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    • 71. 发明授权
    • High-purity nitrogen gas production equipment
    • 高纯氮气生产设备
    • US4668260A
    • 1987-05-26
    • US845278
    • 1986-03-12
    • Akira Yoshino
    • Akira Yoshino
    • F17C9/04F25J3/04F25J3/00
    • F25J3/044F17C9/04F25J3/042F25J3/04218F25J3/04254F25J3/0426F25J3/0443F25J3/04636F25J3/04824F25J3/0486F17C2205/0326F17C2205/0341F17C2221/011F17C2221/014F17C2221/05F17C2223/0161F17C2223/033F17C2225/0123F17C2227/0311F17C2227/039F17C2227/045F17C2250/0408F17C2250/0439F17C2265/015F25J2200/30F25J2200/50F25J2200/74F25J2205/60F25J2210/42F25J2245/40F25J2245/42F25J2250/20F25J2250/40F25J2250/50F25J2290/10F25J2290/62Y10S62/913
    • There is disclosed high-purity nitrogen gas production equipment for production of ultra-high-purity nitrogen gas for use in the electronics and other industries, for example in connection with the production of silicon semiconductors. The conventional nitrogen gas production equipment of cryogenic air separation type tends to develop troubles and yields product nitrogen gas only at high cost and in comparatively low purity. The equipment according to the invention is such that a liquid nitrogen storage means (23) is connected via a first feeding pipeline (24a) to a distillation column (15) into which air is introduced from the outside via an air compression means (9) and heat exchange means (13), (14) while the above storage means (23) is also connected via a second feeding line (24b) to the above heat exchange means (13), (14). In this way, the raw material air is chilled to a cryogenic temperature as a result of absorption of the latent heat of evaporation by liquid nitrogen in the heat exchangers and the cryogenic compressed air is further chilled in the distillation column (15 ) by the heat of evaporation of liquid nitrogen. By taking advantage of the difference in boiling point, the nitrogen is withdrawn in gaseous state while oxygen is retained in liquid state. The resulting nitrogen gas is combined with the vaporized liquid nitrogen originating from the liquid nitrogen storage tank (23) to give product nitrogen gas. By these features, low-cost, high-purity nitrogen gas can be produced without machine troubles.
    • PCT No.PCT / JP85 / 00385 Sec。 371日期:1986年3月12日 102(e)日期1986年3月12日PCT提交1985年7月8日PCT公布。 出版物WO86 / 00693 日期为1986年1月30日。公开了用于生产用于电子等行业的超高纯度氮气的高纯度氮气生产设备,例如与硅半导体的生产有关。 常规的低温空气分离型氮气生产设备倾向于产生麻烦,仅以高成本和较低纯度产生产品氮气。 根据本发明的设备使得液氮存储装置(23)经由第一供给管线(24a)经由空气压缩装置(9)从外部引入空气的蒸馏塔(15)连接, 和热交换装置(13),(14),而上述存储装置(23)也经由第二供给管线(24b)连接到上述热交换装置(13),(14)。 以这种方式,原料空气由于在热交换器中吸收液氮的蒸发潜热而冷却至低温,低温压缩空气通过热量在蒸馏塔(15)中进一步冷却 的液氮蒸发。 通过利用沸点的差异,氮以气态取出,而氧保持在液态。 将得到的氮气与来自液氮储罐(23)的汽化液氮合并,得到产物氮气。 通过这些特征,可以在没有机器故障的情况下生产低成本,高纯度的氮气。
    • 74. 发明授权
    • 산소제조설비에 있어서의 액체공기 레벨 제어장치
    • 用于控制氧气制造装置中的液体空气水平的装置
    • KR100784029B1
    • 2007-12-07
    • KR1020010085274
    • 2001-12-26
    • 주식회사 포스코
    • 노경호김용엽강승익
    • F25J3/04
    • F25J3/04769F25J3/0486F25J2205/20F25J2220/52F25J2280/02
    • 본 발명은 철강생산시 사용되는 산소,질소,아르곤가스를 제조하는 산소제조설비의 제조공정에서 발생하는 이산화탄소(CO
      2 ) 및 탄화수소 성분이 액체공기를 저장하는 공기분리장치의 탱크 하부에 축적되면서 막히는 현상을 방지할 수 있도록 한 산소제조설비에 있어서의 액체공기 레벨 제어장치에 관한 것이다.
      본 발명은 공기분리장치내에서 미분리된 이산화탄소(CO
      2 ) 및 탄화수소 성분이 상기 공기분리장치의 하부에서 액체공기의 레벨을 감지하는 레벨발신기의 고압측 라인에 적치되는 것을 방지하기 위한 산소제조설비에 있어서의 액체공기 레벨 제어장치에 있어서, 상기 레벨발신기의 저압, 고압측 라인에 연결되어 차압의 변동에 따른 이상유무를 판정하는 차압검출부; 상기 고압측 라인에 연결설치되어 상기 공기분리장치내의 고체상태의 이산화탄소(CO
      2 ) 및 탄화수소 성분을 녹이는 가온장치부; 상기 차압검출부와 연결되어 상기 고압측 라인의 막힘 신호에 따라 배출밸브가 열려서 상기 가온장치부에 의해 녹은 이산화탄소(CO
      2 ) 및 탄화수소 성분을 배출하는 배출부;를 포함하여 구성된 것을 특징으로 한다.
      산소제조설비, 액체공기, 레벨발신기, 차압발신기, 방열판
    • 75. 发明授权
    • 심랭식 공기분리장치에 의한 질소가스 제조 방법
    • 심랭식공기분리장치에의한질소가스제조방심
    • KR100454810B1
    • 2004-11-05
    • KR1020020008421
    • 2002-02-18
    • 대성산업가스 주식회사
    • 문흥만용평순
    • F25J3/04
    • F25J3/04793F25J3/04254F25J3/044F25J3/0486F25J3/0489F25J2200/72F25J2210/42F25J2250/42F25J2250/52
    • PURPOSE: A method for generating nitrogen gas using cryogenic air separation unit is provided to maintain level of liquid surface of liquid-air separator or rectifying column to a certain level by sensing the elevation of liquid surface of the liquid-air separator and rectifying column and controlling supply of liquid nitrogen or liquid air. CONSTITUTION: The method for generating nitrogen gas using cryogenic air separation unit comprises the liquid nitrogen gas supply control process comprising a step of sensing level of liquid surface of liquid air of rectifying column(10) using first liquid surface meter(24), and a step of outputting low liquid surface signal if the level of the liquid surface is less than a certain level and opening the automatic valve so that liquid nitrogen is supplied to the rectifying column from liquid nitrogen storage tank(22) if the automatic valve is in the closed state by checking the state of automatic valve(19), and outputting high liquid surface signal if the level of the liquid surface is the same as or higher than a certain level and closing the automatic valve, thereby stopping supply of liquid nitrogen to the rectifying column from liquid nitrogen storage tank so that the level of liquid surface of the liquid air of the rectifying column is recovered to a certain level if the automatic valve is in the opened state by checking the state of the automatic valve; and the liquid air supply control process comprising a step of sensing elevation of liquid surface of liquid air of liquid-air separator(12) using second liquid surface meter(25), and a step of outputting low liquid surface signal if the elevation of the liquid surface is less than a certain level and opening the expansion valve so that liquid air is supplied to the liquid-air separator from the rectifying column if the expansion valve is in the closed state by checking the state of expansion valve(11), and outputting high liquid surface signal if the elevation of the liquid surface is the same as or higher than a certain level and closing the expansion valve, thereby stopping supply of liquid air to the liquid-air separator(12) from a lower region of the rectifying column so that the elevation of liquid surface of the liquid air is recovered to a certain level if the expansion valve is in the opened state by checking the state of the expansion valve.
    • 目的:提供一种利用低温空气分离装置产生氮气的方法,通过检测液 - 气分离器和精馏塔的液面高度,使液 - 气分离器或精馏塔的液面保持在一定水平,并且 控制液氮或液态空气的供应。 构成:使用低温空气分离单元产生氮气的方法包括液氮气体供应控制过程,该过程包括使用第一液体表面计量器(24)感测精馏塔(10)的液体空气的液面水平的步骤,以及 如果液面低于一定水平,则输出低液面信号的步骤,并打开自动阀,使得如果自动阀处于自动阀的状态,则液氮从液氮储罐(22)供应到精馏塔 通过检查自动阀(19)的状态来检测液体的关闭状态,并且如果液面的液位等于或高于一定水平并关闭自动阀,则输出高液面信号,从而停止向液体供给液氮 从液氮储罐中排出精馏塔,以使精馏塔液体空气的液面高度恢复到一定水平 通过检查自动阀的状态来使阀处于打开状态; 所述液体空气供应控制过程包括使用第二液体表面仪(25)感测液体 - 空气分离器(12)的液体空气的液面升高的步骤,以及如果所述液体空气分离器 液面低于一定水平并打开膨胀阀,以便通过检查膨胀阀(11)的状态在膨胀阀处于关闭状态时将液体空气从精馏塔供应到液气分离器,以及 如果液面的高度等于或高于一定水平并关闭膨胀阀,则输出高液面信号,从而停止从整流的下部区域向液气分离器(12)供应液体空气 以便通过检查膨胀阀的状态,如果膨胀阀处于打开状态,则液体空气的液面的高度恢复到一定水平。
    • 78. 发明专利
    • Low temperature air separating device
    • 低温空气分离装置
    • JP2004232967A
    • 2004-08-19
    • JP2003022508
    • 2003-01-30
    • Hitachi Ltd株式会社日立製作所
    • YOSHIDA JUNKANO TARO
    • B01D53/04F25J3/04
    • F25J3/04775F25J3/0409F25J3/04157F25J3/04181F25J3/04193F25J3/04206F25J3/04303F25J3/04412F25J3/0486F25J2205/32F25J2205/34F25J2205/68F25J2205/70F25J2245/40F25J2245/50F25J2250/40F25J2250/50
    • PROBLEM TO BE SOLVED: To provide a method and a device for controlling a low temperature air separating device having a pre-treatment device including an adsorption tower automatically controlled to optimum regenerative gas conditions. SOLUTION: This low temperature air separating device with a TSA system pre-treatment device comprises a DCS control calculator 30 having a function to monitor the peak value Tp and the final value Te of the regenerative gas outlet temperature of the adsorption tower 3 and, when the monitored value comes out of a proper range, automatically correcting regenerative gas conditions. The DCS control calculator 30 comprises a function to predict the regenerative gas outlet temperature by using an air temperature Ti at an inlet to the adsorption tower 3 by automatically functionally generating the optimum values of the regenerative gas conditions subsequent to the air temperature Ti and automatically performing a control to correct that temperature. COPYRIGHT: (C)2004,JPO&NCIPI
    • 解决的问题:提供一种控制低温空气分离装置的方法和装置,其具有包括自动控制到最佳再生气体条件的吸附塔的预处理装置。 解决方案:具有TSA系统预处理装置的这种低温空气分离装置包括DCS控制计算器30,其具有监测吸附塔3的再生气体出口温度的峰值Tp和最终值Te的功能 并且当监测值超出适当范围时,自动校正再生气体条件。 DCS控制计算器30包括通过在空气温度Ti之后自动功能地产生再生气体条件的最佳值并且自动执行的功能,通过在吸附塔3的入口处使用空气温度Ti来预测再生气体出口温度的功能 一个控制来纠正这个温度。 版权所有(C)2004,JPO&NCIPI