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71. 发明授权

US2628259A Process of making vinylidene chloride and vinyl chloride 失效
标题翻译：制造偏二氯乙烯和氯乙烯的工艺
公开(公告)号：US2628259A
公开(公告)日：1953-02-10
申请号：US78447647
申请日：1947-11-06
申请人： DOW CHEMICAL CO
发明人： DIRSTINE PHILIP H , DANCE ELDRED L
IPC分类号： C07C17/00
CPC分类号： C07C17/00 , C07C17/10 , C07C21/06 , C07C21/08

72. 发明授权

US2610214A Method of preparing vinylidene chloride 失效
公开(公告)号：US2610214A
公开(公告)日：1952-09-09
申请号：US7973849
申请日：1949-03-05
申请人： DOW CHEMICAL CO
发明人： AMOS JAMES L
IPC分类号： C07C17/25
CPC分类号： C07C17/25 , C07C21/08

73. 发明授权

US2136348A Stabilizing vinylidene chloride 失效
公开(公告)号：US2136348A
公开(公告)日：1938-11-08
申请号：US19761638
申请日：1938-03-23
申请人： DOW CHEMICAL CO
发明人： WILEY RALPH M
IPC分类号： C07C17/42
CPC分类号： C07C17/42 , C07C21/08

74. 发明授权

US08207384B2 Catalytic gas phase fluorination of 243db to 1234yf 有权
标题翻译：催化气相氟化243db至1234yf
公开(公告)号：US08207384B2
公开(公告)日：2012-06-26
申请号：US12978288
申请日：2010-12-23
申请人： Laurent Wendlinger , Anne Pigamo , Dominique Deur-Bert
发明人： Laurent Wendlinger , Anne Pigamo , Dominique Deur-Bert
IPC分类号： C07C17/00
CPC分类号： C07C17/206 , B01J23/866 , B01J37/26 , C07C17/25 , C07C17/42 , C07C21/08 , Y02P20/582 , C07C19/10 , C07C21/18
摘要： The invention provides a process for preparing 1234yf, comprising: (i) contacting 243db with hydrogen fluoride HF in gas phase in the presence of a fluorination catalyst under conditions sufficient to produce a reaction mixture; (ii) separating the reaction mixture into a first stream comprising HCl, 1234yf and a second stream comprising HF, 1233xf and 245cb; (iii) recycling at least a part of the second stream at least in part back to step (i). The invention also provides a process for preparing 1234yf, comprising: (i) contacting 243db with hydrogen fluoride HF in gas phase in the presence of a fluorination catalyst under conditions sufficient to produce a reaction mixture; (ii) separating the reaction mixture into HCl and a stream containing the fluorinated products; (iii) separating said stream containing the fluorinated products into a first stream comprising 1234yf and a second stream comprising HF, 1233xf and 245cb; (iv) recycling at least a part of the second stream at least in part back to step (i).
摘要翻译：本发明提供一种制备1234yf的方法，其包括：（i）在足以产生反应混合物的条件下，在氟化催化剂存在下，使气体中的243db与氟化氢HF接触; （ii）将反应混合物分离成包含HCl，1234yf和包含HF，1233xf和245cb的第二料流的第一料流; （iii）至少部分地将第二流的至少一部分再循环回到步骤（i）。本发明还提供了一种制备1234yf的方法，其包括：（i）在足以产生反应混合物的条件下，在氟化催化剂存在下，将气体中的243db与氟化氢HF气相接触; （ii）将反应混合物分离成HCl和含有氟化产物的料流; （iii）将含有氟化产物的物流分离成包含1234yf的第一物流和包含HF，1233xf和245cb的第二物流; （iv）至少部分地将至少一部分第二流再循环到步骤（i）。

75. 发明申请

US20080242902A1 Composition For the Vapor Phase Dehydrohalogenation of 1,1,2-Trihaloethane To 1,1-Dihaloethylene and Methods For Preparing and Using Such Composition 失效
标题翻译： 1,1,2-三氯乙烷对1,1-二卤乙烯的气相脱卤化氢的组成及其制备方法
公开(公告)号：US20080242902A1
公开(公告)日：2008-10-02
申请号：US11913803
申请日：2005-06-03
申请人： Yurii Oleksiyovych Serhuchev , Yurii Vasyliyovych Bilokopytov , Igorlvanovych Chernobaev
发明人： Yurii Oleksiyovych Serhuchev , Yurii Vasyliyovych Bilokopytov , Igorlvanovych Chernobaev
IPC分类号： C07C17/25 , B01J31/02
CPC分类号： C07D487/04 , B01J21/18 , B01J31/0244 , B01J31/0254 , C07C17/25 , C07D235/04 , C07C21/08
摘要： Described are compositions adapted to catalyze the vapor phase dehydrohalogenation of 1,1,2-trihaloethane to 1,1-dihaloethylene, e.g., 1,1,2-trichloroethane to vinylidene chloride. These materials include activated carbon and at least one benzimidazole-containing material defined herein as including benzimidazole, a derivative thereof, a salt thereof or mixtures thereof. Also described are methods for producing and using these catalytic compositions.
摘要翻译：描述了适于催化1,1,2-三氯乙烷至1,1-二卤代乙烷（例如1,1,2-三氯乙烷）至偏二氯乙烯的气相脱卤化氢的组合物。这些材料包括活性炭和本文所定义的至少一种含苯并咪唑的材料，包括苯并咪唑，其衍生物，其盐或其混合物。还描述了用于生产和使用这些催化组合物的方法。

76. 发明授权

US07268262B2 Method for recovering trans-1,2-dichloroethene 有权
标题翻译：回收1,2-二氯乙烯的方法
公开(公告)号：US07268262B2
公开(公告)日：2007-09-11
申请号：US10834408
申请日：2004-04-29
申请人： Clark S. Graybill , Stephen R. Lester
发明人： Clark S. Graybill , Stephen R. Lester
IPC分类号： C07C17/358 , C07C21/02
CPC分类号： C07C17/38 , C07C17/383 , C07C17/395 , Y02P20/127 , C07C21/08
摘要： Describes a method for recovering trans-1,2-dichloroethene from a liquid feed composition comprising both the cis-and trans-isomers of 1,2-dichloroethene and contaminating amounts of other chlorinated hydrocarbons, e.g., lower alkyl chlorinated hydrocarbons, such as C1-C2 chlorinated hydrocarbons. In one of the described methods, the liquid feed composition is introduced into a first distillation column 10 wherein the stereoisomers and chlorinated hydrocarbons more volatile than the stereoisomers are removed as overhead 12 and charged to a second distillation column 20. In column 20, the stereoisomers are separated from the more volatile chlorinated hydrocarbons, and a bottoms fraction 24 comprising the stereoisomers is charged to a reactive distillation column 30 wherein the cis-isomer is isomerized to the trans-isomer in the liquid phase and in the presence of an organic free-radical initiator, e.g., an azonitrile initiator. Substantially pure trans 1,2-dichloroethene is recovered as overhead 32 from reactive distillation column 30.
摘要翻译：描述了从包含1,2-二氯乙烯的顺式和反式异构体和污染量的其它氯化烃（例如低级烷基氯化烃）的液体进料组合物中回收反式1,2-二氯乙烯的方法，例如C 1 - 2 C 2氯化烃。在所述方法之一中，将液体进料组合物引入第一蒸馏塔10中，其中立体异构体和比立体异构体更易挥发的氯代烃作为塔顶馏出物12被除去并装入第二蒸馏塔20。在第20列中，将立体异构体与更易挥发的氯代烃分离，将包含立体异构体的塔底馏分24装入反应性蒸馏塔30中，其中顺式异构体在液相中异构化为反式异构体，存在有机自由基引发剂，例如偶氮腈引发剂。从反应蒸馏塔30回收基本上纯的反式1,2-二氯乙烯作为塔顶馏出物32。

77. 发明申请

US20060014661A1 1,2-Dichloroethylene compositions 有权
标题翻译： 1,2-二氯乙烯组合物
公开(公告)号：US20060014661A1
公开(公告)日：2006-01-19
申请号：US10780449
申请日：2004-02-13
申请人： Michael Dobrasko , Ronald Olinger
发明人： Michael Dobrasko , Ronald Olinger
IPC分类号： C11D17/00
CPC分类号： C23G5/0289 , C07C17/42 , C23G5/02806 , C23G5/0288 , H05K3/26 , C07C21/08
摘要： Describes compositions of 1,2-dichloroethylene, particularly trans-1,2-dichloroethylene, stabilized with effective stabilizing amounts of a combination of (a) C3 to C12 alkylene oxide, e.g., butylene oxide, (b) alcohol chosen from aliphatic and cycloaliphatic alcohols having from 2 to 8 carbon atoms, e.g., isopropanol, and (c) a material chosen from (i) C1 to C5 alkoxyphenol, e.g., 4-methoxyphenol, (ii) free radical stabilizer having at least one 2,2,6,6-tetra(lower alkyl)-1-piperidinyloxy-yl group, and (iii) mixtures of (i) and (ii). Also describes use of such compositions for vapor degreasing of soiled articles, e.g., metal parts and soldered circuit boards.
摘要翻译：描述了用有效稳定量的（a）C3至C12环氧烷的组合（例如环氧丁烷）稳定的1,2-二氯乙烯，特别是反式-1,2-二氯乙烯的组合物，（b）选自脂族和脂环族具有2至8个碳原子的醇，例如异丙醇，和（c）选自（i）C1至C5烷氧基苯酚的物质，例如4-甲氧基苯酚，（ii）具有至少一个2,2,6 ，6-四（低级烷基）-1-哌啶氧基 - 基，和（iii）（i）和（ii）的混合物。还描述了这种组合物用于蒸汽去污污染物品例如金属部件和焊接电路板的用途。

78. 发明授权

US06924403B2 Synthesis of hexafluoropropylene 有权
标题翻译：六氟丙烯的合成
公开(公告)号：US06924403B2
公开(公告)日：2005-08-02
申请号：US10431407
申请日：2003-05-07
申请人： John James Barnes , Kenneth Paul Kelch , Thomas D. Sandbrook , David John Van Bramer
发明人： John James Barnes , Kenneth Paul Kelch , Thomas D. Sandbrook , David John Van Bramer
IPC分类号： C07C17/37 , C07B61/00 , C07C17/26 , C07C17/269 , C07C21/18 , C07C17/25 , C07C17/093 , C07C17/35
CPC分类号： C07C17/26 , C07C17/269 , C07C21/08 , C07C21/18
摘要： The present invention relates to the process of pyrolyzing tetrafluoroethylene to hexafluoropropylene by carrying out the pyrolysis in a tubular reactor that is lined with either nickel or nickel alloy which contains no greater than 8 wt % chromium.
摘要翻译：本发明涉及通过在包含不超过8重量％铬的镍或镍合金衬里的管式反应器中进行热解而将四氟乙烯热解为六氟丙烯的方法。

79. 发明申请

US20040002621A1 Synthesis of hexafluoropropylene 有权
标题翻译：六氟丙烯的合成
公开(公告)号：US20040002621A1
公开(公告)日：2004-01-01
申请号：US10431407
申请日：2003-05-07
发明人： John James Barnes , Kenneth Paul Kelch , Thomas D. Sandbrook , David John Van Bramer
IPC分类号： C07C017/266
CPC分类号： C07C17/26 , C07C17/269 , C07C21/08 , C07C21/18
摘要： The present invention relates to the process of pyrolyzing tetrafluoroethylene to hexafluoropropylene by carrying out the pyrolysis in a tubular reactor that is lined with either nickel or nickel alloy which contains no greater than 8 wt % chromium.
摘要翻译：本发明涉及通过在包含不超过8重量％铬的镍或镍合金衬里的管式反应器中进行热解而将四氟乙烯热解为六氟丙烯的方法。

80. 发明授权

US3714008A Inhibitors for aqueous phase, radiation polymerization 失效
标题翻译：水相抑制剂，辐射聚合
公开(公告)号：US3714008A
公开(公告)日：1973-01-30
申请号：US3714008D
申请日：1970-05-12
申请人： JAPAN ATOMIC ENERGY RES INST
发明人： TAKEHISA M , SENRUI S
IPC分类号： C07C7/20 , C07C17/42 , C08F2/38 , C08F2/54 , C08D1/00 , C08F1/16
CPC分类号： C07C17/42 , C07C7/20 , C08F2/38 , C07C15/46 , C07C11/06 , C07C11/08 , C07C21/06 , C07C21/08
摘要： In the polymerization, in which an aqueous phase is employed, of ethylene, or ethylene and other unsubstituted or substituted olefinic monomers by means of an ionizing radiation, formation of an undesirable polymer in the aqueous phase of the reaction system is inhibited by using specific polymerization inhibitors. The inhibitors which have no adverse effect on the polymerization in the non-aqueous phase, comprise the electrolytes which have strong oxidizing action and/or react at high reaction rate with active species such as H radicals, OH radicals and/or hydrated electrons formed by ionizing radiation. According to the present invention, adhesion of undesirable polymer to the reactor walls during polymerization reaction is prevented and contamination which lowers the quality of the main polymer is eliminated.
摘要翻译：在使用水相的乙烯或乙烯和其它未取代或取代的烯属单体的聚合中，通过电离辐射，在反应体系的水相中形成不需要的聚合物通过使用特定的聚合来抑制抑制剂。对非水相中的聚合没有不利影响的抑制剂包括具有强氧化作用和/或以高反应速率与活性物质如H自由基，OH自由基和/或水合电子反应的电解质，电离辐射。根据本发明，防止了聚合反应期间不期望的聚合物对反应器壁的粘附，并且消除了降低主聚合物质量的污染。

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