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1. 发明授权

US5707436A Process for the production of purple pigments 失效
标题翻译：紫色颜料生产工艺
公开(公告)号：US5707436A
公开(公告)日：1998-01-13
申请号：US412972
申请日：1995-03-29
申请人： Klaus-Dieter Fritsche , Bernd Dorbath , Norbert Giesecke , Kerstin Ruhnau
发明人： Klaus-Dieter Fritsche , Bernd Dorbath , Norbert Giesecke , Kerstin Ruhnau
IPC分类号： C04B41/86 , C03C1/04 , C03C8/14 , C09C1/00 , C09C1/28 , C09C3/06 , C09C1/62
CPC分类号： C03C8/14 , C03C1/04 , C09C1/0078 , C09C1/28 , C09C3/066 , C01P2002/02 , C01P2004/84 , Y10T428/2993
摘要： Prior art production of purple pigments based on colloidal gold on stovable/sinterable/fireable support material involves the reduction of a gold compound in the presence of a chemical reducing agent. Purple pigments may be produced more simply according to the invention by intimately mixing and/or grinding the support material and the gold compound in dry form or by bringing an aqueous solution or suspension of a gold compound and a support material into contact and then thermally treating the mixture at a temperature above the decomposition temperature of the gold compound and below the sintering temperature of the support material, wherein the gold compound is converted into colloidal gold.
摘要翻译：现有技术生产基于可挥发/烧结/可燃/支持材料上胶体金的紫色颜料包括在化学还原剂存在下还原金化合物。根据本发明可以更简单地制备紫色颜料，通过将干燥形式的载体材料和金化合物紧密混合和/或研磨，或通过使金化合物和载体材料的水溶液或悬浮液接触，然后热处理所述混合物在高于金化合物的分解温度并低于载体材料的烧结温度的温度下，其中金化合物转化为胶体金。

2. 发明授权

US5562748A Manufacturing internally printed laminated glass panes 失效
标题翻译：制造内部印刷的夹层玻璃板
公开(公告)号：US5562748A
公开(公告)日：1996-10-08
申请号：US444922
申请日：1995-05-19
申请人： Adalbert Huber
发明人： Adalbert Huber
IPC分类号： C03C23/00 , B32B17/10 , C03C27/12 , C09D11/033 , C03C17/04 , C03C17/28
CPC分类号： B32B17/10761 , B32B17/10036 , B32B17/10348 , C09D11/033
摘要： The invention relates to an improved color paste for the manufacture of internally printed, curved laminated glass panes.Prior art color pastes cause problems with respect to adhesion and optical accuracy or require a higher technical complexity during the baking process for producing internally printed laminated glass panes.Color pastes which constitute the invention and overcome the previous drawbacks are characterized by a print medium which contains 5,6,8-trihydroxy-1,4-naphthoquinone in addition to solvents.
摘要翻译：本发明涉及一种用于制造内部印刷的弯曲夹层玻璃板的改进的色浆。现有技术的彩色糊剂在粘合和光学精度方面引起问题，或者在用于生产内部印刷的夹层玻璃板的烘烤过程中要求更高的技术复杂性。构成本发明并克服前述缺点的彩色糊料的特征在于除了溶剂之外还含有5,6,8-三羟基-1,4-萘醌的印刷介质。

3. 发明授权

US6004391A Pigments for the production of purple ceramic decoration, process for the production thereof and use thereof 失效
标题翻译：用于生产紫色陶瓷装饰的颜料，其生产方法及其用途
公开(公告)号：US6004391A
公开(公告)日：1999-12-21
申请号：US969366
申请日：1997-11-28
申请人： Hans-Peter Letschert , Jenny Wilfert
发明人： Hans-Peter Letschert , Jenny Wilfert
IPC分类号： C04B41/86 , C03C8/14 , C09C1/00 , C09C1/40 , C09C1/62
CPC分类号： C09C1/0009 , C01P2002/02 , C01P2006/60
摘要： Purple pigments according to the invention based on a stovable support material, in particular a glass frit, having a coat applied by coprecipitation of an oxide hydrate of one or more elements from the range comprising Al, Si, Sn, Pb, Ti, Nb, Ta, Sc, Y, La, Ce and Zn and a water-insoluble gold compound or colloidal gold are distinguished from prior art pigments of a similar composition by improved color stability in high temperature firing. The pigments are obtainable in the aqueous phase by coprecipitation of an oxide hydrate and a gold compound or colloidal gold in the presence of a support material and in the absence of a reducing agent. Pigments containing gold compounds assume a purple color on heat treatment or by chemical reduction. Preferred pigments containing gold compounds, which may directly be used as decorative colorants, conveniently develop their color during firing of the decoration.
摘要翻译：根据本发明的紫色颜料，其基于可焊的支撑材料，特别是玻璃料，其具有通过从包括Al，Si，Sn，Pb，Ti，Nb，Nb的多种元素的一种或多种元素的氧化物水合物共沉淀而施加的涂层， Ta，Sc，Y，La，Ce和Zn以及不溶于水的金化合物或胶态金与现有技术的颜色相似，通过改善高温烧制中的颜色稳定性。颜料可以通过在载体材料的存在下和在不存在还原剂的情况下共沉淀氧化物水合物和金化合物或胶态金而在水相中获得。含有金化合物的颜料在热处理或化学还原时呈现紫色。可以直接用作装饰性着色剂的含金化合物的优选颜料在装饰的烧制过程中方便地显现其颜色。

4. 发明授权

US5939343A Lead-free glass composition and the use thereof 失效
标题翻译：无铅玻璃组合物及其用途
公开(公告)号：US5939343A
公开(公告)日：1999-08-17
申请号：US813033
申请日：1997-03-06
申请人： Gerhard Tunker , Hildegard Paulus
发明人： Gerhard Tunker , Hildegard Paulus
IPC分类号： C03C3/064 , C03C3/089 , C03C8/02 , C03C8/14 , C03C8/16 , C03C8/24 , C03C17/04 , C03C17/36 , C09D1/00
CPC分类号： C03C17/3644 , C03C17/04 , C03C17/36 , C03C3/064 , C03C3/089 , C03C8/02 , C03C8/14
摘要： This invention provides a new lead-free glass composition, a glass frit of this composition, a process for its production and also coloring preparations containing such a glass frit and the use thereof. The glass composition according to the invention contains in mol-%K.sub.2 O 10-17B.sub.2 O.sub.3 10-25TiO.sub.2 15-30SiO.sub.2 35-55Al.sub.2 O.sub.3 0-5Bi.sub.2 O.sub.3 0-5S 0-3 and any oxide from the group consisting of PbO, CdO, ZnO, Li.sub.2 O, Na.sub.2 O, MgO, CaO, SrO, BaO and P.sub.2 O.sub.3 which is present being present in a quality of less than 0.5 wt-% in each case. Glass frits of this composition are very suitable for use in coloring preparations for the production of glass enamels, in particular for panes of glass for automobiles. Glass frits according to the invention can be stoved at low temperatures, exhibit good anti-sticking properties, a high resistance to acids and a diminished migration of silver.
摘要翻译：本发明提供了一种新的无铅玻璃组合物，该组合物的玻璃料，其生产方法以及含有这种玻璃料的着色剂及其用途。根据本发明的玻璃组合物含有以摩尔％K 2 O 10-17 B 2 O 3 10-25 TiO 2 15-30 SiO 2 35-55 Al 2 O 3 0-5 Bi 2 O 3 0-5 S 0-3和由PbO，存在的CdO，ZnO，Li 2 O，Na 2 O，MgO，CaO，SrO，BaO和P 2 O 3在每种情况下以小于0.5重量％的质量存在。该组合物的玻璃料非常适合用于生产玻璃搪瓷的着色剂，特别是用于汽车玻璃的玻璃。根据本发明的玻璃料可以在低温下烘烤，表现出良好的抗粘附性，高耐酸性和银迁移减少。

5. 发明授权

US5656328A Anhydrous gels and xerogels containing no hydroxyl groups, process for the production thereof and use thereof 失效
标题翻译：不含羟基的无水凝胶和干凝胶，其制造方法及其用途
公开(公告)号：US5656328A
公开(公告)日：1997-08-12
申请号：US518602
申请日：1995-08-21
申请人： Martin Jansen , Eberhard Gunther
发明人： Martin Jansen , Eberhard Gunther
IPC分类号： C04B35/622 , B01J13/00 , C01B13/32 , C01G25/02 , C01G31/00 , C07F7/00 , C09C3/06 , B05D7/00
CPC分类号： C09C3/063 , B01J13/00 , C01B13/32 , C01G25/02 , C01G31/00 , C01P2002/82 , C01P2002/88 , C01P2006/36
摘要： Gels based on a network of oxygen-bridged metal and/or semi-metal atoms and produced using a hydrolytic sol-gel process are often not homogeneous. Known non-hydrolytic sol-gel processes give rise to gels containing halogen.A novel non-hydrolytic sol-gel process has been found which gives rise to halogen-free and homogeneous gels and to xerogels obtainable therefrom.In this process, one or more compounds (I) from the series of metal or semi-metal alkoxides, oxoalkoxides, amides or oxoamides are condensed, with elimination of carboxylic acid esters or carboxylic acid amides, until gelation occurs with one or more compounds (II) from the series of metal or semi-metal carboxylates or oxocarboxylates in an anhydrous organic solvent containing no hydroxyl groups.Preferred gels and xerogels contain in the network metal or semi-metal atoms from main group and subgroup III to V and from the rare-earth elements.The gels and xerogels may be used for the production of oxide ceramic materials and for encapsulating pigments.
摘要翻译：基于氧桥接金属和/或半金属原子网络的凝胶，并且使用水解溶胶 - 凝胶法制备的凝胶通常是不均匀的。已知的非水解溶胶 - 凝胶法产生含有卤素的凝胶。已经发现了一种新型的非水解溶胶 - 凝胶法，其产生无卤素和均匀的凝胶以及由其获得的干凝胶。在该方法中，一系列金属或半金属醇盐，氧代烷氧化物，酰胺或氧代酰胺的一种或多种化合物（I）被缩合，除去羧酸酯或羧酸酰胺，直到与一种或多种化合物发生凝胶化（ II）由不含羟基的无水有机溶剂中的金属或半金属羧酸盐或氧代羧酸盐系列组成。优选的凝胶和干凝胶含有来自主族和亚组III至V族和稀土元素的网络金属或半金属原子。凝胶和干凝胶可用于生产氧化物陶瓷材料和用于包封颜料。

6. 发明授权

US5639901A Organosulfur gold compounds, a process for their production and their use 失效
标题翻译：有机硫金化合物，其生产和使用的过程
公开(公告)号：US5639901A
公开(公告)日：1997-06-17
申请号：US390483
申请日：1995-02-17
申请人： Andreas Schulz , Marco Hofler
发明人： Andreas Schulz , Marco Hofler
IPC分类号： C03C17/10 , C07C323/52 , C07F1/12 , H05K1/09 , B05D5/10
CPC分类号： C07C323/52 , C03C17/10 , C03C2217/255 , C03C2218/11 , H05K1/092
摘要： Various organosulfur gold compounds and their use for the production of gold decorations are known.The invention relates to new organosulfur gold compounds, to a process for their production and to their use for the production of preparations for producing a gold decoration on firing-resistant substrates.The gold compounds according to the invention are obtainable from monogold(I) dimercaptosuccinic acid and compounds of similar structure by dissolution thereof in water in the presence of a base and precipitation by acidification and, if desired, repetition of the dissolving and precipitating steps. The gold compounds according to the invention are characterized by a gold content of 60 to 90% by weight, an atomic ratio of greater than 0.7 to 4. Preferred gold compounds are soluble in water and are suitable as a constituent of organic/aqueous and exclusively aqueous bright and burnished gold preparations for the decoration of glass, porcelain and ceramic.
摘要翻译：各种有机硫金化合物及其用于生产黄金装饰品的用途是已知的。本发明涉及新的有机硫金化合物，其生产方法及其用于生产耐燃基材上的金装饰制备的用途。根据本发明的金化合物可以通过在碱的存在下在水中溶解并且通过酸化沉淀得到相似结构的化合物，并且如果需要，可以重复溶解和沉淀步骤，从而获得单金属（I）二巯基琥珀酸和类似结构的化合物。根据本发明的金化合物的特征在于金含量为60至90重量％，原子比大于0.7至4.优选的金化合物可溶于水，并且适合作为有机/水性和专有的成分水性光亮抛光金制品用于装饰玻璃，瓷器和陶瓷。

7. 发明授权

US5439660A Oxonitrides of the formula LnTaOn.sub.2 with enhanced brightness and a process for their production and use 失效
标题翻译：具有增强亮度的式LnTaOn2的氧化氮及其生产和使用的方法
公开(公告)号：US5439660A
公开(公告)日：1995-08-08
申请号：US213537
申请日：1994-03-16
申请人： Martin Jansen , Hans-Peter Letschert , Dietrich Speer
发明人： Martin Jansen , Hans-Peter Letschert , Dietrich Speer
IPC分类号： C01B21/20 , C01B21/082 , C01G31/00 , C08K3/28 , C09C1/00 , C01F17/00
CPC分类号： C01B21/0821 , C08K3/28 , C01P2002/34 , C01P2006/60
摘要： Oxonitrides with a perovskite of the general formula LnTaON.sub.2, where Ln is a rare-earth element, and which exhibit an enhanced brightness, are produced by annealing a powder mixture consisting of a Ta (V) compound and a Ln compound in a reducing atmosphere that contains ammonia. Added to the powder mixture being annealed is a mineralizing agent from the series of alkali metal or alkaline earth halides, Na.sub.3 AlF.sub.6, Na.sub.2 SiF.sub.6, AlF.sub.3 or of the ammonia salts of carbonic acid or a mono- or dicarboxylic acid with 1 to 4 C atoms in a quantity of 0.1 to 10 parts by weight, relative to 1 part by weight of the mixture of the Ta and Ln compounds. Such oxonitrides can be used as pigments that are yellow-orange to reddish brown in color.
摘要翻译：通过在还原气氛中退火由Ta（V）化合物和Ln化合物组成的粉末混合物来制备具有通式LnTaON2的钙钛矿的氧化氮，其中Ln是稀土元素，并且显示出增强的亮度，含有氨。加入待退火的粉末混合物是一系列碱金属或碱土金属卤化物，Na 3 AlF 6，Na 2 SiF 6，AlF 3或碳酸的氨盐或具有1至4个C原子的单羧酸或二羧酸的矿化剂，相对于1重量份的Ta和Ln化合物的混合物，其量为0.1至10重量份。这种氧氮化物可以用作黄橙色至红棕色的颜料。

8. 发明授权

US06103312A Process for the production of decorated tableware with increased resistance to scratches caused by cutlery 失效
标题翻译：生产装饰餐具的过程具有增加的餐具耐刮擦性
公开(公告)号：US06103312A
公开(公告)日：2000-08-15
申请号：US166228
申请日：1998-10-05
申请人： Adalbert Huber , Dietrich Speer , Gabriele Wachowitz , Holger Jarnicki
发明人： Adalbert Huber , Dietrich Speer , Gabriele Wachowitz , Holger Jarnicki
IPC分类号： C03C8/14 , C03C8/18 , C04B41/50 , C04B41/86 , C09C1/00 , C09C1/40 , B05D3/02 , B05D1/38
CPC分类号： C04B41/009 , C03C8/14 , C03C8/18 , C04B41/5022 , C04B41/86 , C09C1/0009 , C09C1/405 , C01P2002/02 , C04B2111/00965 , C04B2111/2038
摘要： The resistance of tableware decorations to cutlery scratches can be improved by using a decoration coloring substance whose coloring component is a molecular sieve charged with a metal selected from V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Ag, Au, Ru, Rh, Pd, Os, Ir, Pt and/or an ion or a compound of the metal. The coloring component is preferably an aluminosilicate or silicalite charged with Au, Pt, Pd or Cu.
摘要翻译：可以通过使用着色成分为带有选自V，Cr，Mn，Fe，Co，Ni，Cu，Zn，Ag，Au的金属的分子筛的装饰着色物质来改善餐具装饰对餐具划痕的抵抗性， Ru，Rh，Pd，Os，Ir，Pt和/或金属的离子或化合物。着色组分优选为带有Au，Pt，Pd或Cu的硅铝酸盐或硅沸石。

9. 发明授权

US6063446A Process for the production of decorated tableware with increased resistance to scratches caused by cutlery and coloring substance therefor 失效
标题翻译：用于生产装饰餐具的方法，其具有增加的由餐具和着色物质引起的划伤的抵抗力
公开(公告)号：US6063446A
公开(公告)日：2000-05-16
申请号：US166279
申请日：1998-10-05
申请人： Dietrich Speer , Adalbert Huber , Kai Dorer , Gabriele Wachowitz
发明人： Dietrich Speer , Adalbert Huber , Kai Dorer , Gabriele Wachowitz
IPC分类号： C03C8/14 , C04B41/50 , C04B41/86 , B05D3/02
CPC分类号： C04B41/009 , C03C8/14 , C04B41/5022 , C04B41/86 , C04B2111/00965 , C04B2111/20
摘要： The resistance of tableware decorations to cutlery abrasion traces can be increased by using, in the production of the decoration, a decoration coloring substance containing a pigment and a glass flux with the characteristics profile according to the invention: the pigment of the decoration coloring substance has an average grain diameter equal to or less than 2 .mu.m, and the glass flux of the decoration coloring substance has a density equal to or less than 2.6 g/cm.sup.3 and a hemisphere temperature less than 930.degree. C.
摘要翻译：可以通过在装饰生产中使用含有颜料的装饰着色物质和具有本发明特征的玻璃助熔剂来增加餐具装饰对餐具磨损痕迹的抵抗力：装饰着色物质的颜料具有平均粒径等于或小于2μm，装饰着色物质的玻璃熔点的密度等于或小于2.6g / cm 3，半球温度低于930℃。

10. 发明授权

US5710081A Black glass frit, process for the production thereof and use thereof 失效
标题翻译：黑色玻璃料，其制造方法及其用途
公开(公告)号：US5710081A
公开(公告)日：1998-01-20
申请号：US798925
申请日：1997-02-12
申请人： Gerhard Tunker
发明人： Gerhard Tunker
IPC分类号： C03C8/02
CPC分类号： C03C8/02
摘要： Using conventional glass frits for the production of black glass coating compositions makes it necessary also to use a relatively large quantity of black pigments. The quantity of pigment used may be reduced by using black glass frits according to the invention, thin layers of which already have a low transmission. The glass frit according to the invention is black and contains in the glass composition (in mol. %): 10-17% of K.sub.2 O, 10-25% of B.sub.2 O.sub.3, 15-30% of TiO.sub.2, 30 to 55% of SiO.sub.2, 0-5% of Al.sub.2 O.sub.3, 0-5% of Bi.sub.2 O.sub.3, 0.05-3% of Fe.sub.2 O.sub.3 (total iron) and 0.1-3% of sulphur (total sulphur).
摘要翻译：使用常规玻璃料制备黑色玻璃涂料组合物，还需要使用相对大量的黑色颜料。使用的颜料的量可以通过使用本发明的黑色玻璃料减少，其薄层已经具有低透射率。根据本发明的玻璃料是黑色的并且含有玻璃组合物（摩尔％）：10-17％的K2O，10-25％的B2O3，15-30％的TiO2，30到55％的SiO2， 0-5％的Al2O3，0-5％的Bi2O3，0.05-3％的Fe2O3（总铁）和0.1-3％的硫（总硫）。

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