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    • 86. 发明专利
    • PRODUCTION OF SINGLE CRYSTAL
    • JPH07133185A
    • 1995-05-23
    • JP27858593
    • 1993-11-08
    • JAPAN ENERGY CORP
    • YAMAMOTO HIROMASAKANO MANABU
    • C30B15/16C30B15/20C30B29/40H01L21/208
    • PURPOSE:To provide a process for production of a single crystal capable of producing the long-sized crystal having a high single crystallization rate by a pulling up method. CONSTITUTION:A sub-heater 9 is disposed between a grown crystal 7 which is pulled up together with a seed crystal 6 by a crystal pulling-up shaft 5 from a raw material melt 4 sealed by a liquid sealing material 3 in a crucible 2 installed above a crucible shaft 1 and a heat insulating material 8. The raw material melt 4 is heated by a main heater 10 and the grown crystal 7 is heated by the sub-heater 9. The amt. of the electric power to be supplied to the sub- heater 9 is controlled to suppress the fluctuation in the electric power of the main heater 10 by diameter control within a prescribed range. As a result, the solid-liquid boundary of the grown crystal and the raw material melt is maintained in the stable state during the crystal growth, by which the production of the long-sized single crystal is enabled. The establishment of the operating conditions of various kinds of single crystal growth furnaces is easily executed and the process is extremely industrially useful.
    • 89. 发明专利
    • DEVICE FOR MANUFACTURING SEMICONDUCTOR SINGLE CRYSTAL
    • JPS61146786A
    • 1986-07-04
    • JP26532184
    • 1984-12-18
    • TOSHIBA CORP
    • SAITO TETSUO
    • C30B15/16C30B15/14H01L21/18H01L21/208
    • PURPOSE:To manufacture easily a high-purity semiconductor single crystal by providing an endothermic body consisting of a noncarbonaceous heat-resistant member and a heater consisting of an infrared heater and an infrared reflector and formed by the noncarbonaceous heat-resistant member. CONSTITUTION:A heater is composed of an infrared heater 15 coated with a heat-resistant member and an infrared reflector 18 capable of reflecting efficiently infrared rays from the infrared radiation heater 15 at high temps. and coated with an infrared ray-transmissive and heat-resistant member. Consequently, the heat loss is reduced, and hence a semiconductor material can be melted with less electric power to manufacture a semiconductor single crystal. An endothermic body 19 furnished at the outside of a crucible 2 helps to save the power. Since the heater and the endothermic body 19 both exposed to high temps. are formed of a noncarbonaceous heat-resistant member in the device for manufacturing a semiconductor single crystal, carbon is never brought into the semiconductor crystal, and the desired high-purity single crystal can be obtained.
    • 90. 发明专利
    • Method for controlling diameter of single crystal
    • 用于控制单晶直径的方法
    • JPS5945991A
    • 1984-03-15
    • JP15135482
    • 1982-08-31
    • Nippon Telegr & Teleph Corp Sumitomo Electric Ind Ltd
    • MIYAZAWA SHINTAROUNAKAI RIYUUSUKE
    • C30B15/18C30B15/16C30B15/22H01L21/208
    • C30B15/22C30B15/16
    • PURPOSE: To control the diameter of a single crystal at a definite value, in the pulling of the single crystal using the Czochralski method, by heating the molten liquid around the single crystal locally with infrared heating.
      CONSTITUTION: In the pulling of a single crystal by the Czochralski method, a pair of condenser-type infrared heaters 7 are placed at the symmetrical positions slantly above the crucible 5, and the infrared ray reflected by the condenser mirror 9 is focused to a part 10 of the molten raw material liquid 1 around the single crystal. The lowering of the height of the molten liquid according to the growth of the crystal is calculated by the computer 12 from the change in the weight of the crystal, and the angle and the position of the infrared heater 7 are controlled by the computer so as to keep the focus of the infrared ray and the distance of the part 10 heated by the infrared heater 7 from the center of the crucible to the preset levels. The symmetrical parts 10, 10 at the circumference of the single crystal 3 are concentratedly irradiated with infrared ray, and the surface of the molten liquid is locally heated at a high temperature, however, the ring 11 can be heated uniformly by the rotation of the crucible 5.
      COPYRIGHT: (C)1984,JPO&Japio
    • 目的:为了以一定的值控制单晶的直径,在使用Czochralski法拉伸单晶时,通过红外加热局部加热单晶周围的熔融液体。 构成:在通过Czochralski法拉制单晶时,将一对冷凝器型红外线加热器7放置在坩埚5上方的对称位置处,并且将由聚光镜9反射的红外线聚焦到部分 10个熔融原料液1围绕单晶。 计算机12根据晶体重量的变化计算熔融液体的高度随着晶体生长而降低,红外加热器7的角度和位置由计算机控制,以便 将红外线的焦点和由红外线加热器7加热的部分10的距离从坩埚的中心保持到预设水平。 在单晶3的周围的对称部分10,10被红外线集中照射,并且熔融液体的表面在高温下被局部加热,然而,可以通过旋转来均匀地加热环11 坩埚5。