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71. 发明授权

US4925646A Process and composition for drying of gaseous hydrogen halides 失效
标题翻译：用于干燥气态卤化氢的方法和组合物
公开(公告)号：US4925646A
公开(公告)日：1990-05-15
申请号：US357049
申请日：1989-05-25
申请人： Glenn M. Tom , Duncan W. Brown
发明人： Glenn M. Tom , Duncan W. Brown
IPC分类号： B01D53/28 , C01B7/07 , C01B7/09 , C01B7/13 , C01B7/19 , C01G1/06
CPC分类号： C01B7/093 , B01D53/28 , C01B7/0718 , C01B7/135 , C01B7/197 , C01G1/06
摘要： A process for drying a gaseous hydrogen halide of the formula HX, wherein X is bromine, Chlorine, FLuorine, or iodine, to remove water impurity therefrom, in which a scavenger precursor composition is provided, including a support having associated therewith partially or fully alkylated metal alkyl compounds or pendant groups. The precursor composition is reacted with gaseous hydrogen halide to convert the metal alkyl compounds and/or pendant functional groups to the corresponding metal halide compounds and/or pendant functional groups, which in turn react with the water impurity to produce an essentially completely water-free (below 0.1 ppm) gaseous hydrogen halide effluent. The process of the invention has utility for producing high purity, anhydrous gaseous hydrogen halides for semiconductor manufacturing operations.
摘要翻译：一种用于干燥式HX的气态卤化氢的方法，其中X是溴，氯，氟嘌呤或碘，以除去其中含有杂质的水分杂质，其中提供了一种清除剂前体组合物，包括其部分或完全烷基化的载体金属烷基化合物或侧基。前体组合物与气态卤化氢反应以将金属烷基化合物和/或侧链官能团转化成相应的金属卤化物化合物和/或侧基官能团，其又与水杂质反应以产生基本上完全无水的（低于0.1ppm）气态卤化氢流出物。本发明的方法可用于生产用于半导体制造操作的高纯度无水气态卤化氢。

72. 发明授权

US3402525A Separation of hydrogen fluoride from gas mixtures containing hydrogen chloride and hydrogen fluoride 失效
标题翻译：从含有氯化氢和氟化氢的气体混合物中分离氟化氢
公开(公告)号：US3402525A
公开(公告)日：1968-09-24
申请号：US67876367
申请日：1967-10-27
申请人： HOECHST AG
发明人： PETER FRISCH , JURGEN KORINTH
IPC分类号： C01B7/00 , C01B13/10 , C01B13/11
CPC分类号： C01B7/197 , C01B7/0725 , C01B7/0737 , C01B7/195

73. 发明专利

JP5931867B2 フッ素の精製方法有权
标题翻译：纯化氟方法
公开(公告)号：JP5931867B2
公开(公告)日：2016-06-08
申请号：JP2013522239
申请日：2011-08-03
申请人：ソルヴェイ(ソシエテアノニム)
发明人：オリヴィエロ・ダイアナ , ペーター・エム・プレディカント , フィリップ・モレル , マウリッツィオ・パガーニン , クリストフ・ゾンマー
IPC分类号： C01B7/20
CPC分类号： C01B7/20 , C01B7/197 , H01L21/02057 , H01L21/30604

74. 发明专利

JP5817373B2 トランス−1,3,3,3−テトラフルオロプロペンの製造方法有权
标题翻译：对于反式1,3,3,3-四氟丙烯的方法
公开(公告)号：JP5817373B2
公开(公告)日：2015-11-18
申请号：JP2011202071
申请日：2011-09-15
申请人：セントラル硝子株式会社
发明人：日比野泰雄 , 吉川悟 , 西口祥雄 , 岡本覚 , 佐久冬彦
IPC分类号： C07C21/18 , C07C17/38 , C07C17/20
CPC分类号： C07C17/206 , B01J21/04 , B01J21/18 , B01J23/26 , B01J27/12 , B01J27/128 , B01J27/132 , B01J27/135 , B01J27/138 , B01J37/0201 , B01J37/26 , C01B7/0737 , C01B7/196 , C01B7/197 , C07C17/38 , C07C17/383 , Y02P20/582

76. 发明专利

JP2012116830A Method for producing trance-1,3,3,3-tetrafluoropropene 有权
标题翻译：用于生产1,3,3,3-四氯丙烯的方法
公开(公告)号：JP2012116830A
公开(公告)日：2012-06-21
申请号：JP2011202071
申请日：2011-09-15
申请人： Central Glass Co Ltd , セントラル硝子株式会社
发明人： HIBINO YASUO , YOSHIKAWA SATORU , NISHIGUCHI SACHIO , OKAMOTO SATORU , SAKU FUYUHIKO
IPC分类号： C07C17/20 , B01J27/132 , C07B61/00 , C07C17/383 , C07C21/18
CPC分类号： C07C17/206 , B01J21/04 , B01J21/18 , B01J23/26 , B01J27/12 , B01J27/128 , B01J27/132 , B01J27/135 , B01J27/138 , B01J37/0201 , B01J37/26 , C01B7/0737 , C01B7/196 , C01B7/197 , C07C17/38 , C07C17/383 , Y02P20/582 , C07C21/18
摘要： PROBLEM TO BE SOLVED: To provide a method for efficiently obtaining trans-1,3,3,3-tetrafluoropropene by reusing an unreacted material.SOLUTION: The method comprises: a reaction step of reacting 1-chloro-3,3,3-trifluoropropene and HF to obtain a product including trans-1,3,3,3-tetrafluoropropene, unreacted 1-chloro-3,3,3-trifluoropropene and HF, and by-produced cis-1,3,3,3-tetrafluoropropene, 1,1,1,3,3-pentafluoropropane and HCL; a rough separation step of distilling the product to recover 1-chloro-3,3,3-trifluoropropene and HF and supply them to the reaction step; a hydrogen fluoride separation step of recovering HF from the residue after the step, and supplying it to the reaction step; a hydrogen chloride separation step of bringing water or NaOH aqueous solution into contact with the residue after the step to remove HCL; a drying step of dehydrating the residue after the step; and a purification step of distilling the residue after the step.
摘要翻译：待解决的问题：提供通过重复使用未反应材料有效获得反式-1,3,3,3-四氟丙烯的方法。解决方案：该方法包括：使1-氯-3,3,3-三氟丙烯与HF反应得到包含反式-1,3,3,3-四氟丙烯，未反应的1-氯-3 ，3,3-三氟丙烯和HF，以及副产的顺式-1,3,3,3-四氟丙烯，1,1,1,3,3-五氟丙烷和HCL; 蒸馏产物以回收1-氯-3,3,3-三氟丙烯和HF并将其供应到反应步骤的粗分离步骤; 氟化氢分离步骤，从步骤后的残渣中回收HF，并将其供给到反应步骤; 氯化氢分离步骤，在步骤之后使水或NaOH水溶液与残留物接触以除去HCL; 干燥步骤，使步骤后的残渣脱水; 以及在该步骤之后蒸馏残余物的纯化步骤。版权所有（C）2012，JPO＆INPIT

77. 发明专利

JP4122769B2 Of hydrogen fluoride recovery process 有权
公开(公告)号：JP4122769B2
公开(公告)日：2008-07-23
申请号：JP2001563430
申请日：2001-03-02
申请人：ダイキン工業株式会社
发明人：昌宏近藤 , 洋之助逢坂
IPC分类号： C01B7/19 , B01J41/04 , B01J49/00 , C02F1/42
CPC分类号： B01J41/04 , C01B7/197 , C02F1/42

78. 发明专利

JP2007524502A Apparatus and method for purifying corrosive gases flow 审中-公开
公开(公告)号：JP2007524502A
公开(公告)日：2007-08-30
申请号：JP2006517572
申请日：2004-06-23
申请人：インテグリス・インコーポレーテッド
发明人：アルバレス，ダニエル，ジユニア , グエン，トラム・デイー , スピーゲルマン，ジエフリー・ジエイ , ホルムズ，ラツセル・ジエイ , レフ，ダニエル・エイ
IPC分类号： B01D53/28 , B01D53/02 , B01D53/26 , B01J20/06 , B01J20/34
CPC分类号： B01J20/3204 , B01D53/261 , B01D53/28 , B01J20/0211 , B01J20/041 , B01J20/06 , B01J20/28057 , B01J20/28097 , B01J20/3236 , B01J20/3433 , B01J20/3458 , B01J20/3483 , C01B7/0718 , C01B7/0743 , C01B7/093 , C01B7/096 , C01B7/197 , C01B7/20 , C01B7/24
摘要： A process, composition and apparatus for the removal of impurities from corrosive gases, particularly halogen-containing gases, down to about 100 ppb concentration are described. The critical component is zirconia (ZrO 2 ), which in a variety of physical forms is capable of dehydrating such gases. The zirconia can be in the form of a coating on a substrate, as a granular bulk material, or deposited within the pores of a porous body. The zirconia is retained in a simple container which is easily installed in a gas supply line, such as to a gas- or vapor-deposition manufacturing unit. The purification process can be operated for long periods of time in the presence of these gases. The invention provides final purification to gas streams intended for gas- or vapor-deposition formation of high purity electronic, prosthetic or similar products, and can be used in combination with a preliminary dehydration process or a solid particulate removal unit upstream.

79. 发明公开

EP3010637A2 A PROCESS FOR THE REMOVAL OF METAL CONTAMINANTS FROM FLUIDS 审中-公开
标题翻译：方法去除金属污染物的油液
公开(公告)号：EP3010637A2
公开(公告)日：2016-04-27
申请号：EP14812933.1
申请日：2014-06-17
申请人： Reliance Industries Limited
发明人： KUMAR, Prakash , PURANIK, Vijayalakshmi Ravi , PATIL, Mallikarjun , GOPALKRISHNAN, Kalpana , JASRA, Raksh Vir
IPC分类号： B01J20/08 , B01D53/58
CPC分类号： C01B7/0718 , C01B7/093 , C01B7/197 , C07C7/12
摘要： The present disclosure provides a process for removing metal contaminants from a contaminated fluid stream comprising the step of contacting said fluid stream with macroporous alpha alumina to obtain a fluid stream containing less than 50 ppm of metal. The fluid stream can be selected from the group consisting of a stream of mineral acid(s) and a stream of alkylene(s); and the metal contaminant can be at least one of elemental metals and metal oxides. The process further comprises a step of obtaining spent macroporous alpha alumina and regenerating active macroporous alpha alumina therefrom by washing said spent macroporous alpha alumina with at least one purified stream selected from the group consisting of a stream of mineral acid(s) and a stream of alkylene(s).

80. 发明授权

EP1092678B1 Method for removing water from gaseous hydrogen halide 有权
标题翻译：一种用于水从气态卤化氢分离过程
公开(公告)号：EP1092678B1
公开(公告)日：2011-12-28
申请号：EP00121382.6
申请日：2000-10-12
申请人： AIR PRODUCTS AND CHEMICALS, INC.
发明人： Dong, Chun CHristine , Schwarz, Alexander , Roth, Dean V. , Christman, Delbert Dean
IPC分类号： C01B7/07 , B01D53/26 , B01J20/04
CPC分类号： C01B7/197 , B01D53/261 , B01D2253/102 , B01J20/046 , B01J20/20 , B01J20/28057 , B01J20/3078 , B01J20/3204 , B01J20/3236 , C01B7/0718 , C01B7/093 , C01B7/135 , Y10S95/901

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