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1. 发明授权

US4308345A Silver halide photographic emulsion 失效
标题翻译：卤化银照相乳剂
公开(公告)号：US4308345A
公开(公告)日：1981-12-29
申请号：US730900
申请日：1976-10-08
申请人： Masanao Hinata , Haruo Takei , Akira Sato , Atsuo Iwamoto , Jun Hayashi
发明人： Masanao Hinata , Haruo Takei , Akira Sato , Atsuo Iwamoto , Jun Hayashi
IPC分类号： G03C1/28 , G03C1/29 , G03C1/14
CPC分类号： G03C1/29
摘要： A silver halide photographic emulsion selectively spectrally sensitized, particularly to red light, with a combination of at least one sensitizing dye represented by general formula (I): ##STR1## wherein Z.sup.1 and Z.sup.2 each represents the atoms necessary to form a benzothiazole nucleus or a benzoselenazole nucleus, R.sup.1 and R.sup.2 l each represents an alkyl group or a substituted alkyl group, wherein at least one of R.sup.1 or R.sup.2 should represent a sulfo group-containing substituted alkyl group, a carboxyalkyl group or a hydroxyalkyl group, R.sup.3 represents an alkyl group, X.sub.1 represents an acid anion, and m represents 1 or 2, wherein m equals 1 when the dye forms an intramolecular salt (betaine-like structure); at least one sensitizing dye represented by general formula (II): ##STR2## wherein Z.sup.3 represents a sulfur atom or a selenium atom, Z.sup.4 represents the atoms necessary to form a benzothiazole nucleus, a benzoselenazole nucleus, a naphtho[1,2-d]thiazole nucleus or a naphtho[1,2-d]selenazole nucleus, R.sup.4 and R.sup.5 each represents an alkyl group or a substituted alkyl group, wherein at least one of R.sup.4 or R.sup.5 should be a sulfo group-containing substituted alkyl group, a carboxyalkyl group or a hydroxyalkyl group, R.sup.6 represents an alkyl group, an aryl group, a furyl group or a thienyl group, X.sub.2 represents an acid anion, and n represents 1 or 2, wherein n equals 1 when the dye forms an intramolecular salt (betaine-like structure), and at least one benzimidazolothiacarbocyanine dye, which exhibits increased color reproducibility, high sensitivity and reduced residual coloration.
摘要翻译：通过至少一种由通式（I）表示的敏化染料的组合，选择性地光致敏化，特别是红光的卤化银照相乳剂：其中Z1和Z2各自表示形成苯并噻唑所必需的原子核或苯并硒唑核，R 1和R 2各自表示烷基或取代的烷基，其中R 1或R 2中的至少一个应表示含磺基的取代的烷基，羧基烷基或羟烷基，R 3表示烷基，X1表示酸阴离子，m表示1或2，当染料形成分子内盐（甜菜碱样结构）时，m等于1; 至少一种由通式（II）表示的敏化染料：其中Z 3表示硫原子或硒原子，Z 4表示形成苯并噻唑核所需的原子，苯并硒唑核，萘并[1， 2-d]噻唑核或萘并[1,2-d]硒唑核，R 4和R 5各自表示烷基或取代的烷基，其中R 4或R 5中的至少一个应为含磺基取代的烷基基团，羧基烷基或羟烷基，R6表示烷基，芳基，呋喃基或噻吩基，X2表示酸阴离子，n表示1或2，其中当染料形成时，n等于1 分子内盐（甜菜碱样结构）和至少一种苯并咪唑硫羰花青染料，其表现出增加的颜色再现性，高灵敏度和降低的残留着色。

2. 发明授权

US4154616A Silver halide photographic emulsion 失效
标题翻译：卤化银照相乳剂
公开(公告)号：US4154616A
公开(公告)日：1979-05-15
申请号：US796283
申请日：1977-05-12
申请人： Akira Sato , Akira Ogawa , Masanao Hinata , Haruo Takei
发明人： Akira Sato , Akira Ogawa , Masanao Hinata , Haruo Takei
IPC分类号： G03C1/22
CPC分类号： G03C1/22
摘要： A silver halide photographic emulsion containing at least one sensitizing dye represented by the following general formula (I), ##STR1## in which Z represents an atomic group necessary for forming a benzoxazole nucleus or a naphthoxazole nucleus; R.sub.1 represents an aliphatic group; R.sub.2 represents an alkyl group, an allyl group or an aryl group; R.sub.3 represents a 2-(2-hydroxyethoxy)-ethyl group, a 2-(2-acyloxyethyoxy)-ethyl group, an N-(N,N-dialkylaminoalkyl)carbamoylalkyl group, an N-(N,N,N-trialkylammoniumalkyl)carbamoylalkyl group or an N,N,N-trialkylammoniumalkyl group; X represents an acid anion; and n represents 0 or 1.
摘要翻译：含有由以下通式（I）表示的至少一种敏化染料的卤化银照相乳剂，其中Z表示形成苯并恶唑核或萘并恶唑核所必需的原子团; R1表示脂肪族基团; R2表示烷基，烯丙基或芳基; R3表示2-（2-羟基乙氧基） - 乙基，2-（2-酰氧基乙氧基） - 乙基，N-（N，N-二烷基氨基烷基）氨基甲酰基烷基，N-（N，N，N-三烷基铵烷基）氨基甲酰基烷基或N，N，N-三烷基铵烷基; X表示酸性阴离子; n表示0或1。

3. 发明授权

US4040841A Silver halide photographic emulsion 失效
标题翻译：卤化银照相乳剂
公开(公告)号：US4040841A
公开(公告)日：1977-08-09
申请号：US602508
申请日：1975-08-06
申请人： Masanao Hinata , Haruo Takei , Akira Sato , Tadashi Ikeda , Atsuo Iwamoto
发明人： Masanao Hinata , Haruo Takei , Akira Sato , Tadashi Ikeda , Atsuo Iwamoto
IPC分类号： G03C1/28 , G03C1/29 , G03C1/14
CPC分类号： G03C1/29
摘要： A silver halide photographic emulsion spectrally sensitized in the relatively shorter wavelength region ranging from blue to green with a supersensitizing combination of at least one sensitizing dye represented by the general formula (I) ##STR1## WHEREIN Z.sup.1 represents the atoms necessary to form a benzimidazole ring, an oxazole ring, a benzoxazole ring or a naphthoxazole ring; Z.sup.2 represents the atoms necessary to form a thiazole ring, a benzothiazole ring, a naphthothiazole ring, a selenazole ring, a benzoselenazole ring or a naphthoselenazole ring; R.sup.1 and R.sup.2 each represents an aliphatic group containing up to 8 carbon atoms, which may be unsubstituted or substituted, and the carbon chain of which may be interrupted with an oxygen atom or a sulfur atom; R.sup.3 represents an alkyl group containing up to 3 carbon atoms, an aryl group or an aralkyl group; X.sup.1 represents an acid anion; and m represents 1 or 2, wherein m equals 1 when the dye forms an intramolecular salt; and at least one dye selected from the group consisting of a simple merocyanine and a dimethinemerocyanine dye, or with a supersensitizing combination of at least one sensitizing dye represented by the general formula (I) as defined above and at least one sensitizing dye represented by the general formula (II) ##STR2## wherein Z.sup.3 represents the atoms necessary to form a 5- or 6-membered heterocyclic ring; Q represents the atoms necessary to form a rhodanine ring, a thiohydantoin ring or a 2-thioxazolidinedione ring; R.sup.4 represents an aliphatic group containing up to 4 carbon atoms, which may be unsubstituted or substituted and the carbon chain of which may be interrupted by an oxygen atom or a sulfur atom; R.sup.5 represents a hydrogen atom, an alkyl group, an aryl group or an aralkyl group; and n represents 1 or 2.
摘要翻译：在由蓝色到绿色的相对短的波长区域中进行光谱增感的卤化银照相乳剂，其具有由通式（I）（I）表示的至少一种敏化染料的超敏化组合，其中Z1表示形成所需的原子苯并咪唑环，恶唑环，苯并恶唑环或萘并恶唑环; Z2表示形成噻唑环所需的原子，苯并噻唑环，萘并噻唑环，硒咯环，苯并硒唑环或萘并吩唑环。 R1和R2各自表示含有至多8个碳原子的脂族基团，其可以是未取代的或取代的，并且其碳链可以被氧原子或硫原子间隔; R3表示含有至多3个碳原子的烷基，芳基或芳烷基; X1表示酸性阴离子; m表示1或2，当染料形成分子内盐时，m等于1; 和至少一种选自简单的部花菁和二甲基异亮氨酸染料的染料，或与如上定义的由通式（I）表示的至少一种敏化染料的超敏化组合和至少一种由通式（II）（II）其中Z 3表示形成5-或6-元杂环所必需的原子; Q表示形成绕丹宁环所需的原子，硫代乙内酰脲环或2-噻恶唑烷二酮环; R4表示含有至多4个碳原子的脂族基团，其可以是未取代的或取代的，并且其碳链可被氧原子或硫原子间隔; R5表示氢原子，烷基，芳基或芳烷基; n表示1或2。

4. 发明授权

US3973969A Silver halide photographic emulsion 失效
标题翻译：卤化银照相乳剂
公开(公告)号：US3973969A
公开(公告)日：1976-08-10
申请号：US574147
申请日：1975-05-02
申请人： Keisuke Shiba , Masanao Hinata , Hirotetu Kato , Akiro Sato , Akira Ogawa
发明人： Keisuke Shiba , Masanao Hinata , Hirotetu Kato , Akiro Sato , Akira Ogawa
IPC分类号： C09B23/06 , G03C1/29 , G03C1/14
CPC分类号： G03C1/29 , C09B23/06
摘要： Silver halide photographic emulsions are supersensitized by a combination of at least one sensitizing dye represent by following general formula (I): ##EQU1## And at least one sensitizing dye represented by following general formula (II): ##SPC1##Specific moieties given in the above formulae are identified in the specification.
摘要翻译：通过以下通式（I）表示的至少一种增感染料的组合使卤化银照相乳液过敏：ZRoZ1 | R1-N-C = CH-C = CH-C = N-R2（X） n-1 I +和由以下通式（II）表示的至少一种敏化染料：

5. 发明授权

US3955996A Method for spectrally sensitizing photographic light-sensitive emulsion 失效
标题翻译：摄影感光乳剂光谱增感方法
公开(公告)号：US3955996A
公开(公告)日：1976-05-11
申请号：US524185
申请日：1974-11-15
申请人： Masanao Hinata , Masanaga Ohki , Haruo Takei , Yuji Mihara
发明人： Masanao Hinata , Masanaga Ohki , Haruo Takei , Yuji Mihara
IPC分类号： G03C1/08 , G03C1/12 , G03C1/24 , G03C1/16
CPC分类号： G03C1/12
摘要： A method for spectrally sensitizing a photographic light-sensitive emulsion, which comprises dissolving a photographic spectrally sensitizing dye having an amidinium ion auxochrome in an organic solvent containing a substantially water-free acid having a pKa not exceeding about 5, and adding this dye-containing acid-organic solvent solution to a light-sensitive emulsion.
摘要翻译：一种用于对照相感光乳剂进行光谱增感的方法，其包括将具有脒离子辅助色素的照相光谱增感染料溶解在含有pKa不超过约5的基本上无水的酸的有机溶剂中，并加入该染料酸 - 有机溶剂溶液加到感光乳剂上。

6. 发明授权

US3930860A Spectrally sensitized color photographic materials suitable for high temperature rapid development 失效
标题翻译：适用于高温快速开发的光谱敏感型彩色摄影材料
公开(公告)号：US3930860A
公开(公告)日：1976-01-06
申请号：US429983
申请日：1974-01-02
申请人： Keisuke Shiba , Masanao Hinata , Seiiti Kubodera
发明人： Keisuke Shiba , Masanao Hinata , Seiiti Kubodera
IPC分类号： G03C7/26 , G03C1/12 , G03C7/00
CPC分类号： G03C1/12
摘要： A light-sensitive silver halide material for the high temperature and rapid color development at least 30.degree.C, which light-sensitive silver halide material comprises at least one spectrally sensitized silver halide photographic emulsion layer, the emulsion layer containing at least one sensitizing dye having an halogen ion concentration increasing effect.

7. 发明授权

US4040833A Radiographic process and sensitive material for the same 失效
标题翻译：摄影过程和敏感材料相同
公开(公告)号：US4040833A
公开(公告)日：1977-08-09
申请号：US672947
申请日：1976-04-02
申请人： Masanao Hinata , Haruo Takei , Nobuaki Miyasaka , Kenji Takahashi
发明人： Masanao Hinata , Haruo Takei , Nobuaki Miyasaka , Kenji Takahashi
IPC分类号： C09K11/77 , G03C1/28 , G03C5/16 , G03C5/17 , G21K4/00 , G03C1/92 , G03C1/14
CPC分类号： C09K11/7771 , G03C1/28 , G03C5/16 , G03C5/17 , G21K4/00 , Y10S430/167
摘要： In a process for forming radiographic images which comprises exposing a photograhic sensitive material comprising a support and at least one silver halide photographic emulsion layer to radiation from a fluorescent intensifying screen to form a latent image and thereafter developing the same, the improvement which comprises the fluorescent intensifying screen having a maximum emission wavelength in the range of about 500 to about 570 nm and a distribution such that at least about 1/2 of the emission energy is at a wavelength of above about 400 nm, and said silver halide photographic emulsion layer contains at least one sensitizing dye represented by formula (I) and at least one sensitizing dye represented by formula (II): ##STR1## WHEREIN R.sub.o represents an alkyl group and R.sub.1 and R.sub.2 each represent an alkyl group but at least one of R.sub.1 and R.sub.2 represents a sulfoalkyl group, X represents an anion, and m represents an integer of 1 or 2, and m = 1 when the dye forms an inner salt; ##STR2## wherein Z represents the group of atoms necessary to complete a benzoxazole nucleus, R.sub.3 represents an alkyl group, and Q represents the group of atoms necessary to complete a 2-thioimidazolidine-2,4-dione nucleus.
摘要翻译：在用于形成放射线照相图像的方法中，其包括将包含支持体和至少一个卤化银照相乳剂层的照相感光材料暴露于来自荧光增强屏幕的辐射以形成潜像，然后显影，其改进包括荧光具有约500至约570nm范围内的最大发射波长的增强屏幕和使得至少约1/2的发射能量在高于约400nm的波长处的分布，并且所述卤化银照相乳剂层含有至少一种由式（I）表示的敏化染料和至少一种由式（II）表示的敏化染料：（I）其中R a表示烷基，R 1和R 2各自表示烷基，但是至少一个 R1和R2表示磺基烷基，X表示阴离子，m表示1或2的整数，当染料形成内盐时m = 1; 其中Z表示完成苯并恶唑核所需的原子团，R 3表示烷基，Q表示完成2-硫代咪唑烷-2,4-二酮核所需的原子团。

8. 发明授权

US4039335A Photographic silver halide emulsions 失效
标题翻译：摄影卤化银乳剂
公开(公告)号：US4039335A
公开(公告)日：1977-08-02
申请号：US737130
申请日：1976-10-29
申请人： Masanao Hinata , Haruo Takei , Akira Sato , Atsuo Iwamoto , Jun Hayashi
发明人： Masanao Hinata , Haruo Takei , Akira Sato , Atsuo Iwamoto , Jun Hayashi
IPC分类号： G03C1/28 , G03C1/29 , G03C1/14
CPC分类号： G03C1/29
摘要： A silver halide photographic emulsion spectrally sensitized with a combination of sensitizing dyes consisting essentially of at least one sensitizing dye represented by the following general formula [I] and at least one sensitizing dye represented by the following general formula [II] in supersensitizing amounts: ##STR1## wherein R.sup.1 and R.sup.2 each is an alkyl group, R.sup.3 is an alkyl group, X.sub.1 is an acidic anion, m is 1 or 2, and m is 1 when the dye forms an intramolecular salt (betaine-like structure). ##STR2## WHEREIN Z.sup.1 is a sulfur atom or a selenium atom, Z.sup.2 is an atomic group necessary to form a benzothiazole ring, a benzoselenazole ring, a naphtho[1,2-d]thiazole ring or a naphtho[1,2-d]selenazole ring, R.sup.4 and R.sup.5 is an alkyl group, R.sup.6 is an alkyl group, a phenyl group, an aralkyl group, a furyl group or a thienyl group, X.sub.2 is an acidic anion, n is 1 or 2, and n is 1 when the dye forms an intramolecular salt (betaine-like structure).
摘要翻译：用基本上由以下通式[I]表示的至少一种敏化染料和至少一种由以下通式[II]表示的敏化染料在超敏化剂中组合的敏化染料的光致增感的卤化银照相乳剂：一般其中R1和R2各自为烷基，R3为烷基，X1为酸性阴离子，m为1或2，当染料形成分子内时，m为1 盐（甜菜碱样结构）。通式[II]其中Z 1为硫原子或硒原子，Z 2为形成苯并噻唑环所需的原子团，苯并硒唑环，萘并[1,2-d]噻唑环或萘并[ 1,2-d]硒唑环，R4和R5是烷基，R6是烷基，苯基，芳烷基，呋喃基或噻吩基，X2是酸性阴离子，n是1或2 ，当染料形成分子内盐（甜菜碱样结构）时，n为1。

9. 发明授权

US4021247A Method of dispersing organic compounds useful in photography 失效
标题翻译：分散有机化合物的分散方法
公开(公告)号：US4021247A
公开(公告)日：1977-05-03
申请号：US523650
申请日：1974-11-13
申请人： Masanao Hinata , Yuji Mihara
发明人： Masanao Hinata , Yuji Mihara
IPC分类号： B65H3/00 , G03C1/005 , G03C1/06 , G03C7/388 , E03C1/02 , E03C1/28
CPC分类号： G03C1/005 , G03C7/388
摘要： A method for dispersing organic compounds which are substantially insoluble in water and are used in photographic materials, such as chemical sensitizers (except spectral sensitizing dyes), antifoggants, antioxidants, ultraviolet absorbents, color couplers, coating aids, hardening agents, etc., effectively in a silver halide photosensitive emulsion comprising dissolving the organic compounds in an acid having a pKa of not over about 5, such as methanesulfonic acid, ethanesulfonic acid, etc., and adding the solution to the silver halide photosensitive emulsion directly or after dispersing in an aqueous solution.
摘要翻译：用于分散有机化合物的方法，该方法基本上不溶于水并用于照相材料，如化学增感剂（光谱增感染料除外），防灰雾剂，抗氧化剂，紫外线吸收剂，着色剂，涂料助剂，硬化剂等在包含将有机化合物溶解在pKa不超过约5的酸中的卤化银感光乳剂中，如甲磺酸，乙磺酸等，并将溶液直接或分散在卤化银感光乳剂中水溶液。

10. 发明授权

US4002480A Photographic silver halide emulsion 失效
标题翻译：摄影卤化银乳剂
公开(公告)号：US4002480A
公开(公告)日：1977-01-11
申请号：US555912
申请日：1975-03-06
申请人： Masanao Hinata , Yuji Mihara , Reiichi Ohi , Keiichi Adachi , Akira Sato
发明人： Masanao Hinata , Yuji Mihara , Reiichi Ohi , Keiichi Adachi , Akira Sato
IPC分类号： G03C1/12 , G03C1/22 , G03C1/28 , G03C1/34 , G03C1/08
CPC分类号： G03C1/34 , G03C1/12 , G03C1/22 , G03C1/28
摘要： A photographic silver halide emulsion containing at least one dinuclear merocyanine sensitizing dye, and at least one compound represented by the following formula: ##STR1## wherein D represents a divalent aromatic group, R.sub.2, R.sub.3, R.sub.4, and R.sub.5 each represents a hydrogen atom, a hydroxyl group, an alkoxyl group, an aryloxy group, a halogen atom, a heterocyclic group, a mercapto group, an alkylthio group, an arylthio group, a heterocyclic thio group, an amino group, an alkylamino group, a cycloalkylamino group, an arylamino group, a heterocyclic amino group, an aralkylamino group, or an aryl group.
摘要翻译：含有至少一种双核部花菁敏化染料的照相卤化银乳剂和至少一种由下式表示的化合物：其中D表示二价芳族基团，R 2，R 3，R 4和R 5各自表示氢原子，羟基，烷氧基，芳氧基，卤素原子，杂环基，巯基，烷硫基，芳硫基，杂环硫基，氨基，烷基氨基，环烷基氨基，芳基氨基，杂环氨基，芳烷基氨基或芳基。

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