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81. 发明授权

US06773261B2 Processes for forming dental materials 失效
标题翻译：牙科材料成型工艺
公开(公告)号：US06773261B2
公开(公告)日：2004-08-10
申请号：US10185436
申请日：2002-06-28
申请人： Bradley D. Craig , Rajdeep S. Kalgutkar , Joel D. Oxman
发明人： Bradley D. Craig , Rajdeep S. Kalgutkar , Joel D. Oxman
IPC分类号： A61C500
CPC分类号： A61K6/083 , A61K6/0017 , A61K6/0023 , A61K6/087 , C08L33/00 , C08L63/00
摘要： Processes for forming dental materials that include applying a hardenable dental adhesive to a surface and a second hardenable dental composite to the dental adhesive. The hardenable dental composite includes at least two adjacent regions with different concentrations of a photoinitiator, at least two adjacent regions with different photoinitiators, or both.
摘要翻译：用于形成牙科材料的方法，包括将可硬化牙科粘合剂施加到表面，将第二可硬化牙科复合物施加到牙科粘合剂上。可硬化牙科复合材料包括至少两个具有不同浓度的光引发剂的相邻区域，至少两个具有不同光引发剂的相邻区域，或两者。

82. 发明授权

US06692611B2 Method of producing a laminated structure 有权
标题翻译：层压结构体的制造方法
公开(公告)号：US06692611B2
公开(公告)日：2004-02-17
申请号：US09995038
申请日：2001-11-26
申请人： Joel D. Oxman , Michael A. Kropp , Peter B. Hogerton
发明人： Joel D. Oxman , Michael A. Kropp , Peter B. Hogerton
IPC分类号： B32B3128
CPC分类号： B32B7/12 , B32B2037/243 , B32B2038/0092 , B32B2307/40 , B32B2429/02 , B32B2457/08 , C08F2/46 , C08F290/067 , C09J4/00 , C09J4/06 , H01L2224/16 , H01L2224/16225 , H01L2224/32225 , H01L2224/73204 , H01L2224/83102 , H01L2224/92125 , H01L2924/0102 , H01L2924/01021 , H01L2924/01025 , H01L2924/01037 , H01L2924/01046 , H01L2924/01077 , H01L2924/01078 , H01L2924/01322 , H01L2924/12041 , C08F222/1006 , H01L2924/00
摘要： A method of laminating a structure comprises at least two layers and a photopolymerizable adhesive composition between the layers, at least one of the layers being opaque, colored, or reflective. One or both of the layers is transmissive to actinic radiation in wavelengths in the range of greater than 400 nm and up to 1200 nm. The photopolymerizable adhesive composition absorbs radiation in the identified spectral region of the radiation transmissive layer. Curing is effected by directing radiation in the identified spectral region through the radiation transmissive layer and produces a laminated structure. An underfilled flip chip assembly on an integrated circuit board substrate can be prepared by the method described above. The photopolymerizable adhesive composition can be applied directly to one or both surfaces of an aligned integrated chip and circuit board substrate or the chip aligned on an integrated circuit board substrate can be capillary underfilled with the photopolymerizable adhesive composition, which is subsequently cured. Data storage disks can also be prepared by the method of the invention.
摘要翻译：层压结构的方法包括至少两层和在这些层之间的可光聚合的粘合剂组合物，至少一层是不透明的，有色的或反射的。这些层中的一层或两层对波长在大于400nm和高达1200nm的波长的光化辐射是透射的。可光聚合的粘合剂组合物吸收辐射透射层的所识别的光谱区域中的辐射。通过通过辐射透射层引导识别的光谱区域中的辐射来实现固化，并产生层压结构。可以通过上述方法制备集成电路板基板上的未充满的倒装芯片组件。可光聚合的粘合剂组合物可以直接施加到对准的集成芯片和电路板基板的一个或两个表面，或者在集成电路板基板上排列的芯片可以被毛发填充，然后可光聚合的粘合剂组合物随后被固化。数据存储盘也可以通过本发明的方法来制备。

83. 发明授权

US06187836B1 Compositions featuring cationically active and free radically active functional groups, and methods for polymerizing such compositions 失效
标题翻译：具有阳离子活性和自由基活性官能团的组合物，以及聚合这种组合物的方法
公开(公告)号：US06187836B1
公开(公告)日：2001-02-13
申请号：US09092550
申请日：1998-06-05
申请人： Joel D. Oxman , Matthew C. Trom , Dwight W. Jacobs
发明人： Joel D. Oxman , Matthew C. Trom , Dwight W. Jacobs
IPC分类号： C08F248
CPC分类号： A61K6/0017 , A61K6/0023 , A61K6/083 , A61K6/087 , C08G59/68 , C08G65/105 , Y10S522/908 , C08L63/00 , C08L33/00
摘要： Photopolymerizable compositions that include free radically active and cationically active functional groups, and methods for polymerizing such compositions, in which the onset of cationic polymerization is controllably delayed to extend the time between formation of a moldable gel and formation of a hardened solid.
摘要翻译：包括游离的自由基活性和阳离子活性官能团的光聚合组合物和聚合这种组合物的方法，其中阳离子聚合的开始被可控地延迟以延长形成可模制凝胶和形成硬化固体之间的时间。

84. 发明授权

US6159012A Process for treating hard tissues 有权
标题翻译：硬组织治疗方法
公开(公告)号：US6159012A
公开(公告)日：2000-12-12
申请号：US387449
申请日：1999-09-01
申请人： Joel D. Oxman , Hoa T. Bui , Dwight W. Jacobs
发明人： Joel D. Oxman , Hoa T. Bui , Dwight W. Jacobs
IPC分类号： A61K6/00 , A61K6/083 , A61K6/087 , A61B17/06 , A61C5/00 , A61K6/08 , C08L63/00
CPC分类号： A61K6/0023 , Y10S522/908
摘要： In a first aspect, a method for treating hard tissue that includes: (a) applying to hard tissue a composition that includes a cationically active functional group, a free radically active functional group, and a polymerization initiator capable of initiating free radical polymerization, where the number of moles of cationically active functional groups per gram of composition is no greater than about 0.0075; and (b) exposing the composition to polymerization conditions to form an adhesive bonded to the hard tissue.In a second aspect, a method for treating hard tissue that includes: (a) applying to hard tissue a first polymerizable composition that includes a free radically active functional group and a polymerization initiator capable of initiating free radical polymerization, but is essentially free of polymerizable components having cationically active functional groups and is capable of forming an adhesive bonded to the hard tissue upon exposure to polymerization conditions; (b) applying a second polymerizable composition; and (c) exposing the second composition to polymerization conditions to form a hardened composition adhered to the hard tissue. The second composition includes (i) a cationically active functional group and (ii) an polymerization initiator capable of initiating cationic polymerization.
摘要翻译：第一方面，一种硬组织处理方法，包括：（a）向硬组织施加包含阳离子活性官能团，自由基活性官能团和能引发自由基聚合的聚合引发剂的组合物，其中每克组合物中阳离子活性官能团的摩尔数不大于约0.0075; 和（b）将组合物暴露于聚合条件以形成粘合到硬组织的粘合剂。在第二方面，一种硬组织处理方法，包括：（a）向硬组织施加包含自由基活性官能团的第一可聚合组合物和能引发自由基聚合的聚合引发剂，但基本上不含可聚合的具有阳离子活性官能团的组分并且能够在暴露于聚合条件时形成粘合到硬组织的粘合剂; （b）施加第二可聚合组合物; 和（c）将第二组合物暴露于聚合条件以形成粘附到硬组织的硬化组合物。第二组合物包括（i）阳离子活性官能团和（ii）能够引发阳离子聚合的聚合引发剂。

85. 发明授权

US6151433A Optical fiber connector using photocurable adhesive 失效
标题翻译：光纤连接器使用光固化胶
公开(公告)号：US6151433A
公开(公告)日：2000-11-21
申请号：US85198
申请日：1998-05-27
申请人： William V. Dower , Joel D. Oxman , Brian N. Holmes
发明人： William V. Dower , Joel D. Oxman , Brian N. Holmes
IPC分类号： G02B6/38 , G02B6/30
CPC分类号： G02B6/3861 , Y10S359/90
摘要： A fiber optic connector including a holder for one ore more optical cables, each optical cable having an optical fiber surrounded by strengthening fibers, both of which are surrounded by at least one polymeric coating layer. The cable is stripped in a layerwise manner such that an area of exposed fiber is succeeded by an area of exposed strengthening fibers, succeeded by an area of coated cable. A visible light curable adhesive is injected into the holder and cured by exposure to visible light for up to about 30 seconds, bonding the optical fiber layers and the holder into a unified structure.
摘要翻译：一种光纤连接器，其包括用于一个或多个光缆的保持器，每个光缆具有被强化纤维包围的光纤，两者都被至少一个聚合物涂层包围。电缆以分层方式被剥离，使得暴露的纤维的区域由暴露的强化纤维的区域继续，接着是涂覆电缆的区域。将可见光可固化粘合剂注入保持器中并通过暴露于可见光固化长达约30秒，将光纤层和保持器结合成统一的结构。

86. 发明授权

US6017660A Inks containing a ternary photoinitiator system and image graphics prepared using same 失效
标题翻译：含有三元光引发剂体系的油墨和使用其制备的图像图形
公开(公告)号：US6017660A
公开(公告)日：2000-01-25
申请号：US94184
申请日：1998-06-09
申请人： Michael C. Palazzotto , F. Andrew Ubel, III , Joel D. Oxman , M. Zaki Ali
发明人： Michael C. Palazzotto , F. Andrew Ubel, III , Joel D. Oxman , M. Zaki Ali
IPC分类号： A61K6/083 , C08F2/46 , C08F2/50 , C09D11/10 , G03F7/028 , G03F7/029 , G03F7/031 , G03C1/73 , B32B27/16
CPC分类号： A61K6/083 , C08F2/50 , C09D11/101 , G03F7/029 , G03F7/031 , Y10S430/116 , Y10S430/117 , Y10S430/12
摘要： Photocurable addition-polymerizable compositions containing a free-radically-polymerizable monomer and a photoinitiator system containing i) an arylidonium salt, ii) a sensitizing compound, and iii) an electron donor having an oxidation potential that is greater than zero and less than or equal to that of p-dimethyoxybenzene (1.32 volts vs. S.C.E.). The compositions cure rapidly and deeply under ultraviolet or visible light.
摘要翻译：含有可自由基聚合的单体和光引发剂体系的光固化的可加成聚合组合物，其含有i）芳基化钠盐，ii）增感化合物，和iii）具有大于零且小于或等于0的氧化电位的电子给体到对二甲基苯（1.32伏对SCE）。组合物在紫外线或可见光下快速且深入地固化。

87. 发明授权

US5709548A Dental crown liner composition and methods of preparing provisional applications 失效
标题翻译：牙冠冠衬垫组成及制备临时应用方法
公开(公告)号：US5709548A
公开(公告)日：1998-01-20
申请号：US801288
申请日：1997-02-18
申请人： Joel D. Oxman , Scott E. Anderson
发明人： Joel D. Oxman , Scott E. Anderson
IPC分类号： A61C9/00 , A61C13/00 , A61K6/08 , A61K6/083 , A61K6/087 , A61K6/09 , C08L67/02 , C08L67/04 , C08G63/08 , A61C5/08
CPC分类号： C08L67/025 , A61C13/0003 , A61C9/0006 , A61K6/083 , A61K6/087 , A61K6/09 , A61K6/10 , C08L67/04 , Y10S522/908
摘要： Thermoplastic compositions are used for the fabrication of provisional (i.e., temporary) prosthetic devices, especially for the fabrication of crowns and bridges, and as liners for crowns. Preferably, the thermoplastic compositions comprise free-radically polymerizable functionality so that the material can be polymerized after being shaped to a desired configuration.
摘要翻译：热塑性组合物用于制造临时（即临时）假体装置，尤其用于制造牙冠和牙桥，以及用作牙冠的衬垫。优选地，热塑性组合物包含可自由基聚合的官能团，使得材料可以在成形为期望的构型之后进行聚合。

88. 发明授权

US4916169A Visible radiation activated hydrosilation reaction 失效
标题翻译：可见辐射激活硅氢化反应
公开(公告)号：US4916169A
公开(公告)日：1990-04-10
申请号：US242478
申请日：1988-09-09
申请人： Larry D. Boardman , Joel D. Oxman
发明人： Larry D. Boardman , Joel D. Oxman
IPC分类号： C08K5/01 , A61K6/10 , C08F2/46 , C08K5/56 , C08L83/04 , C08L83/05 , C08L83/07
CPC分类号： A61K6/10 , C08K5/56 , C08L83/04 , C08G77/12 , C08G77/20 , C08G77/24 , C08G77/70
摘要： A process for the addition of compounds containing silicon-bonded hydrogen to compounds containing aliphatic unsaturation and compositions suitable for said process. The process is activated by visible radiation and is conducted in the presence of a platinum complex having one cyclopentadienyl group that is eta-bonded to the platinum atom and three aliphatic groups that are sigma-bonded to the platinum atom and a sensitizer that is capable of absorbing visible light and is capable of transferring energy to said platinum complex such that the hydrosilation reaction is initiated upon exposure to visible light. The invention also provides for use in the aforementioned process.

89. 发明授权

US4880660A Method for priming hard tissue 失效
标题翻译：灌注硬组织的方法
公开(公告)号：US4880660A
公开(公告)日：1989-11-14
申请号：US91051
申请日：1987-08-28
申请人： Steven M. Aasen , Joel D. Oxman
发明人： Steven M. Aasen , Joel D. Oxman
IPC分类号： A61K6/00 , A61K8/81 , A61L24/00 , A61Q3/00 , C09J5/02
CPC分类号： A61Q3/00 , A61K6/0017 , A61K6/0023 , A61K8/8152
摘要： A single phase aqueous solution containing water, a water-soluble film former (e.g., 2-hydroxyethylacrylate) and a salt of an acid (e.g., calcium trifluoroacetate) is used as a primer for adhering to or overcoating hard tissue such as tooth dentin.

90. 发明授权

US4871786A Organic fluoride sources 失效
标题翻译：有机氟源
公开(公告)号：US4871786A
公开(公告)日：1989-10-03
申请号：US252530
申请日：1988-10-03
申请人： Steven M. Aasen , Joel D. Oxman , F. Andrew Ubel, III
发明人： Steven M. Aasen , Joel D. Oxman , F. Andrew Ubel, III
IPC分类号： A61K6/083 , C08F4/14 , C08F20/10 , C08K5/55
CPC分类号： A61K6/083 , C08F4/14
摘要： Organic fluoride sources comprising a tetrafluoroborate salt and capable of releasing fluoride ions into dentition in order to provide inhibition and/or prevention of dental caries are disclosed. A method of releasing fluoride ion into dental tissue is also disclosed.

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