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1. 发明专利

JP2004107345A Anti-perspirant composition gentle to skin, and preparation method therefor 审中-公开
公开(公告)号：JP2004107345A
公开(公告)日：2004-04-08
申请号：JP2003323396
申请日：2003-09-16
申请人： Reheis Inc , リヘイスインコーポレイテッド
发明人： PAREKH JAWAHAR C , LI ZIJUN
IPC分类号： A61K8/20 , A61K8/26 , A61K8/28 , A61K8/34 , A61K8/44 , A61Q15/00 , A61K7/38
CPC分类号： A61K8/44 , A61K8/26 , A61K8/28 , A61K8/345 , A61K2800/58 , A61Q15/00
摘要： PROBLEM TO BE SOLVED: To obtain an anti-perspiration activator composition having an improved combination of functional characteristics such as superior perspiration inhibitability, skin conditioning, moisture retaining in prescribing an anti-perspirant stick.
SOLUTION: An improved anti-perspirant gentle to skin is obtained by complexing a suitable polyhydroxy alcohol, for example, glycerol, with an anti-perspirant that is generally considered to be an anti-perspiration activator material and takes a form of an active or in-active aluminum or an aluminum/zirconium salt designated in the FDA OTC Tentative Final Monograph.
COPYRIGHT: (C)2004,JPO

2. 发明专利

JP2004035553A Amino acid-free and stable aluminum / zirconium anti-perspirant solution 审中-公开
公开(公告)号：JP2004035553A
公开(公告)日：2004-02-05
申请号：JP2003184271
申请日：2003-06-27
申请人： Reheis Inc , リヘイスインコーポレイテッド
发明人： LI ZIJUN , PAREKH JAWAHAR CHUNILAL
IPC分类号： A61K8/20 , A61K8/23 , A61K8/26 , A61K8/28 , A61K8/34 , A61Q15/00 , A61K7/34 , A61K7/38
CPC分类号： A61K8/28 , A61K8/26 , A61K8/345 , A61Q15/00
摘要： PROBLEM TO BE SOLVED: To prepare a stable aluminum-zirconium anti-perspirant solution containing a high amount of an active material, requiring no amino acid such as glycine and simply produced.
SOLUTION: The anti-perspirant is an amino acid-free and stable aqueous aluminum-zirconium solution and comprises about 20-55% active anti-perspirant material as anhydrous solid content, about 20-75 mass% water and about 1-20 mass% polyhydric alcohol having at least two carbon atoms and at least two hydroxy groups. The aqueous solution has about 0.8-10 Aluminum/Zirconium ratio and 0.8-2.1 metal/chloride ratio.
COPYRIGHT: (C)2004,JPO

3. 发明专利

JP2004285049A New perspiration suppressor/deodorant for stick and soft solid without having white residual material 审中-公开
标题翻译：用于固体和软固体的新型吸收抑制剂/除臭剂，不含白色残留物
公开(公告)号：JP2004285049A
公开(公告)日：2004-10-14
申请号：JP2003398140
申请日：2003-10-23
申请人： Reheis Inc , リヘイスインコーポレイテッド
发明人： PAREKH JAWAHAR C , AMIN PRADIP T
IPC分类号： A61K8/25 , A61K8/26 , A61K8/28 , A61K8/31 , A61K8/33 , A61K8/34 , A61K8/37 , A61K8/39 , A61K8/40 , A61K8/60 , A61K8/86 , A61K8/89 , A61K8/891 , A61Q15/00 , C08L83/04 , A61K7/38
CPC分类号： A61K8/26 , A61K8/28 , A61Q15/00
摘要： PROBLEM TO BE SOLVED: To improve a perspiration suppression active agent formulation with which white residual materials can not be discernible by eyes even against a black colored background by reducing particle size at a point of losing a capacity of forming an interaction discernible by the eyes, which interaction is formed between the perspiration suppression active agent and the passage of a light wave when using a refractive index-modifier.
SOLUTION: The perspiration suppression active agent composition is provided by containing a specific active agent, having 1.40-1.50 refractive index of a selected non-aqueous phase, perspiration suppression agent of
摘要翻译：要解决的问题：为了改善出汗抑制活性剂配方，白色残留物质即使在黑色背景下也不能被黑色背景识别，通过在失去形成可辨别的相互作用的能力的位置上减小粒径眼睛，当使用折射率调节剂时，在排汗抑制活性剂和光波通过之间形成相互作用。排汗抑制活性剂组合物是通过含有特定的活性剂提供的，具有选择的非水相的1.40-1.50的折射率，平均粒度为3μm的排汗抑制剂和润湿时的<50,000粘度。版权所有（C）2005，JPO＆NCIPI

4. 发明专利

JP2004161772A Antiperspirant composition with enhanced efficacy containing strontium 审中-公开
公开(公告)号：JP2004161772A
公开(公告)日：2004-06-10
申请号：JP2003382688
申请日：2003-11-12
申请人： Reheis Inc , リヘイスインコーポレイテッド
发明人： LI ZIJUN , PAREKH JAWAHAR C
IPC分类号： A61K8/19 , A61K8/20 , A61K8/26 , A61K8/28 , A61K8/34 , A61K8/44 , A61Q15/00 , C07F3/00 , A61K7/38 , A61K7/34
CPC分类号： A61K8/19 , A61K8/26 , A61K8/28 , A61K8/44 , A61Q15/00
摘要： PROBLEM TO BE SOLVED: To provide an antiperspirant composition with enhanced efficacy and stability and to provide a method for making the same.
SOLUTION: Antiperspirant actives of aluminum and aluminum-zirconium with enhanced efficacy containing strontium and an amino acid that have a stable high Band III/II ratio of HPLC are disclosed. The invention also discloses method for making the antiperspirant actives.
COPYRIGHT: (C)2004,JPO

5. 发明申请

WO2008070218A1 POLYALUMINUM CALCIUM HYDROXYCHLORIDES AND METHODS OF MAKING THE SAME 审中-公开
标题翻译：聚羟基羟基氯化镁及其制备方法
公开(公告)号：WO2008070218A1
公开(公告)日：2008-06-12
申请号：PCT/US2007/075433
申请日：2007-08-08
申请人： Reheis, Inc. , LI, Zijun , REREK, Mark , JANAK, Kevin
发明人： LI, Zijun , REREK, Mark , JANAK, Kevin
IPC分类号： C01F7/00 , C01F7/16 , C01F7/56 , A61Q15/00 , A61K8/26 , C02F1/52
CPC分类号： C01F7/002 , A61K8/26 , A61Q15/00 , C01F7/56 , C01P2002/87 , C01P2006/90 , C02F1/5245
摘要： A process is provided for the preparation of a novel polyaluminum calcium hydroxychloride composition of enhanced efficiency for water treatment, paper sizing, and antiperspirant applications. The polyaluminum calcium hydroxychloride compositions are prepared via the acidification of higher basicity reaction products to form mid-to-high basicity final products. Two methods are provided for the preparation of higher basicity products, contemplated in the first, and an aqueous acid solution, such as hydrochloric acid, aluminum chloride, or a mixture thereof, is mixed with a strong alkaline calcium salt such as calcium oxide or calcium carbonate and aluminum powder at temperatures greater than 60°C. In a second method, bauxite, aluminum hydrate, or aluminum metal, and calcium aluminate are mixed with hydrochloric acid and are reacted at high temperatures and/or elevated pressures for a certain period of time whereby, when the reaction is complete, the mixtures are filtered to obtain clear solutions. The final PAC-Ca solutions may be dried to powder to have a wide range of basicities from about 40% to about 80%. At lower basicities, the polyaluminum calcium hydroxychloride sales are used preferably as antiperspirants, while at higher basicities, the solutions are used preferably as water treatment chemicals.
摘要翻译：提供了一种制备用于水处理，纸张施胶和止汗剂应用的增强效率的新型聚羟基氯化铝羟氯化物组合物的方法。通过酸化较高的碱性反应产物来制备羟基氯化铝铝组合物，以形成中至高碱性的最终产物。提供两种方法用于制备较高碱度的产品，首先考虑，酸性溶液如盐酸，氯化铝或其混合物与强碱性钙盐如氧化钙或钙混合碳酸盐和铝粉末，温度大于60℃。在第二种方法中，将铝土矿，铝水合物或铝金属和铝酸钙与盐酸混合并在高温和/或高压下反应一段时间，由此当反应完成时，混合物为过滤以获得明确的解决方案。最终的PAC-Ca溶液可以被干燥成粉末以具有约40％至约80％的宽范围碱度。在较低的碱度下，聚羟基氯化钙销售优选用作止汗剂，而在较高碱度下，该溶液优选用作水处理化学品。

6. 发明申请

WO2007130143A3 PROCESS FOR PRODUCING STABLE POLYALUMINUM HYDROXYCHLORIDE AND POLYALUMINUM HYDROXYCHLOROSULFATE AQUEOUS SOLUTIONS 审中-公开
标题翻译：生产稳定的羟基氯化汞和聚羟基氯化铵水溶液的方法
公开(公告)号：WO2007130143A3
公开(公告)日：2008-01-10
申请号：PCT/US2006060150
申请日：2006-10-23
申请人： REHEIS INC , JANAK KEVIN , THOMPSON MICHAEL
发明人： JANAK KEVIN , THOMPSON MICHAEL
IPC分类号： C01B17/45 , C01B17/46
CPC分类号： C01F7/007 , C02F1/5245
摘要： The production of polyaluminum hydroxychlorosulfates (PACS) suitable for effective use as flocculants and coagulants in water treatment is described. The product is a fluid, clear solution that is stable with respect to precipitation and gelling for extended periods of time. Key features of the process include: i) the production of a PACS solution of about 12 - 16% Al2O3 and about 40 - 60% basicity at moderate temperatures (50 - 60°C) using a zerovalent aluminum source, such as aluminum powder, ii) the addition of an alkali metal or alkali earth metal base at low temperatures (20 - 30°C) to produce PACS products ranging from 9 - 12 % Al2O3 with basicities ranging from 70 - 80%, iii) the addition of an alkali metal base at low temperatures without the use of high shear mixing, iv) a PACS product that does not contain significant amounts of the Al13-mer Keggin complex, v) a product with greater than 80 - 95% of the aluminum polymers bimodally distributed in the range of 20,000 - 40,000 Daltons and 135 - 750 Daltons, and vi) the formation a PACS whereby greater than 95% of the sulfate is bound to aluminum and is contained in the aluminum polymers distributed in the range of 20,000 - 40,000 Daltons.
摘要翻译：描述了适用于在水处理中有效用作絮凝剂和凝结剂的聚羟基氯代硫酸氢铝（PACS）的生产。该产品是一种液体，透明的溶液，对于沉淀和胶凝长时间稳定。该方法的主要特征包括：i）使用零价铝源（如铝粉）在中等温度（50-60℃）下生产约12-16％Al2O3和约40-60％碱度的PACS溶液， ii）在低温（20-30℃）下加入碱金属或碱土金属碱以产生碱度为70-80％的9-12％Al 2 O 3的PACS产品，iii）加入碱金属基底，而不使用高剪切混合，iv）不含显着量的Al13-mer Keggin复合物的PACS产品，v）具有大于80-95％双峰分布的铝聚合物的产物范围为20,000-40,000道尔顿和135-750道尔顿，以及vi）形成PACS，其中大于95％的硫酸盐与铝结合并且包含在分布在20,000-40,000道尔顿范围内的铝聚合物中。

7. 发明申请

WO2007130143A2 PROCESS FOR PRODUCING STABLE POLYALUMINUM HYDROXYCHLORIDE AND POLYALUMINUM HYDROXYCHLOROSULFATE AQUEOUS SOLUTIONS 审中-公开
标题翻译：生产稳定的羟基氯化汞和聚羟基氯化铵水溶液的方法
公开(公告)号：WO2007130143A2
公开(公告)日：2007-11-15
申请号：PCT/US2006/060150
申请日：2006-10-23
申请人： REHEIS, INC. , JANAK, Kevin , THOMPSON, Michael
发明人： JANAK, Kevin , THOMPSON, Michael
IPC分类号： C01B17/46
CPC分类号： C01F7/007 , C02F1/5245
摘要： The production of polyaluminum hydroxychlorosulfates (PACS) suitable for effective use as flocculants and coagulants in water treatment is described. The product is a fluid, clear solution that is stable with respect to precipitation and gelling for extended periods of time. Key features of the process include: i) the production of a PACS solution of about 12 - 16% Al2O3 and about 40 - 60% basicity at moderate temperatures (50 - 60°C) using a zerovalent aluminum source, such as aluminum powder, ii) the addition of an alkali metal or alkali earth metal base at low temperatures (20 - 30°C) to produce PACS products ranging from 9 - 12 % Al2O3 with basicities ranging from 70 - 80%, iii) the addition of an alkali metal base at low temperatures without the use of high shear mixing, iv) a PACS product that does not contain significant amounts of the Al13-mer Keggin complex, v) a product with greater than 80 - 95% of the aluminum polymers bimodally distributed in the range of 20,000 - 40,000 Daltons and 135 - 750 Daltons, and vi) the formation a PACS whereby greater than 95% of the sulfate is bound to aluminum and is contained in the aluminum polymers distributed in the range of 20,000 - 40,000 Daltons.
摘要翻译：描述了适用于在水处理中有效用作絮凝剂和凝结剂的聚羟基氯代硫酸氢铝（PACS）的生产。该产品是一种液体，透明的溶液，对于沉淀和胶凝长时间稳定。该方法的主要特征包括：i）使用零价铝源（如铝粉）在中等温度（50-60℃）下生产约12-16％Al2O3和约40-60％碱度的PACS溶液， ii）在低温（20-30℃）下加入碱金属或碱土金属碱以产生碱度为70-80％的9-12％Al 2 O 3的PACS产品，iii）加入碱金属基底，而不使用高剪切混合，iv）不含显着量的Al13-mer Keggin复合物的PACS产品，v）具有大于80-95％双峰分布的铝聚合物的产物范围为20,000-40,000道尔顿和135-750道尔顿，以及vi）形成PACS，其中大于95％的硫酸盐与铝结合并且包含在分布在20,000-40,000道尔顿范围内的铝聚合物中。

8. 发明申请

WO2005009376A2 STABLE ALUMINUM/ZIRCONIUM ANTIPERSPIRANT SOLUTION 审中-公开
标题翻译：稳定的铝/ ZIRCONIUM抗反应溶液
公开(公告)号：WO2005009376A2
公开(公告)日：2005-02-03
申请号：PCT/US2004/023501
申请日：2004-07-09
申请人： REHEIS,INC. , PAREKH, Jawahar, C. , LI, Zijun
发明人： LI, Zijun
IPC分类号： A61K
CPC分类号： A61K8/28 , A61Q15/00
摘要： A stable aluminum-zirconium aqueous solution of enhanced efficacy having a high concentration free of amino acid and polyhydric alcohol is disclosed. Such aluminum-zirconium salts are selected from aluminum/zirconium tetrachlorohydrate; aluminum/zirconium pentachlorohydrate, and aluminum/zirconium octachlorohydrate in which the aluminum to zirconium (Al/Zr) atomic ratio of said salt falls within the limits of the shaded areas A, B, and C, respectively, of the drawing graph wherein the aluminum/zirconium tetrachlorohydrate has an Al/Zr atomic ratio from about 2 to about 6 and metal/chloride molecular ratio about 0.9 to about 1.25; aluminum/zirconium pentachlorohydrate having Al/Zr atomic ratio from about 6 to about 10 and metal/chloride atomic ratio from about 1.5 to about 1.65; and aluminum/zirconium octachlorohydrate having Al/Zr molecular ratio from about 6 to about 10 and metal/chloride molecular ratio from about 0.9 to about 1.5.
摘要翻译：公开了一种具有高浓度的氨基酸和多元醇的高效率的稳定的铝 - 锆水溶液。这种铝 - 锆盐选自四氯水合铝/锆; 铝/锆五氯水合物，以及所述盐的铝与锆（Al / Zr）原子比分别落在阴影区域A，B和C的限制范围内的铝/锆八水合物，其中铝 /锆四氯水合物具有约2至约6的Al / Zr原子比和约0.9至约1.25的金属/氯化物分子比; 铝/锆五氯水合物，其Al / Zr原子比为约6至约10，金属/氯化物原子比为约1.5至约1.65; 铝/锆八水合物，其Al / Zr分子比为约6至约10，金属/氯化物分子比为约0.9至约1.5。

9. 发明申请

WO2013077832A3 ALUMINUM COMPOSITIONS OF ENHANCED EFFICACY HAVING HIGH HPLC BANDS IL L AND IV 审中-公开
公开(公告)号：WO2013077832A3
公开(公告)日：2013-05-30
申请号：PCT/US2007/070374
申请日：2007-11-19
申请人： REHEIS, INC. , LI, Zijun , REREK, Mark , JANAK, Kevin
发明人： LI, Zijun , REREK, Mark , JANAK, Kevin
IPC分类号： A61K8/26 , A61Q15/00
摘要： Novel aluminum antiperspiram compositions of enhanced efficacy activated by both heat and acid are produced comprising basic aluminum salts of having the formula: Al 2 (OH) 6-a X a wherein X is CI - , Br - , I - , or NO 3 - . a is from abut 1.1 10 about 1.7, with basic aluminum chloride being the preferred salt. When analyzed by SEC-HPLC at: about 10% concentration (i.e., by 2% A1 ) in water, these compositions exhibit an SEC-HPLC Band I area of less than 10%, a Band III area of at 'least 20%, with a Band III/II area ratio of at l east 0.7. a Band IV area of at least 20%, and have at least 60% aluminum species contained in Bands III and Band IV.

10. 发明申请

WO2007098400A2 STABLE BUFERED ALUMINUM COMPOSITIONS HAVING HIGH HPLC BANDS III AND IV CONTAINING CALCIUM/STRONTIUM 审中-公开
标题翻译：具有包含钙/锶的高效液相色谱柱III和IV的稳定的保护的铝组合物
公开(公告)号：WO2007098400A2
公开(公告)日：2007-08-30
申请号：PCT/US2007/062306
申请日：2007-02-16
申请人： REHEIS, INC. , LI, Zijun , REREK, Mark
发明人： LI, Zijun , REREK, Mark
IPC分类号： A61Q15/00 , A61K8/26
CPC分类号： A61K8/26 , A61K2800/52 , A61Q15/00
摘要： A novel aluminum antiperspirant active composition of enhanced efficacy is provided. The composition is activated by both heat and acid and characterized by having high HPLC Band III and high HPLC Band IV, prepared by the addition of an acid such as AlCl3 to (1) the aluminum calcium and/or strontium betaine solutions, where the calcium and/or strontium is derived from a soluble salt such as calcium and/or strontium chloride or nitrate and (2) the aluminum calcium and/or strontium glycine and/or betaine solutions, where calcium and/or strontium is from strongly alkaline calcium/strontium oxide or hydroxide. The novel aluminum compositions derived according to the invention have HPLC Band I of less than 2%; a Band III of at least 20%; a Band III/II ratio of at least about 0.7; and a Band IV of at least 20%.
摘要翻译：提供了一种增强功效的新型铝止汗剂活性组合物。组合物由热和酸两者活化，其特征在于通过加入酸（例如AlCl 3）制备的（1）铝钙和/或锶甜菜碱溶液制备的具有高的HPLC带III和高的HPLC带IV，其中钙和/或锶衍生自可溶性盐如钙和/或氯化锶或硝酸锶和（2）铝钙和/或锶甘氨酸和/或甜菜碱溶液，其中钙和/或锶来自强碱性钙/ 氧化锶或氢氧化物。根据本发明衍生的新型铝组合物具有小于2％的HPLC带I; 至少20％的乐队III; 至少约0.7的Band III / II比率; 和一个至少20％的乐队IV。

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