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81. 发明申请

US20060287418A1 Nanoparticulate phosphorus-containing flame retardant system 审中-公开
标题翻译：纳米微粒含磷阻燃体系
公开(公告)号：US20060287418A1
公开(公告)日：2006-12-21
申请号：US11182459
申请日：2005-07-15
申请人： Harald Bauer , Werner Krause , Martin Sicken , Norbert Weferling
发明人： Harald Bauer , Werner Krause , Martin Sicken , Norbert Weferling
IPC分类号： C08K5/52
CPC分类号： C08K5/5313 , C07F9/30 , C07F9/305 , C08K5/0091
摘要： The invention relates to a nanoparticulate phosphorus-containing flame retardant system, which comprises a phosphinic salt of the formula (I) and/or a diphosphinic salt of the formula (II) and/or their polymers, where R1 and R2 are identical or different and are C1-C6-alkyl, linear or branched, and/or aryl; R3 is C1-C10-alkylene, linear or branched, C6-C10-arylene, -alkylarylene, or -arylalkylene; M is Mg, Ca, Al, Sb, Sn, Ge, Ti, Fe, Zr, Zn, Ce, Bi, Sr, Mn, Li, Na, K, and/or a protonated nitrogen base; m is from 1 to 4; n is from 1 to 4; x is from 1 to 4; and to a process for the preparation of these flame retardant systems, and to their use.
摘要翻译：本发明涉及一种纳米颗粒含磷阻燃体系，其包含式（I）的次膦酸盐和/或式（II）的二膦酸盐和/或其聚合物，其中R 1， O 2和R 2相同或不同，为C 1 -C 6 - 烷基，直链或支链和/或芳基; R 3是C 1 -C 10 - 亚烷基，直链或支链C 6 -C 13 - - 亚芳基， - 亚烷基亚芳基或 - 芳基亚烷基; M是Mg，Ca，Al，Sb，Sn，Ge，Ti，Fe，Zr，Zn，Ce，Bi，Sr，Mn，Li，Na，K和/或质子化氮碱; m为1〜4; n为1至4; x为1至4; 以及制备这些阻燃体系的方法及其应用。

82. 发明授权

US07148276B2 Granular flame-retardant composition 有权
标题翻译：颗粒阻燃组合物
公开(公告)号：US07148276B2
公开(公告)日：2006-12-12
申请号：US10656398
申请日：2003-09-05
申请人： Harald Bauer , Sebastian Hoerold , Werner Krause , Martin Sicken
发明人： Harald Bauer , Sebastian Hoerold , Werner Krause , Martin Sicken
IPC分类号： C08K5/53
CPC分类号： C08K5/5313
摘要： The invention relates to a flame retardant combination comprising, as component A, a phosphinate of the formula (I) and/or a diphosphinate of the formula (II) and/or polymers of these where R1 and R2 are identical or different and are C1–C6-alkyl, linear or branched, and/or aryl; R3 is C1–C10-alkylene, linear or branched, C6–C10-arylene, -alkylarylene or -arylalkylene; M is calcium ions, magnesium ions, aluminum ions and/or zinc ions, m is 2 or 3; n is 1 or 3; x is 1 or 2; and comprising a component B1, B2 and/or B3 wherein B1 is a salt of 1,3,5-triazine compound with polyphosphoric acid, and wherein B2 is a melamine polymetaphosphate, and wherein B3 is a composite salt of polyphosphoric acid with melamine, melam and/or melem.
摘要翻译：本发明涉及一种阻燃剂组合物，其包含作为组分A的式（I）的次膦酸盐和/或式（II）的二膦酸盐和/或这些的聚合物，其中R 1和 R 2相同或不同，为C 1 -C 6 - 烷基，直链或支链和/或芳基; R 3是C 1 -C 10 - 亚烷基，直链或支链C 6 -C 13 - - 亚芳基， - 烷基亚芳基或 - 芳基亚烷基; M是钙离子，镁离子，铝离子和/或锌离子，m是2或3; n为1或3; x为1或2; 并且包含B1，B2和/或B3组分，其中B1是1,3,5-三嗪化合物与多磷酸的盐，其中B2是三聚氰胺聚偏磷酸盐，并且其中B3是多磷酸与三聚氰胺的复合盐，黑夜和/或混战。

83. 发明申请

US20060127308A1 Method to improve the efficacy of therapeutic radiolabeled drugs 审中-公开
标题翻译：提高治疗放射性标记药物疗效的方法
公开(公告)号：US20060127308A1
公开(公告)日：2006-06-15
申请号：US11009518
申请日：2004-12-13
申请人： Werner Krause
发明人： Werner Krause
IPC分类号： A61K51/00 , C07F5/00
CPC分类号： A61K51/1093
摘要： Disclosed are radiolabeled drugs and methods to improve their efficacy by using a radiosensitizer such that the radiosensitizer is either part of the radiolabeled drug by directly attaching the radiosensitizer to the radiolabeled drug or by producing a mixture of the radiolabeled drug and an analogue of the drug with the radiosensitizer attached to the drug instead of the radiolabel.
摘要翻译：公开了通过使用放射增敏剂来提高其功效的放射性标记药物和方法，使得放射增敏剂是放射性标记药物的一部分，通过将放射增敏剂直接附着到放射性标记的药物或通过产生放射性标记的药物和药物的类似物的混合物与放射敏剂附着于药物而不是放射性标记物。

84. 发明申请

US20050143503A1 Phosphorus-containing flame retardant agglomerates 有权
标题翻译：含磷阻燃剂
公开(公告)号：US20050143503A1
公开(公告)日：2005-06-30
申请号：US10959515
申请日：2004-10-06
申请人： Harald Bauer , Sebastian Hoerold , Werner Krause , Martin Sicken
发明人： Harald Bauer , Sebastian Hoerold , Werner Krause , Martin Sicken
IPC分类号： C09K21/12 , B01J2/28 , C08K5/00 , C08K5/5313 , C08K9/04 , C08L101/00 , C09K21/02 , C09K21/10 , C08K5/49
CPC分类号： C08K5/0066 , C08J3/223 , C08J2367/02 , C08J2377/02 , C08J2377/06 , C08K5/5313
摘要： The invention relates to phosphorus-containing flame retardant agglomerates comprising a) from 99.99 to 80% by weight of aggregates and/or primary particles composed of a phosphinic salt of the formula (I) and/or composed of a diphosphinic salt of the formula (II), and/or composed of polymers of these, where R1,R2 are identical or different and are C1-C6-alkyl, linear or branched, and/or aryl; R3 is C1-C10-alkylene, linear or branched, C6-C10-arylene, -alkylarylene or -arylalkylene; M is Mg, Ca, Al, Sb, Sn, Ge, Ti, Fe, Zr, Ce, Bi, Sr, Mn, Li, Na, K and/or a protonated nitrogen base; m is from 1 to 4; n is from 1 to 4; x is from 1 to 4 and b) from 0.01 to 20% by weight of auxiliaries. The invention likewise relates to a process for the production of these phosphorus-containing flame retardant agglomerates, and also to polymeric compositions and moldings which comprise these phosphorus-containing flame retardant agglomerates.
摘要翻译：本发明涉及含磷阻燃附聚物，其包含a）99.99至80重量％的由式（I）的次膦酸盐组成的和/或由式（I）的次膦酸盐和/或由式（I）的二膦酸盐组成的聚集体和/ II）和/或由它们的聚合物组成，其中R 1，R 2，R 2相同或不同，为C 1 -C 3烷基，直链或支链的亚烷基，和/或芳基; R 3是C 1 -C 10 - 亚烷基，直链或支链C 6 -C 13 - - 亚芳基， - 烷基亚芳基或 - 芳基亚烷基; M是Mg，Ca，Al，Sb，Sn，Ge，Ti，Fe，Zr，Ce，Bi，Sr，Mn，Li，Na，K和/或质子化氮碱; m为1〜4; n为1至4; x为1至4，b）为0.01至20重量％的助剂。本发明同样涉及一种生产这些含磷阻燃附聚物的方法，以及包含这些含磷阻燃剂附聚物的聚合物组合物和模制品。

85. 发明授权

US06254850B1 Metal complexes, suitable for use in diagnosis and therapy 失效
标题翻译：金属络合物，适用于诊断和治疗
公开(公告)号：US06254850B1
公开(公告)日：2001-07-03
申请号：US09480153
申请日：2000-01-10
申请人： Werner Krause , Franz-Karl Maier , Michael Bauer , Gabriele Schuhmann-Giampieri , Wolf-Rudiger Press , Peter Muschik
发明人： Werner Krause , Franz-Karl Maier , Michael Bauer , Gabriele Schuhmann-Giampieri , Wolf-Rudiger Press , Peter Muschik
IPC分类号： A61K5104
CPC分类号： A61K49/06 , C07C229/16 , C07C229/36 , C07C233/63 , C07C233/83 , C07C237/06
摘要： The invention relates to diethylenetriaminepentaacetic acid derivatives, their complexes and complex salts, containing an element of atomic numbers 20-32, 39-51 or 57-83, pharmaceutical agents containing these compounds, their use as contrast media and antidotes and process for their production.
摘要翻译：本发明涉及含有原子序数20-32,39-51或57-83的元素的二亚乙基三胺五乙酸衍生物及其络合物和络合盐，含有这些化合物的药剂，它们作为对照介质和解毒剂的用途及其生产方法。

86. 发明授权

US6156873A Bismuth dendrimers, processes for their preparation, and their use as x-ray contrast agents 失效
标题翻译：铋树枝状大分子，其制备方法以及它们作为X射线造影剂的用途
公开(公告)号：US6156873A
公开(公告)日：2000-12-05
申请号：US242673
申请日：1999-05-07
申请人： Werner Krause , Herbert Schumann
发明人： Werner Krause , Herbert Schumann
IPC分类号： A61K49/04 , C07F9/50 , C07F9/94 , C08G79/00
CPC分类号： C07F9/5009 , A61K49/0433 , C07F9/94
摘要： The invention relates to dendrimeric organometallic bismuth compounds (bismuth dendrimers), which can advantageously be used as x-ray contrast media, as well as processes for their production.
摘要翻译： PCT No.PCT / DE97 / 01823 Sec。 371日期1999年5月7日 102（e）日期1999年5月7日PCT 1997年8月18日PCT公布。出版物WO98 / 07732 日期1998年2月26日本发明涉及可有利地用作x射线造影剂的树枝状有机金属铋化合物（铋树枝状大分子）以及其生产方法。

87. 发明授权

US4503016A Process for extracting heavy metal ions from aqueous solutions 失效
标题翻译：从水溶液中提取重金属离子的方法
公开(公告)号：US4503016A
公开(公告)日：1985-03-05
申请号：US582138
申请日：1984-02-23
申请人： G/u/ nther Schimmel , Werner Krause , Reinhard Gradl
发明人： G/u/ nther Schimmel , Werner Krause , Reinhard Gradl
IPC分类号： C02F1/26 , C01B25/238 , C02F1/62 , C22B3/38 , C01G3/00 , C01G9/00 , C01G11/00 , C01G28/00
CPC分类号： C22B3/007 , C01B25/238 , Y02P10/234 , Y10S423/14
摘要： The disclosure relates to a process for liquid/liquid-extraction of heavy metal ions from acid aqueous solutions with the aid of water-insoluble dithiophosphoric acid diesters as extracting agents. More particularly, use is made of phosphoric acid solutions with a P.sub.2 O.sub.5 -content of from 3 to 80 weight %, the solutions being free from emulsion-forming organic contaminants or having previously been freed therefrom in known manner. The resulting aqueous phase is separated from the phase containing the dithiophosphoric acid diester.
摘要翻译：本公开涉及借助于不溶于水的二硫代磷酸二酯作为提取剂从酸性水溶液中液/液萃取重金属离子的方法。更具体地，使用P2O5含量为3至80重量％的磷酸溶液，该溶液不含乳液形成有机污染物，或者已知以已知的方式从其中释放出来。将得到的水相与含有二硫代磷酸二酯的相分离。

88. 发明授权

US4468355A Process for making 1-hydroxy-alkane-1-phosphonic acids 失效
标题翻译：制备1-羟基 - 烷烃-1-膦酸的方法
公开(公告)号：US4468355A
公开(公告)日：1984-08-28
申请号：US540191
申请日：1983-10-07
申请人： Werner Krause , Werner Pieper
发明人： Werner Krause , Werner Pieper
IPC分类号： C07F9/38
CPC分类号： C07F9/3808
摘要： The disclosure provides a novel process for making 1-hydroxyalkane-1-phosphonic acids by reacting an aldehyde with tetraphosphorus hexoxide.
摘要翻译：本公开提供了通过使醛与四氧化四磷反应制备1-羟基烷-1-膦酸的新方法。

89. 发明授权

US4452768A Process for removing heavy metal ions from wet-processed phosphoric acid 失效
标题翻译：从湿法磷酸中去除重金属离子的方法
公开(公告)号：US4452768A
公开(公告)日：1984-06-05
申请号：US455252
申请日：1983-01-03
申请人： Reinhard Gradl , Gunther Schimmel , Werner Krause , Gero Heymer
发明人： Reinhard Gradl , Gunther Schimmel , Werner Krause , Gero Heymer
IPC分类号： C01B25/238 , B01D11/04 , C01B25/237 , C01B25/46 , C01G1/00 , C01B25/16 , B01D11/00 , B03C1/00 , C01G17/00
CPC分类号： C01B25/237 , C22B3/24 , Y02P10/234
摘要： The disclosure relates to process for removing heavy metal ions, especially cadmium, copper, lead and mercury ions from wet-processed phosphoric acid. To this end, the crude acid is contacted with a mixture consisting of an adsorbent and a diorganyldithiophosphoric acid ester or, after treatment with the ester, the acid is contacted with the adsorbent alone, and the purified phosphoric acid is ultimately separated from the ester and adsorbent.
摘要翻译：本公开涉及从湿法处理的磷酸中去除重金属离子，特别是镉，铜，铅和汞离子的方法。为此，将粗酸与由吸附剂和二有机基二硫代磷酸酯组成的混合物接触，或者在用酯处理后，酸与吸附剂单独接触，纯化的磷酸最终与酯分离，吸附剂。

90. 发明授权

US09279085B2 Method for the production of monofunctionalized dialkylphosphinic acids, esters and salts, and use thereof 有权
标题翻译：用于制备单官能二烷基次膦酸，酯和盐的方法及其用途
公开(公告)号：US09279085B2
公开(公告)日：2016-03-08
申请号：US13140555
申请日：2009-10-06
申请人： Michael Hill , Harald Bauer , Werner Krause , Martin Sicken
发明人： Michael Hill , Harald Bauer , Werner Krause , Martin Sicken
IPC分类号： C07F9/02 , C07F9/22 , C07F9/28 , C08K5/53 , C09K21/12 , C07F9/30 , C07F9/32 , C08K5/5313
CPC分类号： C09K21/12 , C07F9/301 , C07F9/3211 , C08K5/5313
摘要： The invention relates to a method for producing monofunctionalized dialkylphosphinic acids, esters, and salts, characterized in that a phosphinic acid source (I) is reacted with olefins (IV) in the presence of a catalyst A to obtain an alkylphosphonous acid, the salt or ester thereof, whereupon said alkylphosphonous acid, the salt or ester (II) thereof is reacted with compounds containing C═C, C═O, or C═N double bonds to obtain compounds of type (III), wherein R1, R2, R3, R4, R5, R6 are identical or different from each other and independently represent, inter alia, H, C1-C18-alkyl, C6-C18-aryl, C6-C18-aralkyl, X represents, inter alia, H, C1-C18-alkyl, C6-C18-aryl, and/or Mg, Ca, Al, Sb, Sn, Ge, Ti, Fe, Zr, Zn, Ce, Bi, Sr, Mn, Cu, Ni, Li, Na, K, H, and wherein A represents OH, NH2, NHR, NR2, or O—CO—R8, and W represents a mineral acid, carboxylic acid, Lewis acid, or organic acid, wherein n is a whole or a fractional number from 0 to 4, and catalyst A represents transition metals and/or transition metal compounds and/or catalyst systems composed of a transition metal and/or a transition metal compound and at least one ligand. The use of said dialkylphosphonic acids, esters, and salts is also disclosed.
摘要翻译：本发明涉及一种制备单官能化二烷基次膦酸，酯和盐的方法，其特征在于，在催化剂A存在下，次膦酸源（I）与烯烃（Ⅳ）反应得到烷基亚磷酸，其盐或酯，因此所述烷基亚膦酸，其盐或酯（II）与含有C = C，C = O或C = N双键的化合物反应，得到式（III）化合物，其中R1，R2，R3 ，R 4，R 5，R 6彼此相同或不同，并且独立地代表H，C 1 -C 18 - 烷基，C 6 -C 18 - 芳基，C 6 -C 18 - 芳烷基，X尤其表示H， C18烷基，C6-C18-芳基和/或Mg，Ca，Al，Sb，Sn，Ge，Ti，Fe，Zr，Zn，Ce，Bi，Sr，Mn，Cu，Ni，Li，Na，K ，H，其中A表示OH，NH2，NHR，NR2或O-CO-R8，W表示无机酸，羧酸，路易斯酸或有机酸，其中n为0或分数至4，催化剂A代表转化我 tals和/或过渡金属化合物和/或由过渡金属和/或过渡金属化合物和至少一种配体组成的催化剂体系。还公开了所述二烷基膦酸，酯和盐的用途。

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