method.

2. 发明授权

US08067331B2 Bulk catalyst comprising nickel tungsten metal oxidic particles 有权
标题翻译：包含镍钨金属氧化物颗粒的散装催化剂
公开(公告)号：US08067331B2
公开(公告)日：2011-11-29
申请号：US12091322
申请日：2006-10-25
申请人： Sona Eijsbouts-Spickova , Robertus Gerardus Leliveld , Marinus Bruce Cerfontain , Frans L. Plantenga , Eelco Titus Carel Vogt , Jacobus Nicolaas Louwen , Stuart Leon Soled , Sabato Miseo , Kenneth L. Riley
发明人： Sona Eijsbouts-Spickova , Robertus Gerardus Leliveld , Marinus Bruce Cerfontain , Frans L. Plantenga , Eelco Titus Carel Vogt , Jacobus Nicolaas Louwen , Stuart Leon Soled , Sabato Miseo , Kenneth L. Riley
IPC分类号： C10G45/04
CPC分类号： B01J23/888 , B01J23/002 , B01J35/002 , B01J37/0009 , B01J37/03 , B01J37/10 , B01J37/20 , B01J2523/00 , C10G45/08 , C10G2300/202 , B01J2523/69 , B01J2523/847 , B01J2523/68 , B01J2523/56
摘要： The invention relates to a nickel tungsten bulk catalyst, to a process for the manufacture of said catalyst and to the use of said catalyst for the hydrotreatment, in particular the hydrodesulphurisation and hydrodenitrogenation of hydrocarbon feedstock. The catalyst comprises nickel tungsten metal oxidic particles obtainable by a process comprising forming a slurry of a first solid metal compound comprising Group VNI metal nickel and a second solid metal compound comprising Group VIB metal tungsten in a protic liquid, reacting the first and second solid metal compounds at elevated temperature whereby the first and second solid metal compounds remain at least partly in the solid state during the entire reaction to form the nickel tungsten oxidic bulk catalyst.
摘要翻译：本发明涉及镍钨体积催化剂，制备所述催化剂的方法以及所述催化剂用于加氢处理的用途，特别是烃原料的加氢脱硫和加氢脱氮。该催化剂包括可通过以下工艺获得的镍钨金属氧化物颗粒，所述方法包括在质子液体中形成包含VNI族金属镍的第一固体金属化合物和包含第VIB族金属钨的第二固体金属化合物的浆料，使第一和第二固体金属化合物在高温下由此第一和第二固体金属化合物在整个反应期间保持至少部分为固体状态以形成镍钨氧化物本体催化剂。

3. 发明授权

US07513989B1 Hydrocracking process using bulk group VIII/Group VIB catalysts 有权
标题翻译：使用本体VIII / VIB族催化剂的加氢裂化工艺
公开(公告)号：US07513989B1
公开(公告)日：2009-04-07
申请号：US09869990
申请日：2000-01-14
申请人： Stuart Leon Soled , Kenneth Lloyd Riley , Gary P. Schleicher , Richard A. Demmin , Darlene Schuette, legal representative , Ian Alfred Cody
发明人： William L. Schuette
IPC分类号： C10G47/04
CPC分类号： C08F8/00 , B01J23/002 , B01J23/8885 , B01J35/1019 , B01J35/1038 , B01J37/03 , B01J37/04 , B01J37/20 , B01J2523/00 , C08F8/04 , C08F8/50 , C10G45/08 , C10G45/16 , C10G47/04 , C10G65/04 , C10G65/08 , C10G65/12 , C10G2400/10 , C10G2400/14 , C08F240/00 , B01J2523/68 , B01J2523/69 , B01J2523/847
摘要： The invention relates to a hydrocracking process for hydrocracking petroleum and chemical feedstocks using bulk Group VIII/VIB catalysts. Preferred catalysts include those comprised of Ni—Mo—W.
摘要翻译：本发明涉及使用本体VIII / VIB催化剂加氢裂化石油和化学原料的加氢裂化方法。优选的催化剂包括由Ni-Mo-W组成的催化剂。

4. 发明授权

US5728644A Dispersed metal sulfide catalysts for hydroprocessing 失效
标题翻译：用于加氢处理的分散金属硫化物催化剂
公开(公告)号：US5728644A
公开(公告)日：1998-03-17
申请号：US524228
申请日：1995-09-05
申请人： Teh Chung Ho , Stuart Leon Soled , Sabato Miseo , Gary Brice Mc Vicker , Michel Daage , Viktor Buchholz
发明人： Teh Chung Ho , Stuart Leon Soled , Sabato Miseo , Gary Brice Mc Vicker , Michel Daage , Viktor Buchholz
IPC分类号： B01J31/22 , B01J23/887 , B01J23/889 , B01J27/051 , B01J37/08 , B01J37/20 , C07B35/02 , C10G45/46 , C10G45/50 , B01J27/047 , B01J23/63 , B01J31/00
CPC分类号： B01J37/086 , B01J23/887 , B01J23/8878 , B01J23/8892 , B01J27/051 , B01J37/20 , C10G45/46 , C10G45/50
摘要： The present invention is directed toward a catalyst composition comprising a catalyst prepared by a process comprising: (a) impregnating an oxide precursor selected from the group consisting of rare earth oxide precursors, yttria precursors and mixtures thereof, onto an inorganic refractory oxide support; (b) drying said support at a temperature of about 100.degree. to about 120.degree. C. followed by calcining said support at a temperature of about 400.degree. to about 600.degree. C.; and (c) compositing or depositing on said support of step (b), a catalyst precursor salt represented by (ML)(Mo.sub.y W.sub.1-y O.sub.4).sub.a wherein M comprises Cr and/or one or more divalent promoter metals selected from the group consisting of Mn, Fe, Co, Ni, Cu, Zn and mixtures thereof, wherein y is any value ranging from 0 to 1, and wherein L is one or more neutral, nitrogen-containing ligands at least one of which is a chelating polydentate ligand; a=1 when chromium is not one of the promoter metals and 0.5.ltoreq.a.ltoreq.3 when Cr is one of the promoter metals. (d) sulfiding said deposited or composited supports of step (c) with an excess amount of sulfur in the form of one or more sulfur bearing compounds and at a temperature of at least about 250.degree. C. to form catalysts. In a preferred embodiment, the process will further comprise decomposing the composited or deposited supports of step (c) in a nonoxidizing atmosphere at a temperature of at least about 250.degree. C. prior to said sulfiding step (d). In a second aspect of the invention there is provided an improved aromatics hydrogenation process.
摘要翻译：本发明涉及一种催化剂组合物，其包含通过以下方法制备的催化剂，所述催化剂包括：（a）将选自稀土氧化物前体，氧化钇前体及其混合物的氧化物前体浸渍到无机耐火氧化物载体上; （b）在约100至约120℃的温度下干燥所述载体，然后在约400至约600℃的温度下煅烧所述载体; 和（c）在步骤（b）的所述载体上合成或沉积由（ML）（MoyW1-yO4）a表示的催化剂前体盐，其中M包含Cr和/或一种或多种选自以下的二价助催化剂金属： Mn，Fe，Co，Ni，Cu，Zn及其混合物，其中y是0至1的任何值，并且其中L是一种或多种中性含氮配体，其中至少一种是螯合多齿配体; 当Cr不是助催化剂金属之一时，a = 1，当Cr是助催化剂金属之一时，a = 1。（d）用一种或多种带硫化合物形式的过量硫磺和至少约250℃的温度硫化所述步骤（c）的沉积或复合载体以形成催化剂。在优选的实施方案中，该方法还包括在所述硫化步骤（d）之前，在至少约250℃的温度下，在非氧化气氛中分解步骤（c）的复合或沉积的载体。在本发明的第二方面，提供了一种改进的芳族化合物氢化方法。

5. 发明授权

US07718564B2 Partially decomposed catalyst and hydrocarbon oxidation processes using the same 有权
标题翻译：部分分解的催化剂和烃氧化方法使用它们
公开(公告)号：US07718564B2
公开(公告)日：2010-05-18
申请号：US11434717
申请日：2006-05-16
申请人： Jihad Mohammed Dakka , Sabato Miseo , Stuart Leon Soled , Jose Guadalupe Santiesteban , Joseph Ernest Baumgartner , Michiel Christian Alexander Van Vliet , Roger Arthur Sheldon
发明人： Jihad Mohammed Dakka , Sabato Miseo , Stuart Leon Soled , Jose Guadalupe Santiesteban , Joseph Ernest Baumgartner , Michiel Christian Alexander Van Vliet , Roger Arthur Sheldon
IPC分类号： B01J23/72 , B01J23/755 , B01J31/00 , B01J27/24
CPC分类号： B01J31/2243 , B01J23/76 , B01J2231/70 , B01J2531/16 , B01J2531/847 , C07C68/00 , C07C69/96
摘要： The present invention is related to a hydrocarbon oxidation process. The process comprises bringing one or more hydrocarbons into contact with a source of oxygen in the presence of a radical initiator and a catalyst. The catalyst comprises an organic metal complex located on a catalyst support, and is obtained by partial decomposition of the organic metal complex. For example, the process can be used to produce dimethyl carbonate from dimethoxy methane. The invention is also related to a partially decomposed catalyst that comprises a silica support and an organic metal complex, wherein at least 5% of the organic compound remains in the catalyst. The organic metal complex comprises an organic compound and a metal-based compound wherein the metal is selected from copper, nickel, and combinations thereof. The invention is also related to a process for manufacturing of a catalyst comprising mixing L-arginine, a Cu-based compound, water, and optionally another metal-based compound to form a solution; impregnating the solution onto a silica support to form a catalyst precursor; and partially decomposing the L-arginine to form the catalyst so that at least 5% of L-arginine remains in the catalyst.
摘要翻译：本发明涉及烃氧化方法。该方法包括在自由基引发剂和催化剂的存在下使一种或多种烃与氧源接触。催化剂包含位于催化剂载体上的有机金属络合物，并通过有机金属络合物的部分分解获得。例如，该方法可用于从二甲氧基甲烷生产碳酸二甲酯。本发明还涉及包含二氧化硅载体和有机金属络合物的部分分解的催化剂，其中至少5％的有机化合物保留在催化剂中。有机金属络合物包括有机化合物和金属基化合物，其中金属选自铜，镍及其组合。本发明还涉及制造催化剂的方法，其包括将L-精氨酸，Cu基化合物，水和任选的其它金属类化合物混合以形成溶液; 将溶液浸渍到二氧化硅载体上以形成催化剂前体; 并部分分解L-精氨酸以形成催化剂，使得至少5％的L-精氨酸保留在催化剂中。

6. 发明申请

US20090139904A1 Bulk Hydroprocessing Catalyst Comprising A Group VIII Metal And Molybdenum, Preparation And Use Thereof 有权
标题翻译：包含VIII族金属和钼的大量加氢催化剂，其制备和使用
公开(公告)号：US20090139904A1
公开(公告)日：2009-06-04
申请号：US12091328
申请日：2006-10-25
申请人： Sona Eijsbouts-Spickova , Jacobus Nicolaas Louwen , Frans L. Plantenga , Robertus Gerardus Leliveld , Sabato Miseo , Stuart Leon Soled
发明人： Sona Eijsbouts-Spickova , Jacobus Nicolaas Louwen , Frans L. Plantenga , Robertus Gerardus Leliveld , Sabato Miseo , Stuart Leon Soled
IPC分类号： C10G45/04 , B01J23/883 , B01J23/882
CPC分类号： B01J23/88 , B01J23/883 , B01J23/8877 , B01J23/8885 , B01J35/002 , B01J37/03 , B01J37/20 , C10G45/08 , C10G45/12 , C10G2300/1055 , C10G2300/202 , C10G2400/04
摘要： The invention relates to a bulk catalyst comprising at least 60 wt % metal oxidic particles comprising one or more Group VIII metals and Group VIB metal molybdenum, comprising less than 10 mole % of a second Group VIB metal (relative to the total amount of Group VIB metals) and comprising a Group V metal in an amount less than 10 mole % (relative to the total of the Group VIB metals), which bulk catalyst has been calcined at a temperature below a temperature where the hexagonal metastable crystal structure changes to an inactive crystalline structure, preferably below 450° C. and which bulk catalyst has a metastable hexagonal phase characterized by an X-ray diffraction pattern having reflections at 33-35 and 58-61° 2θ. Preferably, the main reflections have a full width at half maximum (FWHM) of less than 2.5. The invention further relates to a process for the manufacture of the bulk catalyst, to the corresponding sulphided bulk catalyst and to the use of said catalyst or sulphided catalyst in the hydroprocessing, in particular the hydrodesulphurisation and hydrodenitrogenation, of a hydrocarbon feedstock.
摘要翻译：本发明涉及一种本体催化剂，其包含至少60重量％的包含一种或多种第VIII族金属和VIB族金属钼的金属氧化物颗粒，其包含小于10摩尔％的第二族VIB金属（相对于VIB族的总量）金属），并且包含少于10摩尔％（相对于第VIB族金属的总量）的第V族金属，该体积催化剂在低于六方晶系亚稳晶体结构变为不活泼的温度的温度下被煅烧晶体结构，优选低于450℃，并且该体积催化剂具有亚稳态六方晶相，其特征在于具有在33-35和58-61°2θ之间的反射的X射线衍射图。优选地，主反射具有小于2.5的半高宽（FWHM）。本发明还涉及一种用于制造本体催化剂的方法，相应的硫化体积催化剂以及所述催化剂或硫化催化剂在烃原料的加氢处理，特别是加氢脱硫和加氢脱氮中的用途。

7. 发明授权

US07232515B1 Hydrofining process using bulk group VIII/Group VIB catalysts 有权
标题翻译：使用本体VIII / VIB族催化剂的加氢精制方法
公开(公告)号：US07232515B1
公开(公告)日：2007-06-19
申请号：US09869987
申请日：2000-01-14
申请人： Richard Alan Demmin , Kenneth Lloyd Riley , Stuart Leon Soled , Sabato Miseo
发明人： Richard Alan Demmin , Kenneth Lloyd Riley , Stuart Leon Soled , Sabato Miseo
IPC分类号： C10G45/60
CPC分类号： B01J23/002 , B01J23/85 , B01J23/88 , B01J23/883 , B01J23/8878 , B01J23/888 , B01J23/8885 , B01J37/03 , B01J37/082 , B01J2523/00 , C08F8/00 , C08F8/04 , C08F8/50 , C10G45/08 , C10G45/16 , C10G47/04 , C10G65/04 , C10G65/08 , C10G65/12 , C10G2400/10 , C10G2400/14 , C08F240/00 , B01J2523/68 , B01J2523/69 , B01J2523/847 , B01J2523/842 , B01J2523/67 , B01J2523/31 , B01J2523/41
摘要： A process for hydrofining a lubricating oil feedstock comprising contacting the feedstock with a hydrofining catalyst in a hydrofining zone under hydrofining conditions wherein the hydrofining catalyst comprises a bulk metal catalyst containing non-noble Group VIII metal molybdate in which at least a portion but less than all of the molybdenum is replaced by tungsten.
摘要翻译：一种用于加氢精炼润滑油原料的方法，包括在加氢精炼条件下在加氢精炼区中将原料与加氢精制催化剂接触，其中加氢精制催化剂包含含有非贵金属VIII族金属钼酸盐的本体金属催化剂，其中至少一部分但少于全部的钼被钨取代。

8. 发明授权

US06863803B1 Production of low sulfur/low nitrogen hydrocrackates 有权
标题翻译：生产低硫/低氮加氢裂化剂
公开(公告)号：US06863803B1
公开(公告)日：2005-03-08
申请号：US09869985
申请日：2000-01-14
申请人： Kenneth Lloyd Riley , Darlene Schuette , Stuart Leon Soled , Sabato Miseo
发明人： William Lee Schuette
IPC分类号： C01G53/00 , B01J23/00 , B01J23/85 , B01J23/88 , B01J23/883 , B01J23/888 , B01J37/03 , B01J37/08 , C07C29/16 , C08F8/00 , C08F8/04 , C08F8/50 , C10G45/08 , C10G45/16 , C10G47/04 , C10G47/12 , C10G49/04 , C10G65/02 , C10G65/04 , C10G65/08 , C10G65/12 , C10G67/04 , C10G45/04
CPC分类号： B01J23/002 , B01J23/85 , B01J23/88 , B01J23/883 , B01J23/8878 , B01J23/888 , B01J23/8885 , B01J37/03 , B01J37/082 , B01J2523/00 , C07C29/16 , C08F8/00 , C08F8/04 , C08F8/50 , C10G45/08 , C10G45/16 , C10G47/04 , C10G65/04 , C10G65/08 , C10G65/12 , C10G2400/10 , C10G2400/14 , C08F240/00 , B01J2523/68 , B01J2523/69 , B01J2523/847 , B01J2523/842 , B01J2523/67 , B01J2523/31 , B01J2523/41
摘要： A two stage hydrodesulfurizing process for producing low sulfur distillates. A distillate boiling range feedstock containing in excess of about 3,000 wppm sulfur is hydrodesulfurized in a first hydrodesulfurizing stage containing one or more reaction zones in the presence of hydrogen and a hydrodesulfurizing catalyst. The liquid product stream thereof is passed to a first separation stage wherein a vapor phase product stream and a liquid product stream are produced. The liquid product stream, which has a substantially lower sulfur and nitrogen content than the original feedstream is passed to a second hydrodesulfurizing stage also containing one or more reaction zones where it is reacted in the presence of hydrogen and a second hydrodesulfurizing catalyst at hydrodesulfurizing conditions. The catalyst in any one or more reaction zones is a bulk multimetallic catalyst comprised of at lease one Group VIII non-noble metal and at least two Group VIB metals.
摘要翻译：一种用于生产低硫馏分的二级加氢脱硫方法。在含氢和加氢脱硫催化剂的情况下，在含有一个或多个反应区的第一加氢脱硫阶段，加氢脱硫含有超过约3,000wppm硫的馏出物沸程原料。将其液体产物流送入其中产生气相产物流和液体产物流的第一分离阶段。将具有比原始原料流显着更低的硫和氮含量的液体产物流传递到还含有一个或多个反应区的第二加氢脱硫阶段，其中在氢气存在下使其反应并在加氢脱硫条件下与第二加氢脱硫催化剂反应。任何一个或多个反应区中的催化剂是由至少一个VIII族非贵金属和至少两种VIB族金属组成的大量多金属催化剂。

9. 发明授权

US06783663B1 Hydrotreating using bulk multimetallic catalysts 有权
标题翻译：使用大量多金属催化剂加氢处理
公开(公告)号：US06783663B1
公开(公告)日：2004-08-31
申请号：US09869988
申请日：2001-08-22
申请人： Kenneth Lloyd Riley , Darryl Patrick Klein , Zhiguo Hou , Stuart Leon Soled , Michael Charles Kerby , Gary Brice McVicker , Edward Stanley Ellis , Michele Sue Touvelle , Sabato Miseo
发明人： Kenneth Lloyd Riley , Darryl Patrick Klein , Zhiguo Hou , Stuart Leon Soled , Michael Charles Kerby , Gary Brice McVicker , Edward Stanley Ellis , Michele Sue Touvelle , Sabato Miseo
IPC分类号： C10G4504
CPC分类号： B01J23/002 , B01J23/85 , B01J23/88 , B01J23/883 , B01J23/8878 , B01J23/888 , B01J23/8885 , B01J37/03 , B01J37/082 , B01J2523/00 , C07C29/16 , C08F8/00 , C08F8/04 , C08F8/50 , C10G45/08 , C10G45/16 , C10G47/04 , C10G65/04 , C10G65/08 , C10G65/12 , C10G2400/10 , C10G2400/14 , C08F240/00 , B01J2523/68 , B01J2523/69 , B01J2523/847 , B01J2523/842 , B01J2523/67 , B01J2523/31 , B01J2523/41
摘要： A hydroprocessing process, comprising: contacting a feedstock, at hydrotreating conditions, with a bulk multimetallic catalyst comprised of at least one Group VIII non-noble metal and at least two Group VIB metals and wherein the ratio of Group VIB metal to Group VIII non-noble metal is from about 10:1 to about 1:10 to form a hydrotreated product.
摘要翻译：一种加氢处理方法，包括：在加氢处理条件下使原料与由至少一种第八族非贵金属和至少两种第VIB族金属组成的本体多金属催化剂接触，并且其中VIB族金属与VIII族非金属的比率，贵金属为约10:1至约1:10以形成加氢处理的产物。

10. 发明授权

US06620313B1 Hydroconversion process using bulk group VIII/Group VIB catalysts 有权
标题翻译：使用本体VIII / VIB族催化剂的加氢转化法
公开(公告)号：US06620313B1
公开(公告)日：2003-09-16
申请号：US09869986
申请日：2001-08-22
申请人： Richard Alan Demmin , Kenneth Lloyd Riley , Stuart Leon Soled , Sabato Miseo
发明人： Richard Alan Demmin , Kenneth Lloyd Riley , Stuart Leon Soled , Sabato Miseo
IPC分类号： C10G7306
CPC分类号： B01J23/002 , B01J23/85 , B01J23/88 , B01J23/883 , B01J23/8878 , B01J23/888 , B01J23/8885 , B01J37/03 , B01J37/082 , B01J2523/00 , C07C29/16 , C08F8/00 , C08F8/04 , C08F8/50 , C10G45/08 , C10G45/16 , C10G47/04 , C10G65/04 , C10G65/08 , C10G65/12 , C10G2400/10 , C10G2400/14 , C08F240/00 , B01J2523/68 , B01J2523/69 , B01J2523/847 , B01J2523/842 , B01J2523/67 , B01J2523/31 , B01J2523/41
摘要： Hydroconversion process of petroleum and chemical feedstocks using bulk Group VIII/Group VIB catalysts. Preferred catalysts include those comprised of Ni—Mo—W.
摘要翻译：石油和化学原料的加氢转化工艺使用大量第VIII / VIB族催化剂。优选的催化剂包括由Ni-Mo-W组成的催化剂。

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