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1. 发明授权

US09371236B2 Highly efficient method for producing ceramic microparticles 有权
标题翻译：高效制备陶瓷微粒的方法
公开(公告)号：US09371236B2
公开(公告)日：2016-06-21
申请号：US14004117
申请日：2011-03-23
申请人： Jun Kuraki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
发明人： Jun Kuraki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
IPC分类号： B01J14/00 , C01B33/113 , C01B13/14 , C01B21/00 , C01B19/00 , C01B31/00 , C01B33/00 , C01B35/00 , C01B9/00 , B01F7/00 , C01B33/193 , C01G9/02 , C01G23/00 , C01B13/36 , B01J19/18 , C01B13/16 , C04B35/626
CPC分类号： C01B33/113 , B01F7/00775 , B01F7/00791 , B01J14/00 , B01J19/1887 , C01B9/00 , C01B13/14 , C01B13/16 , C01B13/36 , C01B19/00 , C01B21/00 , C01B32/00 , C01B33/00 , C01B33/193 , C01B35/00 , C01G9/02 , C01G23/003 , C01P2002/72 , C01P2004/04 , C04B35/62625 , C04B2235/3284 , C04B2235/3418 , C04B2235/5445 , C04B2235/5454 , C04B2235/76
摘要： Provided is a more suitable method for producing ceramic microparticles. The present invention uses at least two types of fluids to be processed; at least one of the fluids to be processed is a fluid containing a ceramic starting material liquid that mixes and/or dissolves a ceramic starting material in a basic solvent; of the fluids aside from the ceramic starting material liquid, at least one of the fluids to be processed is a fluid containing a solvent for precipitating ceramic microparticles; and ceramic microparticles are precipitated by mixing the fluid containing the ceramic starting material liquid and the fluid containing the solvent for precipitating ceramic microparticles within a thin film fluid formed between at least two surfaces (1,2) for processing that are provided facing each other, are able to approach and separate each other, and of which one is able to rotate with respect to the other. Ceramic microparticles having as increased crystallinity are obtained by mixing the fluid containing the precipitated ceramic microparticles precipitate and a fluid containing an acidic substance.
摘要翻译：提供了一种更合适的陶瓷微粒的制造方法。本发明使用至少两种待处理的流体; 要处理的流体中的至少一种是含有在碱性溶剂中混合和/或溶解陶瓷原料的陶瓷原料液的流体; 的待处理流体中的至少一种是含有用于沉淀陶瓷微粒的溶剂的流体; 并且通过将包含陶瓷原料液的流体和含有溶剂的流体混合在陶瓷微粒沉淀物内形成的至少两个彼此面对的表面（1,2）之间形成的薄膜流体中来沉淀陶瓷微粒，能够彼此接近和分离，并且能够相对于另一个旋转。通过混合含有沉淀的陶瓷微粒沉淀物的液体和含有酸性物质的流体，获得结晶度增加的陶瓷微粒。

2. 发明申请

US20140001663A1 METHOD FOR PRODUCING MICROPARTICLES 有权
标题翻译：生产微生物的方法
公开(公告)号：US20140001663A1
公开(公告)日：2014-01-02
申请号：US14005506
申请日：2012-03-21
申请人： Jun Kuraki , Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
发明人： Jun Kuraki , Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
IPC分类号： B01F3/22
CPC分类号： B01F3/22 , B01F7/00775 , B01F7/00791 , B01F13/1027 , B01F2215/0481 , B01J19/10 , B01J19/1806 , B01J19/1875 , B01J19/1887 , B01J19/20 , B01J2219/00779 , B82Y30/00 , C01G9/02 , C01P2004/54 , C01P2004/64
摘要： The problem addressed by the present invention is to provide a method for producing microparticles. Provided is a method that is for producing microparticles and that is characterized by containing at least the the following two steps: (I) a step for preparing a microparticle starting material solution by dissolving at least one type of microparticle starting material in a solvent using high speed stirring or ultrasonic waves, and (II) a step for precipitating microparticles by mixing the microparticle starting material solution and at least one type of precipitation solvent for precipitating the microparticle starting material in a thin film fluid formed between at least two processing surfaces that are disposed facing each other, are able to approach/separate from each other, and of which at least one rotates relative to the others.
摘要翻译：本发明提出的问题在于提供一种微粒的制造方法。本发明提供一种生产微粒的方法，其特征在于，至少包含以下两个步骤：（I）通过使用高分子量将至少一种微粒原料溶解在溶剂中来制备微粒原料溶液的步骤速度搅拌或超声波，以及（II）通过将微粒原料溶液和至少一种沉淀溶剂混合使微粒起始材料沉淀在形成在至少两个处理表面之间的薄膜流体中而使微粒沉淀的步骤彼此面对地布置，能够彼此接近/分离，并且其中至少一个相对于另一个旋转。

3. 发明申请

US20130274462A1 HIGHLY HEAT-RESISTANT PHTHALOCYANINE 有权
标题翻译：高耐热PHTHALOCYANINE
公开(公告)号：US20130274462A1
公开(公告)日：2013-10-17
申请号：US13989082
申请日：2011-11-22
申请人： Masaki Maekawa , Daisuke Honda , Masakazu Enomura
发明人： Masaki Maekawa , Daisuke Honda , Masakazu Enomura
IPC分类号： C07F3/06 , C07F1/08
CPC分类号： C07F3/06 , B01D11/0269 , B01F3/0861 , B82Y30/00 , C01P2004/64 , C01P2004/82 , C07F1/08 , C09B67/0017 , C09B67/0019 , C09B67/0026 , C09B67/0035 , C09B67/0092 , C09C1/0081 , C09C1/04 , C09C1/627
摘要： The problem addressed by the present invention is to provide a high heat-resistant phthalocyanine. The phthalocyanine is separated by mixing a phthalocyanine separation solvent and a phthalocyanine solution wherein a phthalocyanine starting material is dissolved in a solvent. THe phthalocyanine is wherein having high heat resistance, the decomposition temperature of the separated phthalocyanine being at least 10° C. higher than the decomposition temperature of the phthalocyanine starting material. Also, the phthalocyanine solution may be the result of dissolving at least two types of phthalocyanine starting material in the solvent, the separated phthalocyanine being wherein containing a solid solvent of the at least two types of phthalocyanine starting material and by the decomposition temperature of the separated phthalocyanine being at least 10° C. higher than the decomposition temperature of a mixture of at least two types of phthalocyanine separated by mixing the phthalocyanine separation solvent and each of at least two types of phthalocyanine solution resulting from dissolving each of the at least two types of phthalocyanine starting material in a solvent.
摘要翻译：本发明解决的问题是提供高耐热酞菁。通过混合酞菁分离溶剂和酞菁溶液将酞菁原料溶解在溶剂中来分离酞菁。其中酞菁具有高耐热性，分离的酞菁的分解温度比酞菁起始原料的分解温度高至少10℃。此外，酞菁溶液可能是将至少两种类型的酞菁原料溶解在溶剂中的结果，其中分离的酞菁含有至少两种类型的酞菁起始原料的固体溶剂和分离的酞菁比通过混合酞菁分离溶剂和由至少两种类型的酞菁溶液中分离出的至少两种类型的酞菁溶液中的至少两种类型的酞菁溶液的分解温度高至少两种类型的酞菁的分解温度高至少10℃ 的酞菁原料在溶剂中。

4. 发明申请

US20130071664A1 NOVEL COPPER PHTHALOCYANINE PIGMENT AND METHOD FOR PRODUCING COPPER PHTHALOCYANINE MICROPARTICLES 有权
标题翻译：新型铜酞菁颜料和生产铜酞菁微量元素的方法
公开(公告)号：US20130071664A1
公开(公告)日：2013-03-21
申请号：US13701162
申请日：2011-03-04
申请人： Masaki Maekawa , Daisuke Honda , Masakazu Enomura
发明人： Masaki Maekawa , Daisuke Honda , Masakazu Enomura
IPC分类号： C09B47/04 , B82B1/00
CPC分类号： C09B67/0026 , C09B67/0019 , Y10T428/2982
摘要： Disclosed are: copper phthalocyanine pigments which each contain at least one kind of copper phthalocyanine microparticles that has high spectral characteristics and that is in a crystal form other than α-form; and processes for the production of the copper phthalocyanine microparticles. Provided are: a copper phthalocyanine pigment which contains at least one kind of copper phthalocyanine microparticles that is in a crystal form other than α-form and that exhibits, in a region of 380 nm to 780 nm, an absorption spectrum shape extremely similar to that of α-form copper phthalocyanine microparticles; and a process for the production of the copper phthalocyanine microparticles. Also provided are: a copper phthalocyanine pigment which contains at least one kind of copper phthalocyanine microparticles that is in a crystal form other than α- or ε-form and that exhibits a wavelength (λmax) of shorter than 478 nm in the transmission spectrum in a region of 380 nm to 780 nm, said wavelength (λmax) being a wavelength at which the maximum transmittance appears; and a process for the production of the copper phthalocyanine microparticles.
摘要翻译：公开了：铜酞菁颜料，其各自含有至少一种具有高光谱特性且为α型以外的结晶形式的铜酞菁微粒; 以及铜酞菁微粒的制造方法。提供：铜酞菁颜料，其含有至少一种不同于α-形式的结晶形式的铜酞菁微粒，并且在380nm至780nm的区域中显示出与其非常相似的吸收光谱形状的α型铜酞菁微粒; 以及生产铜酞菁微粒的方法。还提供：铜酞菁颜料，其含有除了α-或其它结晶形式的晶体形式的至少一种铜酞菁微粒，并且在透射光谱中表现出小于478nm的波长（λmax）在380nm至780nm的区域中，所述波长（λmax）是出现最大透射率的波长; 以及生产铜酞菁微粒的方法。

5. 发明授权

US09492763B2 Method for producing microparticles having controlled crystallite diameter 有权
标题翻译：具有受控微晶直径的微粒的制造方法
公开(公告)号：US09492763B2
公开(公告)日：2016-11-15
申请号：US14232124
申请日：2012-07-05
申请人： Shiho Aoyagi , Kaeko Araki , Masaki Maekawa , Jun Kuraki , Masakazu Enomura
发明人： Shiho Aoyagi , Kaeko Araki , Masaki Maekawa , Jun Kuraki , Masakazu Enomura
IPC分类号： B01D9/00 , C04B35/626 , C22B15/00 , B01J19/18
CPC分类号： B01D9/0063 , B01D9/0054 , B01J19/1887 , B01J2219/00085 , B01J2219/00164 , B01J2219/00177 , C04B35/626 , C22B15/0089
摘要： At least two types of fluids to be processed are mixed in a thin film fluid formed between at least two processing surfaces which are approachably and separably disposed facing each other. At least one processing surface rotates relative to the other, and a substance to be separated giving a controlled crystallite diameter is caused to separate. Specific conditions related to a fluid to be processed are varied to control the crystallite diameter of the substance to be separated. The specific conditions are the type of substance to be separated; the concentration of the substance to be separated included in the raw material fluid and/or substance included in the separating fluid; the pH of the raw material fluid and/or separating material fluid; the introduction temperature of the raw material fluid and/or separating fluid; and the introduction velocity of the raw material fluid and/or separating fluid.
摘要翻译：要处理的至少两种类型的流体在形成在彼此面对地和可分离地布置的至少两个处理表面之间的薄膜流体中混合。至少一个处理表面相对于另一个处理表面旋转，并且使被分离得到受控微晶直径的物质分离。改变与待处理流体有关的特定条件以控制待分离物质的微晶直径。具体条件是要分离的物质的类型; 要分离的物质的浓度包括在分离流体中包含的原料流体和/或物质中; 原料流体和/或分离材料流体的pH; 原料流体和/或分离流体的引入温度; 以及原料流体和/或分离流体的引入速度。

6. 发明授权

US09481694B2 Solid solution pigment nanoparticles and method for producing solid solution pigment nanoparticles having controlled solid solution ratio 有权
标题翻译：固溶颜料纳米颗粒和固溶颜料纳米粒子的制备方法，其具有可控的固溶比
公开(公告)号：US09481694B2
公开(公告)日：2016-11-01
申请号：US13883692
申请日：2011-05-20
申请人： Masaki Maekawa , Kaeko Araki , Hideyuki Oka , Daisuke Honda , Masakazu Enomura
发明人： Masaki Maekawa , Kaeko Araki , Hideyuki Oka , Daisuke Honda , Masakazu Enomura
IPC分类号： B01D11/02 , B01F3/08 , B01F3/22 , B29B7/38 , C09B67/02 , C09C1/62 , C07F3/06 , C09B67/14 , C09B67/22 , C09C1/00 , C09C1/04 , C07F1/08 , B82Y30/00 , C09B67/42 , C09B67/16 , C09B67/50
CPC分类号： C07F3/06 , B01D11/0269 , B01F3/0861 , B82Y30/00 , C01P2004/64 , C01P2004/82 , C07F1/08 , C09B67/0017 , C09B67/0019 , C09B67/0026 , C09B67/0035 , C09B67/0092 , C09C1/0081 , C09C1/04 , C09C1/627
摘要： The problem addressed by the present invention is to provide; solid solution pigment nanoparticles having a homogeneous solid solution ratio; a method for producing solid solution pigment nanoparticles having a homogeneous solid solution ratio in each primary particle; and a method for controlling the solid solution ratio of solid solution pigment nanoparticles. The solid solution pigment nanoparticles are prepared by precipitating at least two types of pigment by mixing a pigment precipitation solvent and; at least one type of pigment solution wherein at least two types of pigment are dissolved in a solvent: or at least two types of pigment solution wherein at least one type of pigment is dissolved in a solvent. The solid solution pigment nanoparticles are wherein the solid solution ratio of the at least two types of pigment in the primary particles of the precipitated solid solution pigment nanoparticles with respect to the ratio of the at least two types of pigment in the pigment solution mixed with the pigment precipitation solvent having a precision within 25%.
摘要翻译：本发明提出的问题在于：具有均匀固溶比的固溶颜料纳米粒子; 一种在一次粒子中具有均匀固溶比的固溶颜料纳米粒子的制造方法; 以及控制固溶颜料纳米粒子的固溶比的方法。固溶颜料纳米粒子是通过混合颜料沉淀溶剂和至少两种颜料沉淀来制备的; 至少一种类型的颜料溶液，其中至少两种类型的颜料溶解在溶剂中：或至少两种类型的颜料溶液，其中至少一种类型的颜料溶解在溶剂中。固溶颜料纳米粒子，其中沉淀的固溶颜料纳米颗粒的初级颗粒中的至少两种类型的颜料的固溶比相对于颜料溶液中的至少两种类型的颜料与颜料沉淀溶剂的精度在25％以内。

7. 发明授权

US09127331B2 Method for producing oxide/hydroxide 有权
标题翻译：生产氧化物/氢氧化物的方法
公开(公告)号：US09127331B2
公开(公告)日：2015-09-08
申请号：US14112887
申请日：2011-04-28
申请人： Jun Kuraki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
发明人： Jun Kuraki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
IPC分类号： C22B19/00 , C22B19/34 , C01B13/32 , C01B13/34 , C01G9/02 , C01G9/03 , B01F7/00 , B01F15/02 , B01F3/08 , B82Y30/00
CPC分类号： C22B19/34 , B01F3/0807 , B01F7/00775 , B01F7/00791 , B01F15/0203 , B01F15/0243 , B01F15/0291 , B82Y30/00 , C01B13/32 , C01B13/34 , C01G9/02 , C01G9/03 , C01P2002/01 , C01P2002/72 , C01P2002/88 , C01P2004/04 , C01P2004/62 , C01P2004/64
摘要： Provided is a method for producing an oxide and/or hydroxide wherein the ratio of oxide and hydroxide has been controlled. The method produces an oxide, a hydroxide, or a mixture thereof, and obtains an oxide and/or a hydroxide wherein the ratio of oxide and hydroxide has been controlled by means of changing a specific condition relating to at least one fluid to be processed introduced between processing surfaces (1, 2) when causing the precipitation of the oxide, hydroxide, or mixture thereof by mixing an basic fluid containing at least one type of basic substance and a fluid containing at least one type of metal or metallic substance as the fluids to be processed between the processing surfaces (1, 2) that are provided facing each other, are able to approach to and separate from each other, and of which at least one rotates relative to the other. The specific condition is at least one condition selected from the group consisting of: the speed of introduction of at least one of the fluids to be processed; and the pH of at least one of the fluids to be processed.
摘要翻译：提供一种氧化物和/或氢氧化物的制造方法，其中氧化物和氢氧化物的比例已被控制。该方法产生氧化物，氢氧化物或其混合物，并获得氧化物和/或氢氧化物，其中氧化物和氢氧化物的比例已经通过改变与至少一种待处理流体相关的特定条件来控制当通过混合含有至少一种碱性物质的碱性流体和含有至少一种类型的金属或金属物质的流体作为流体而使氧化物，氢氧化物或其混合物沉淀时，处理表面（1,2）之间在彼此面对地设置的处理表面（1,2）之间进行处理，能够彼此接近并分离，并且至少一个相对于另一个旋转。所述具体条件是选自以下的至少一种条件：至少一种待处理流体的引入速度; 和至少一种要处理的流体的pH。

8. 发明申请

US20140155247A1 METHOD FOR PRODUCING MICROPARTICLES HAVING CONTROLLED CRYSTALLITE DIAMETER 有权
标题翻译：用于生产具有控制的结晶直径的微孔的方法
公开(公告)号：US20140155247A1
公开(公告)日：2014-06-05
申请号：US14232124
申请日：2012-07-05
申请人： Shiho Aoyagi , Kaeko Araki , Masaki Maekawa , Jun Kuraki , Masakazu Enomura
发明人： Shiho Aoyagi , Kaeko Araki , Masaki Maekawa , Jun Kuraki , Masakazu Enomura
IPC分类号： B01D9/00 , C04B35/626 , C22B15/00
CPC分类号： B01D9/0063 , B01D9/0054 , B01J19/1887 , B01J2219/00085 , B01J2219/00164 , B01J2219/00177 , C04B35/626 , C22B15/0089
摘要： At least two types of fluids to be processed are mixed in a thin film fluid formed between at least two processing surfaces which are approachably and separably disposed facing each other. At least one processing surface rotates relative to the other, and a substance to be separated giving a controlled crystallite diameter is caused to separate. Specific conditions related to a fluid to be processed are varied to control the crystallite diameter of the substance to be separated. The specific conditions are the type of substance to be separated; the concentration of the substance to be separated included in the raw material fluid and/or substance included in the separating fluid; the pH of the raw material fluid and/or separating material fluid; the introduction temperature of the raw material fluid and/or separating fluid; and the introduction velocity of the raw material fluid and/or separating fluid.
摘要翻译：要处理的至少两种类型的流体在形成在彼此面对地和可分离地布置的至少两个处理表面之间的薄膜流体中混合。至少一个处理表面相对于另一个处理表面旋转，并且使被分离得到受控微晶直径的物质分离。改变与待处理流体有关的特定条件以控制待分离物质的微晶直径。具体条件是要分离的物质的类型; 要分离的物质的浓度包括在分离流体中包含的原料流体和/或物质中; 原料流体和/或分离材料流体的pH; 原料流体和/或分离流体的引入温度; 以及原料流体和/或分离流体的引入速度。

9. 发明申请

US20130156682A1 METHOD FOR PRODUCING ISOLATABLE OXIDE MICROPARTICLES OR HYDROXIDE MICROPARTICLES 有权
标题翻译：生产不溶性氧化镁微量元素或羟基微量元素的方法
公开(公告)号：US20130156682A1
公开(公告)日：2013-06-20
申请号：US13818954
申请日：2011-08-26
申请人： Jun Kuraki , Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
发明人： Jun Kuraki , Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
IPC分类号： C01G23/053 , C01F5/14 , C01F17/00
CPC分类号： C01G23/0536 , B01D9/0009 , B01F7/00775 , B01F7/00791 , B82Y30/00 , C01B13/36 , C01F5/02 , C01F5/14 , C01F5/20 , C01F17/0043 , C01G1/02 , C01G23/0532 , C01G25/02 , C01P2002/54 , C01P2004/04 , C01P2004/64
摘要： A method for producing isolatable oxide microparticles or hydroxide microparticles using an apparatus that processes a fluid between processing surfaces of processing members that are arranged opposite each other so as to be able to approach to or separate from each other and such that at least one can rotate relative to the other. At least two fluids are mixed and oxide microparticles or hydroxide microparticles are separated, said two fluids including: a fluid containing a microparticle raw material solution comprising a microparticle raw material mixed into a solvent, and a fluid containing a microparticle-separation solution. Immediately thereafter, the following are mixed to obtain isolatable oxide microparticles or hydroxide microparticles: a fluid containing the separated oxide microparticles or hydroxide microparticles; and a fluid containing a microparticle-treatment-substance-containing solution that contains a microparticle-treatment substance that adjusts the dispersibility of the separated oxide microparticles or hydroxide microparticles.
摘要翻译：一种用于制造可分离氧化物微粒或氢氧化物微粒的方法，该方法使用处理相互相对布置的处理构件的处理表面之间的流体以便能够彼此接近或分离并使得至少一个可旋转的装置相对于另一个。混合至少两种流体，分离氧化物微粒或氢氧化物微粒，所述两种流体包括：含有混合在溶剂中的微粒原料的微粒原料溶液的流体和含有微粒分离溶液的流体。之后，混合以下物质，得到可分离的氧化物微粒或氢氧化物微粒：含有分离的氧化物微粒或氢氧化物微粒的流体; 以及含有含微粒处理物质的溶液的流体，其含有调节分离的氧化物微粒或氢氧化物微粒的分散性的微粒处理物质。

10. 发明申请

US20130078467A1 NOVEL QUINACRIDONE PIGMENT COMPOSITION, AND METHOD FOR PRODUCING QUINACRIDONE MICROPARTICLES 审中-公开
标题翻译：新型喹吖啶酮颜料组合物及其生产喹诺酮类微量元素的方法
公开(公告)号：US20130078467A1
公开(公告)日：2013-03-28
申请号：US13702270
申请日：2011-03-04
申请人： Masaki Maekawa , Daisuke Honda , Masakazu Enomura
发明人： Masaki Maekawa , Daisuke Honda , Masakazu Enomura
IPC分类号： C09D7/00 , B29B9/10
CPC分类号： C09D7/41 , B29B9/10 , B82Y30/00 , C09B67/0014 , C09B67/0027 , C09B67/0096 , C09D11/322 , G02B5/22 , G03G9/092 , Y10S977/773 , Y10S977/788 , Y10S977/90 , Y10T428/2982
摘要： A quinacridone pigment composition contains quinacridone microparticles which have durability and spectral characteristics equivalent to those required for a magenta color of a dye. The quinacridone pigment composition contains at least one type of quinacridone microparticles, wherein a difference between the maximum transmittance (Tmax1) and the minimum transmittance (Tmin) is 80% or more in a transmission spectrum at 350 nm to 800 nm and the difference between the maximum and minimum transmittance is 30% or more in a transmission spectrum at 350 nm to 580 nm, or the difference between the maximum transmittance (Tmax1) and the minimum transmittance (Tmin) is 80% or more in a transmission spectrum at 350 nm to 800 nm and the wavelength (λmax) at which the transmittance in a transmission spectrum at 350 nm to 500 nm becomes maximum is less than 430 nm. A method is provided for producing the quinacridone microparticles.
摘要翻译：喹吖啶酮颜料组合物含有具有与染料品红色所需的耐久性和光谱特性相同的喹吖啶酮微粒。喹吖啶酮颜料组合物含有至少一种喹吖啶酮微粒，其中，在350nm〜800nm的透射光谱中，最大透射率（Tmax1）与最小透射率（Tmin）之间的差为80％以上，在350nm至580nm的透射光谱中，最大透射率和最小透射率为30％以上，或者在350nm〜550nm的透射光谱中，最大透射率（Tmax1）与最小透射率（Tmin）之间的差为80％以上在350nm至500nm的透射光谱中的透射率变为最大的波长（λmax）小于430nm。提供了制备喹吖啶酮微粒的方法。

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