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81. 发明授权

US4548821A Flavoring with tertiary pentamethylindanol derivatives 失效
标题翻译：用叔五甲基茚醇衍生物调味
公开(公告)号：US4548821A
公开(公告)日：1985-10-22
申请号：US702361
申请日：1985-02-15
申请人： John B. Hall , Takao Yoshida
发明人： John B. Hall , Takao Yoshida
IPC分类号： A24B15/34 , C07C35/23 , C07C35/32 , C11B9/00 , C11D3/50 , A23L1/226 , A23L1/235
CPC分类号： C11D3/50 , A24B15/345 , C07C35/23 , C07C35/32 , C11B9/0049
摘要： Described are tertiary pentamethylindanol derivatives defined according to the structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond and uses thereof in augmenting or enhancing the aroma or taste of consumable materials selected from the group consisting of perfume compositions, colognes, perfumed articles, foodstuffs, smoking tobaccos and smoking tobacco compositions.
摘要翻译：描述了根据以下结构定义的叔五甲基茚醇衍生物：其中虚线表示碳 - 碳单键或碳 - 碳双键，并且其用于增强或增强选自组中的可消耗材料的香气或味道由香水组合物，古龙水，香料制品，食品，烟草烟草和烟草组合物组成。

82. 发明授权

US4520032A Use in augmenting or enhancing the aroma or taste of foodstuffs or chewing gums of tetrahydro-1,1,2,3,3-pentamethyl-3A[4H]-indanol 失效
标题翻译：用于增强或增强四氢-1,1,2,3,3-五甲基-3A [4H] - 茚满的食品或口香糖的香气或味道
公开(公告)号：US4520032A
公开(公告)日：1985-05-28
申请号：US589662
申请日：1984-03-14
申请人： John B. Hall , Takao Yoshida
发明人： John B. Hall , Takao Yoshida
IPC分类号： A23L27/20 , A24B3/12 , A24B15/34 , A61K8/34 , A61Q13/00 , B01J31/00 , C07C27/00 , C07C29/56 , C07C35/23 , C07C35/32 , C07C67/00 , C11B9/00 , C11D3/50 , C11D9/44 , A23L1/226
CPC分类号： C11B9/0049 , A24B15/345 , C07C35/23 , C07C35/32 , C11D3/50
摘要： Described are tertiary pentamethylindanol derivatives defined according to the structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond and uses thereof in augmenting or enhancing the aroma or taste of consumable materials selected from the group consisting of perfume compositions, colognes, perfumed articles, foodstuffs, smoking tobaccos and smoking tobacco compositions.
摘要翻译：描述了根据以下结构定义的叔五甲基茚醇衍生物：其中虚线表示碳 - 碳单键或碳 - 碳双键，并且其用于增强或增强选自组中的可消耗材料的香气或味道由香水组合物，古龙水，香料制品，食品，烟草烟草和烟草组合物组成。

83. 发明授权

US4327749A Alkyl esters of 1-alkanoyl cycloalkanols, process for preparing same and organoleptic uses thereof 失效
标题翻译： 1-烷酰基环烷醇的烷基酯，其制备方法及其感官用途
公开(公告)号：US4327749A
公开(公告)日：1982-05-04
申请号：US133828
申请日：1980-03-25
申请人： Ronald P. Schreck , Kenneth K. Light , John B. Hall , Frederick L. Schmitt , Manfred H. Vock , William L. Schreiber , Joaquin F. Vinals , Jacob Kiwala
发明人： Ronald P. Schreck , Kenneth K. Light , John B. Hall , Frederick L. Schmitt , Manfred H. Vock , William L. Schreiber , Joaquin F. Vinals , Jacob Kiwala
IPC分类号： A24B15/34 , A24B15/30
CPC分类号： A24B15/34
摘要： Described is a process for preparing several substituted or unsubstituted cycloalkyl acyl alkanoates defined according to the generic structure: ##STR1## wherein R.sub.1 and R.sub.2 taken together complete a cycloalkyl moiety or methyl, dimethyl or trimethyl substituted cycloalkyl moiety containing five or six carbon atoms in the ring and wherein R.sub.3 is C.sub.1 -C.sub.3 lower alkyl and R.sub.4 is methyl or hydrogen by reacting a compound having the generic structure: ##STR2## in an aqueous silver-ion containing solution having a weakly acidic pH at elevated temperatures. The compounds so produced are useful for their organoleptic properties in consumable materials, such as foodstuffs, foodstuff flavorants, chewing gums, chewing gum flavorants, toothpastes, toothpaste flavorants, medicinal products, medicinal product flavorants, chewing tobaccos, chewing tobacco flavorants, smoking tobaccos, smoking tobacco flavorants, perfume compositions, perfumed articles, such as cationic, anionic, nonionic and zwitterionic detergents, fabric softener compositions, drier-added fabric softener articles, textile sizing agents and optical brighteners for textiles as well as colognes.
摘要翻译：描述了根据通用结构定义的若干取代或未取代的环烷基酰基链烷酸酯的方法：其中R 1和R 2一起完成环烷基部分或含有5或6个碳原子的甲基，二甲基或三甲基取代的环烷基部分环，其中R 3是C 1 -C 3低级烷基，R 4是甲基或氢，通过使具有通式结构的化合物：在高温下具有弱酸性pH的含水银离子溶液中。如此生产的化合物可用于消费材料如食品，食品香料，口香糖，口香糖调味剂，牙膏，牙膏调味剂，药用产品，药用香料，咀嚼烟草，咀嚼烟草香料，烟草烟草，吸烟烟草调味剂，香料组合物，香料制品，例如阳离子，阴离子，非离子和两性离子洗涤剂，织物柔软剂组合物，干燥剂添加的织物柔软剂制品，纺织品上浆剂和用于纺织品的荧光增白剂以及古龙水。

84. 发明授权

US4245122A Process for the production of allyl acetone 失效
标题翻译：烯丙基丙酮生产方法
公开(公告)号：US4245122A
公开(公告)日：1981-01-13
申请号：US100534
申请日：1979-12-05
申请人： Takao Yoshida , Denis E. Hruza, Sr. , John B. Hall
发明人： Takao Yoshida , Denis E. Hruza, Sr. , John B. Hall
IPC分类号： C07C45/67 , C07C45/82 , C07C59/76 , C07C45/45
CPC分类号： C07C59/76 , C07C45/676 , C07C45/82
摘要： A process is described for the preparation of allyl acetone (5-hexen-2-one) according to the reaction: ##STR1## wherein R is methyl or ethyl; X is chloro or bromo; M is sodium or potassium; and Q is sodium or potassium, the reaction being carried out (i) using a phase transfer agent and (ii) in a two phase system.
摘要翻译：描述了根据以下反应制备烯丙基丙酮（5-己烯-2-酮）的方法：其中R是甲基或乙基; X是氯或溴; M为钠或钾; 并且Q是钠或钾，反应进行（i）使用相转移剂和（ii）在两相体系中进行。

85. 发明授权

US4241228A 2,2,3-Trimethyl-3-cyclopenten-1-ylalkenyl and alkylidene secondary alkanols, alkanones, cycloalkanols and cycloalkanones, organoleptic uses thereof in perfume compositions, colognes and perfumed articles and process for producing same 失效
标题翻译： 2,2,3-三甲基-3-环戊烯-1-基烯基和亚烷基仲链烷醇，链烷酮，环烷醇和环烷酮，在香料组合物，古龙水和香料制品中的感官用途及其制备方法
公开(公告)号：US4241228A
公开(公告)日：1980-12-23
申请号：US23322
申请日：1979-03-22
申请人： Takao Yoshida , Braja D. Mookherjee , Venkatesh Kamath , John B. Hall , William I. Taylor , Frederick L. Schmitt
发明人： Takao Yoshida , Braja D. Mookherjee , Venkatesh Kamath , John B. Hall , William I. Taylor , Frederick L. Schmitt
IPC分类号： C07C33/12 , C07C45/74 , C11B9/00 , C07C35/21
CPC分类号： C11B9/0034 , C07C33/12 , C07C45/74 , C11B9/003
摘要： Described are perfume and fragrance compositions and perfumed articles including soaps, detergents, powders as well as colognes containing 2,2,3-trimethyl-3-cyclopenten-1-ylalkenyl and alkylidene secondary alkanols, alkanones, cycloalkanols and cycloalkanones having the generic structure: ##STR1## wherein one of the lines +++++ is a carbon-carbon double bond and the other of the lines +++++ is a carbon-carbon single bond; wherein X is carbinol having the structure: ##STR2## or carbonyl having the structure ##STR3## wherein A' is hydrogen, CH.sub.3, C.sub.2 H.sub.5 or --CH.sub.2 --; wherein B' is hydrogen, CH.sub.3, C.sub.2 H.sub.5 or --CH.sub.2 --; where n is 0, 1 or 2; wherein each of the dashed lines are the same and each represents a carbon-carbon single bond or no bond; wherein A' and B' are both --CH.sub.2 -- when n is 1 or 2 and the dashed line is a carbon-carbon single bond or A' is hydrogen and B' is C.sub.2 H.sub.5 or CH.sub.3 or both A' and B' are each CH.sub.3 or A' is C.sub.2 H.sub.5 and B' is CH.sub.3 when n is 0 and the dashed line represents no bond, which imparts thereto rich, musky, cedar woody, sandalwood, sweet, floral, ionone-like, soft-fruity (apricot), green and earthy aromas with resinous topnotes and nutty oily nuances. Also described is a process for preparing such compounds according to the reaction schemes: ##STR4## wherein the lines +++++ A', B', the dashed lines and n are as defined above wherein M is alkaline metal.
摘要翻译：描述了香料和香料组合物和包含肥皂，洗涤剂，粉末以及含有具有以下通用结构的2,2,3-三甲基-3-环戊烯-1-基烯基和亚烷基仲链烷醇，链烷酮，环烷醇和环烷酮的香水制品，其中线+++++之一是碳 - 碳双键，另一条线+++++是碳 - 碳单键; 其中X是具有以下结构的甲醇：具有结构的羰基，其中A'是氢，CH 3，C 2 H 5或-CH 2 - ; 其中B'是氢，CH 3，C 2 H 5或-CH 2 - ; 其中n为0,1或2; 其中每个虚线相同并且各自表示碳 - 碳单键或无键; 其中当n为1或2并且虚线为碳 - 碳单键或A'为氢且B'为C 2 H 5或CH 3时，A'和B'均为-CH 2 - ，或者A'和B'均为CH 3 或A'为C 2 H 5，B'为CH 3，n为0，虚线表示无键，赋予其丰富，麝香，雪松木香，檀香，甜，花，紫罗兰酮，软果（杏），绿和土质的香气与树脂的顶部和坚果油的细微差别。还描述了根据反应方案制备这些化合物的方法：其中线+++++ A'，B'，虚线和n 如上所定义，其中M是碱金属。

86. 发明授权

US4199481A Acetylated alpha methyl styrene dimers or derivatives in perfumes 失效
标题翻译：乙酰化α-甲基苯乙烯二聚物或香料中的衍生物
公开(公告)号：US4199481A
公开(公告)日：1980-04-22
申请号：US46551
申请日：1979-06-07
申请人： John B. Hall , Wilhelmus J. Wiegers , Ira D. Hill , Robert M. Novak , Frederick L. Schmitt
发明人： John B. Hall , Wilhelmus J. Wiegers , Ira D. Hill , Robert M. Novak , Frederick L. Schmitt
IPC分类号： C07C45/46 , C07C49/792 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0061 , C07C45/46 , C07C49/792 , C11B9/0034 , C11B9/0049
摘要： A process is described for providing clear extended compositions of essential oils which comprises a composition of an essential oil and an extender material miscible with said essential oil which does not appreciably alter the aroma of the essential oil insofar as its quality or strength is concerned, the proportion of essential oil in extender material being from about 70% up to about 99%, said extender material being an acylated dimerization product of an alpha methyl styrene or a methyl or other C.sub.2 -C.sub.4 lower alkyl homologue thereof or hydrogenated derivative thereof or mixture of same.
摘要翻译：描述了一种用于提供精油的清晰延长组合物的方法，其包含精油和与所述精油混溶的增量剂材料的组合物，其不会明显地改变其质量或强度方面的精油的香味，增量材料中精油的比例为约70％至约99％，所述增量材料是α-甲基苯乙烯或其甲基或其它C 2 -C 4低级烷基同系物的酰化二聚产物或其氢化衍生物或相同。

87. 发明授权

US4169109A Process for preparing ketones using zinc acetate condensation catalysts, products produced thereby and organoleptic uses of same 失效
标题翻译：使用乙酸锌缩合催化剂制备酮的方法，由此生产的产品和感官用途
公开(公告)号：US4169109A
公开(公告)日：1979-09-25
申请号：US932649
申请日：1978-08-10
申请人： Takao Yoshida , John B. Hall
发明人： Takao Yoshida , John B. Hall
IPC分类号： A24B15/30 , C07C45/74 , C07C49/20 , C07C49/203 , C07C49/217 , C11B9/00 , C07C45/00
CPC分类号： C07C403/16 , A24B15/30 , C07C45/74 , C07C49/203 , C07C49/217 , C11B9/0003 , C11B9/0015 , C11B9/0034 , C11B9/0061 , C07C2101/16
摘要： Described is a process for the production of alpha, beta unsaturated ketones by reaction of an aldehyde with a ketone in the presence of a catalyst consisting essentially of either zinc acetate or zinc acetate dihydrate. The ketones obtained are suitable and some cases as solvents and in some cases as intermediates for the production of valuable odorants, dyes, plastics and especially nature-identical substances and are also useful as odorants per se.
摘要翻译：描述的是通过在主要由乙酸锌或乙酸锌二水合物组成的催化剂的存在下，通过醛与酮的反应制备α，β不饱和酮的方法。获得的酮是合适的，有些情况是溶剂，在某些情况下作为生产有价值气味剂，染料，塑料，特别是自然相同物质的中间体，也可用作气味剂本身。

88. 发明授权

US4165301A Uses of terpene dimers in perfumery processes and products 失效
标题翻译：在香料工艺和产品中使用萜烯二聚体
公开(公告)号：US4165301A
公开(公告)日：1979-08-21
申请号：US902436
申请日：1978-05-03
申请人： Wilhelmus J. Wiegers , John B. Hall , Ira D. Hill , Robert M. Novak , Frederick L. Schmitt , Braja D. Mookherjee , Chi-Kuen Shu , William L. Schreiber
发明人： Wilhelmus J. Wiegers , John B. Hall , Ira D. Hill , Robert M. Novak , Frederick L. Schmitt , Braja D. Mookherjee , Chi-Kuen Shu , William L. Schreiber
IPC分类号： C11B9/00
CPC分类号： C11B9/00
摘要： A process is described for providing clear extended compositions of synthetic and/or natural essential oils and/or perfumery chemicals which comprises admixing a composition of a synthetic and/or natural essential oil and/or perfumery chemical and an extender material miscible with said synthetic and/or natural essential oil and/or perfumery chemical which does not appreciably alter the aroma of the synthetic and/or natural essential oil and/or perfumery chemical insofar as its quality or strength is concerned, the proportion of synthetic and/or natural essential oil and/or perfumery chemical in extender material being from about 70% up to about 99%, said extender material being one or more "dimerization" (or "coupling") products of one or more terpenes which are monocyclic and have two carbon-carbon double bonds or which are bicyclic and have one carbon-carbon double bond or one or more hydrogenated derivatives thereof or mixtures of same.
摘要翻译：描述了一种用于提供合成和/或天然精油和/或香料化学品的清晰延长组合物的方法，其包括混合合成和/或天然精油和/或香料化学品的组合物和与所述合成和/或香料化学品可混溶的增量剂材料 /或天然精油和/或香料化学品，其质量或强度在合理和/或天然精油和/或香料化学品的芳香度方面不会明显改变，合成和/或天然精油的比例和/或增量材料中的香料化学品为约70％至约99％，所述增量材料是一种或多种单环的一种或多种萜烯的“二聚”（或“偶联”）产物，并具有两个碳 - 碳双键或双环并具有一个碳 - 碳双键或其一种或多种氢化衍生物或其混合物。

89. 发明授权

US4142998A Uses of alpha methyl styrene dimers in perfumery processes and products 失效
标题翻译：在造纸工艺和产品中使用ALPHA甲基苯乙烯二聚体
公开(公告)号：US4142998A
公开(公告)日：1979-03-06
申请号：US902565
申请日：1978-05-03
申请人： John B. Hall , Wilhelmus J. Wiegers , Ira D. Hill , Robert M. Novak , Frederick L. Schmitt
发明人： John B. Hall , Wilhelmus J. Wiegers , Ira D. Hill , Robert M. Novak , Frederick L. Schmitt
IPC分类号： A23L27/00 , C11B9/02 , C11B9/00
CPC分类号： C11B9/02 , A23L27/70
摘要： A process is described for providing clear extended compositions of essential oils which comprises a composition of an essential oil and an extender material miscible with said essential oil which does not appreciably alter the aroma of the essential oil insofar as its quality or strength is concerned, the proportion of essential oil in extender material being from about 70% up to about 99%, said extender material being a dimerization product of an alpha methyl styrene or a methyl or other C.sub.2 -C.sub.4 lower alkyl homologue thereof or hydrogenated derivative thereof or mixture of same, having one of the generic structures: ##STR1## wherein R.sub.3 and R.sub.4 are the same or different and each represents hydrogen or methyl or other C.sub.2 -C.sub.4 lower alkyl and wherein the dashed lines and wavy lines represent carbon-carbon single bonds or carbon-carbon double bonds with the proviso that when there is one double bond present only the wavy line is a double bond and when there is more than one double bond present, the ring containing the dashed lines and the wavy line is a benzene ring and wherein the line represents either a carbon-carbon single bond or no bond.

90. 发明授权

US4131555A Detergent composition 失效
标题翻译：洗涤剂组成
公开(公告)号：US4131555A
公开(公告)日：1978-12-26
申请号：US847209
申请日：1977-10-31
申请人： John B. Hall , Wilhelmus J. Weigers
发明人： John B. Hall , Wilhelmus J. Weigers
IPC分类号： C07C37/14 , C07C39/17 , C11B9/00 , C11D3/50
CPC分类号： C07C37/14 , C11B9/0046 , C07C2102/42
摘要： Described is a detergent composition containing as a key ingredient, a mixture of compounds having a sandalwood aroma produced according to a process which comprises:(1) Reacting catechol with camphene in the presence of a Friedel Crafts Catalyst to form a first alkylation product; and then(2) Treating said first alkylation product with hydrogen in the presence of a hydrogenation catalyst, thus forming, initially, diol intermediates and then, on continuing the hydrogenation, the mixture useful in the perfume compositions of our invention.
摘要翻译：描述了含有作为关键成分的洗涤剂组合物，根据以下方法制备的具有檀香香气的化合物的混合物，该方法包括：

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