专利快速检索-快速检索全球专利，免费商用专利数据库-IPRDB

81. 发明公开

EP1369413A1 PROCESS FOR PRODUCING LACTAM 审中-公开
标题翻译： VEFAHREN ZUR HERSTELLUNG VON LACTAM
公开(公告)号：EP1369413A1
公开(公告)日：2003-12-10
申请号：EP01914201.7
申请日：2001-03-23
申请人： National Institute of Advanced Industrial Science and Technology
发明人： HATAKEDA, Kiyotaka , SATO, Osamu , IKUSHIMA, Yutaka , TORII, Kazuo
IPC分类号： C07D201/04 , C07D223/10
CPC分类号： C07D201/06 , C07D201/04 , C07D223/10
摘要： A process for continuously producing a lactam in water at a high temperature under a high pressure. Namely, a process for producing a lactam characterized by selectively synthesizing the lactam without causing hydrolysis by introducing an oxime into flowing water at a high temperature under a high pressure, wherein the lactam is continuously synthesized at a high rate from the oxime in water at a high temperature of 250 °C or more under a high pressure of 12 Mpa or more.
摘要翻译：一种在高温下在高压下连续生产内酰胺的方法。即，制造内酰胺的方法，其特征在于，通过在高温下将肟引入流动的水中而不引起水解而选择性合成内酰胺，其中内部酰胺以高的速率从肟在水中以高温250℃以上，高压12Mpa以上。

82. 发明公开

EP1329448A1 Procsess for producing laurolactam from cyclododecanone 有权
标题翻译： Verfahren zur Herstellung von Laurolactam aus Zyklododecanon
公开(公告)号：EP1329448A1
公开(公告)日：2003-07-23
申请号：EP03000846.0
申请日：2003-01-15
申请人： Ube Industries, Ltd.
发明人： Kuroda, Nobuyuki, c/oUbe Chemical Factory , Kawai, Joji, c/oUbe Chemical Factory , Shimomura, Hideo, c/oUbe Chemical Factory
IPC分类号： C07D201/04 , C07D201/06
CPC分类号： C07D201/06 , C07D201/04
摘要： Laurolactam having high quality is produced by reacting cyclododecanone with a hydroxylamine salt of a mineral acid, and converting the resultant cyclododecanoneoxime to laurolactam through the Beckmann rearrangement reaction, wherein a content of each of oxygen atom-containing C 12 organic compounds, for example, cyclododecenone or epoxycyclododecane, and cycloaliphatic unsaturated C 12 hydrocarbon compounds, contained, as an impurity, in the staring cyclododecanone material, is controlled to 1,000 ppm or less.
摘要翻译：通过使环十二烷酮与无机酸的羟胺盐反应，通过贝克曼重排反应将所得的环十二烷酮肟转化成十二内酰胺，生成高品质的月桂内酰胺，其中含有氧原子的C12有机化合物，例如环十二酮或环氧环十二烷和环脂肪族不饱和C12烃化合物被控制在1000ppm以下，作为杂质，作为起始环十二烷酮材料。

83. 发明公开

EP1013643A1 Method for production of hydroxylamine sulfate in the conventional process for the synthesis of caprolactam 有权
标题翻译：在常规方法中生产硫酸胲的用于合成己内酰胺的方法
公开(公告)号：EP1013643A1
公开(公告)日：2000-06-28
申请号：EP99125632.2
申请日：1999-12-22
申请人： PRAXAIR TECHNOLOGY, INC.
发明人： Echegaray, Diego Fernandez , Velloso, Antonio Augusto M. , Wagner, Matthew Lincoln
IPC分类号： C07D201/06 , C07D201/10
CPC分类号： C07D201/06 , C07D201/10
摘要： An improvement in the conventional process for the production of caprolactam. The process involves:

(a) reacting air with ammonia gas in an ammonia conversion zone to produce nitric oxide;
(b) oxidizing a portion of the nitric oxide to nitrogen dioxide to produce an NO x -rich process gas stream;
(c) reacting the NO x -rich stream with ammonium carbonate in a nitriting zone to produce ammonium nitrite;
(d) reducing the ammonium nitrite to hydroxylamine diammonium sulfate;
(e) hydrolyzing the hydroxylamine diammonium sulfate to hydroxylamine sulfate;
(f) oximating the hydroxylamine sulfate with cyclohexanone to produce cyclohexanone oxime; and
(g) converting the cyclohexanone oxime to caprolactam.
The process is improved by adding supplemental oxygen downstream of the ammonia conversion zone to increase the quantity and rate of formation of nitrogen dioxide in the NO x -rich process gas stream.
摘要翻译：在传统工艺的改进生产己内酰胺的。该过程包括：（a）在氨转化区反应用氨气空气以产生一氧化氮; （B）氧化所述一氧化氮的一部分以二氧化氮以生产富含NOx的反应气流; （C）反应与碳酸铵在亚硝化区中，以产生亚硝酸铵的富含NOx的物流; （D）降低了亚硝酸盐对羟胺二硫酸铵; （E）水解所述羟胺硫酸二铵到硫酸羟胺; （F）的肟化的硫酸胲用环己酮，以产生环己酮肟; 及（g）将所述环己酮肟为己内酰胺。该过程通过加入氨转化区，以增加富含NOx反应气流中形成的二氧化氮的量和速率的下游补充氧气改善。

84. 发明公开

EP0645358A1 Verfahren zur selektiven katalytischen Oxidation organischer Verbindugen 失效
标题翻译：维生素Zur selektiven katalytischen氧化组织器Verbindugen。
公开(公告)号：EP0645358A1
公开(公告)日：1995-03-29
申请号：EP94113561.8
申请日：1994-08-31
申请人： BAYER AG
发明人： Kricsfalussy, Zoltan, Dr. , Waldmann, Helmut, Dr. , Traenckner, Hans-Joachim, Dr.
IPC分类号： C07C37/58 , C07C39/07 , C07C39/08 , C07B41/00
CPC分类号： C07D315/00 , C07B33/00 , C07B41/00 , C07C37/58 , C07C249/04 , C07D201/06 , C07D301/08 , Y02P20/52 , C07C39/08 , C07C39/04 , C07C39/07
摘要： Mit einem besonders vorteilhaften Verfahren werden organische Verbindungen selektiv oxidiert, indem man mit elementarem Sauerstoff, einem Katalysator, der Palladium und Kupfer enthält und in Gegenwart von Kohlenmonoxid arbeitet.
摘要翻译：使用特别有利的方法，通过使用元素氧（含有钯和铜的催化剂）和在一氧化碳的存在下进行反应来选择性地氧化有机化合物。

85. 发明公开

EP0086543A1 Crystalline silicate catalysts with deactivated external surface, and process for its deactivation 失效
标题翻译：具有entaktivierter外表面和它们的失活的方法的结晶硅酸盐的催化剂。
公开(公告)号：EP0086543A1
公开(公告)日：1983-08-24
申请号：EP83200221.6
申请日：1983-02-12
申请人： STAMICARBON B.V.
发明人： Frenken, Petrus Mathias Gerardus
IPC分类号： B01J29/04 , B01J37/30
CPC分类号： C07D201/06 , B01J29/40 , B01J29/86 , B01J37/30 , C07C2/00 , C07C2529/06 , C07C2529/86 , C07C15/00
摘要： Disclosed is a method for selectively deactivating catalytically active sites which occur only on the surface of a zeolite of boralite catalyst. Active sites occurring on the interior of the pores are masked by saturating the catalyst with an organic compound which fills substantially the whole of the catalyst pore volume. The catalyst so treated is then exposed to a deactivating agent, such as a solution of an alkali metal salt which is substantially immiscible with, substantially insoluble in, and which is otherwise unreactive to said pore-filling compound. The catalyst is then treated to drive off the pore-filling compound, yielding a catalyst selectively deactivated only on the external surface, but which is not deactivated within the pores. The treatment enables the catalyst to be used for e.g. hydrocarbon conversion for long time periods without carbon buildups around the pore entrances, which buildup would otherwise either restrict entry into the pores by reactants or exit therefrom by product.

86. 发明公开

EP3277664A1 AN EFFICIENT PROCESS FOR THE SYNTHESIS OF CYCLIC AMIDES 有权
标题翻译：一种有效的合成环状酰胺的方法
公开(公告)号：EP3277664A1
公开(公告)日：2018-02-07
申请号：EP15731711.6
申请日：2015-06-04
申请人： Anthea Aromatics Private Limited
发明人： MOHAPATRA, Manoj Kumar , BENDAPUDI, Ramamohanrao , MENACHERRY, Paul Vincent , PAUL, Vincent
IPC分类号： C07D201/04 , C07B43/06 , C07D201/06
CPC分类号： C07D201/06 , B01D3/36 , C01B21/14 , C01G9/02 , C07D201/04 , C07D201/16 , C07D227/087
摘要： Disclosed herein is an efficient, economical, industrially advantageous, straight-through process for the preparation of cyclic amides, also referred as lactams, in substantially pure form and high yield, from the corresponding cyclic ketones and a hydroxylammonium salt, using a combination of amphoteric metal oxide or amphoteric masked metal oxide and a base.

87. 发明授权

EP2738162B1 METHOD FOR PRODUCING AMIDE COMPOUND 有权
标题翻译：生产酰胺化合物的方法
公开(公告)号：EP2738162B1
公开(公告)日：2018-01-03
申请号：EP14156597.8
申请日：2011-03-15
申请人： UBE INDUSTRIES, LTD.
发明人： Kugimoto, Junichi , Kawai, Joji , Yamato, Kazuo , Okada, Masahide , Sugimoto, Tsunemi , Matsumoto, Hiroshi
IPC分类号： C07D201/04 , C07D225/02 , C07B61/00
CPC分类号： C07D201/06 , C07D201/04 , C07D225/02
摘要： The present invention relates to a method for producing a high purity, high quality amide compound, particularly, lactam. A first embodiment of the present invention is characterized in that an amount of each of a halide, an aldehyde compound, an alcohol compound and a nitrile compound contained in a solution recycled into an oxime-forming step is controlled to an amount of 0.4 mol% or less based on the ketone as a starting material. A second embodiment of the present invention is characterized in that one or more compounds selected from the group consisting of a ketone, an oxime and an amide compound are purified by hydrogenation and/or crystallization for eliminating impurities containing a double bond. A third embodiment of the present invention is characterized in that a content of impurities having a cyclic bridge structure is controlled by using a cycloalkanone purified by recrystallization.

88. 发明公开

EP2738162A2 Method for producing amide compound 有权
标题翻译： VERFAHREN ZUR HERSTELLUNG EINER AMIDVERBINDUNG
公开(公告)号：EP2738162A2
公开(公告)日：2014-06-04
申请号：EP14156597.8
申请日：2011-03-15
申请人： Ube Industries, Ltd.
发明人： Kugimoto, Junichi , Kawai, Joji , Yamato, Kazuo , Okada, Masahide , Sugimoto, Tsunemi , Matsumoto, Hiroshi
IPC分类号： C07D201/04 , C07D225/02 , C07B61/00
CPC分类号： C07D201/06 , C07D201/04 , C07D225/02
摘要： The present invention relates to a high purity lactam comprising double-bond-containing impurities in 15 ppm by weight or less and a method for producing the same. The present invention is characterized in that one or more compounds selected from the group consisting of a ketone, an oxime and an amide compound are purified by hydrogenation and/or crystallization for eliminating impurities containing a double bond.
摘要翻译：本发明涉及含有15ppm（重量）以下的含双键杂质的高纯度内酰胺及其制造方法。本发明的特征在于，通过氢化和/或结晶来纯化选自酮，肟和酰胺化合物的一种或多种化合物，以消除含有双键的杂质。

89. 发明公开

EP2738161A1 Method for producing amide compound 有权
标题翻译：生产酰胺化合物的方法
公开(公告)号：EP2738161A1
公开(公告)日：2014-06-04
申请号：EP14156595.2
申请日：2011-03-15
申请人： Ube Industries, Ltd.
发明人： Kugimoto, Junichi , Kawai, Joji , Yamato, Kazuo , Okada, Masahide , Sugimoto, Tsunemi , Matsumoto, Hiroshi
IPC分类号： C07D201/04 , C07D225/02 , C07B61/00
CPC分类号： C07D201/06 , C07D201/04 , C07D225/02
摘要： The present invention relates to a high purity lactam comprising impurities having a cyclic bridge structure in 50 ppm by weight or less and a method for producing the same. The present invention is characterized in that a content of impurities having a cyclic bridge structure is controlled by using a cycloalkanone purified by recrystallization.
摘要翻译：本发明涉及含有50重量ppm以下的具有环状桥结构的杂质的高纯度内酰胺及其制造方法。本发明的特征在于，通过使用通过重结晶纯化的环烷酮来控制具有环状桥结构的杂质的含量。

90. 发明公开

EP2548862A4 METHOD FOR PRODUCING AMIDE COMPOUND 有权
标题翻译：制造方法的酰胺
公开(公告)号：EP2548862A4
公开(公告)日：2013-09-04
申请号：EP11756317
申请日：2011-03-15
申请人： UBE INDUSTRIES
发明人： KUGIMOTO JUNICHI , KAWAI JOJI , YAMATO KAZUO , OKADA MASAHIDE , SUGIMOTO TSUNEMI , MATSUMOTO HIROSHI
IPC分类号： C07D201/04 , C07B61/00 , C07D225/02
CPC分类号： C07D201/06 , C07D201/04 , C07D225/02

你已经成功收藏专利！

检索式保存成功!

IPRDB

热门服务

关于我们

友情链接

联系方式