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71. 发明公开

EP1698606A1 FLUORINATING AGENT AND METHOD FOR PRODUCING FLUORINE-CONTAINING COMPOUND USING SAME 有权
标题翻译：氟化和方法用于生产含福陆连接按及其应用
公开(公告)号：EP1698606A1
公开(公告)日：2006-09-06
申请号：EP04808022.0
申请日：2004-12-21
申请人： Sumitomo Chemical Company, Limited
发明人： HAGIYA, Koji
IPC分类号： C07C17/20 , C07C17/093 , C07C19/08 , C07C22/08 , C07D233/58 , C07D213/61 , C07B39/00
CPC分类号： C07D233/64 , C07B39/00 , C07C17/093 , C07C17/202 , C07C201/12 , C07D213/61 , C07D233/56 , C07C19/08 , C07C22/08 , C07C205/12
摘要： A method for producing a fluorine-containing organic compound represented by the formula (7):

R-Fm (7)

wherein R represents a substituted or unsubstituted saturated hydrocarbon group, or a substituted or unsubstituted aromatic group and m represents an integer satisfying the inequality: 1≦m≦n, which comprises reacting a fluorinating agent represented by the formula (1):

wherein R 1 and R 3 are the same or different, and represent an optionally substituted alkyl group, R 2 , R 4 and R 5 are the same or different, and represent a hydrogen atom or an optionally substituted alkyl group, x satisfies 0 - represents a monovalent anion other than a fluoride ion,
with an organic compound of the formula (6):

R-Ln (6)

wherein R is the same as defined above, L represents a leaving group and n represents an integer of 1 or more, and a fluorinating agent using the same are described.
摘要翻译： €ƒ€ƒ€ƒ€ƒ€ƒ€ƒ€ƒ€ƒR-FM€ƒ€ƒ€ƒ€ƒ€ƒ（7）worin：一种由式（7）制作表示的含氟有机化合物的方法 řdarstellt一个substituiertem奥德unsubstituiertem饱和烃基，或一个substituiertem奥德unsubstituiertem芳族基团，m darstellt整数满足不等式：1个‰‰| M | N，该方法包括使由式（1）表示的氟化剂：worinř 1和R 3是相同的或不同的，并且在任选取代的烷基表示，R 2，R 4和R 5是相同的或不同的，并表示氢原子或任选取代的烷基，X SATIS外资企业0

72. 发明公开

EP1473275A1 METALLIZED MESOPOROUS SILICATE AND METHOD OF OXIDATION WITH THE SAME 审中-公开
标题翻译： METALLISIERTESMESOPORÖSESSILIKAT UND VERFAHREN ZUR OXIDATION DAMIT
公开(公告)号：EP1473275A1
公开(公告)日：2004-11-03
申请号：EP03737492.3
申请日：2003-02-05
申请人： Sumitomo Chemical Company, Limited
发明人： HAGIYA, Koji
IPC分类号： C01B33/20 , C07D309/30 , C07C35/14 , C07C29/03 , C07C43/23 , C07C41/05 , C07C67/44 , C07C69/78 , C07C407/00 , C07C409/04
CPC分类号： C07D309/30 , C01B37/005 , C07C29/48 , C07C41/06 , C07C67/39 , C07C67/42 , C07C67/44 , C07C407/00 , C07C2601/14 , C07C69/78 , C07C35/14 , C07C43/196 , C07C409/04
摘要： A metallized mesoporous silicate which is obtained by (i) reacting (a) either a metal peroxide obtained by the reaction of an aqueous hydrogen peroxide solution with at least one metal or metal compound selected from the group consisting of the following 1) to 4) 1) tungsten 2) molybdenum 3) vanadium 4) compounds comprising 4a) any of tungsten, molybdenum, and vanadium and 4b) at least one element selected from Groups 13 to 16 (excluding oxygen) or a solution of the metal peroxide with (b) a silicon compound in the presence of an alkylamine or a quaternary ammonium salt and separating the resultant silicate; and a process for producing the metallized mesoporous silicate. Also provided is a method of organic synthesis with the silicate.
摘要翻译：一种金属化中孔硅酸盐，其通过以下步骤获得：（i）使（a）通过过氧化氢水溶液与至少一种选自以下1）至4）中的至少一种金属或金属化合物反应获得的金属过氧化物反应， 1）钨2）钼3）钒4）包含4a）任何钨，钼和钒的化合物和4b）至少一种选自第13至16族（不包括氧）的元素或金属过氧化物与（b ）在烷基胺或季铵盐存在下的硅化合物，并分离所得的硅酸盐; 以及用于制备金属化中孔硅酸盐的方法。还提供了一种利用硅酸盐进行有机合成的方法。

73. 发明公开

EP4186882A1 METHOD FOR PRODUCING OPTICALLY ACTIVE COMPOUND 审中-实审
公开(公告)号：EP4186882A1
公开(公告)日：2023-05-31
申请号：EP21842357.2
申请日：2021-07-06
申请人： SUMITOMO CHEMICAL COMPANY, LIMITED
发明人： LUTETE, Leopold Mpaka , HAGIYA, Koji
IPC分类号： C07B53/00 , C07C209/62 , C07C211/60 , C07C231/12 , C07C233/07 , C07F15/06 , C07B61/00 , C07D215/08 , C07D231/14 , B01J31/22
摘要： An object of the present invention is to provide a further more effective process for preparing a certain optically active compound including an optically active 1-acetyl-2,2,4-trimethyl-1,2,3,4-tetrahydroquinoline.
The present invention provides a process for an optically active compound represented by formula (3) (wherein R 5 represents a hydrogen atom etc., R 6 and R 7 each independently represents a hydrogen atom, etc., R 8 represents a C1-C6 alkyl group, and R 9 , R 10 and R 11 each independently represents a hydrogen atom, etc.. The carbon atom with a symbol of the asterisked "*" represents an asymmetric carbon atom),
which comprises a reacting a compound represented by formula (2) (wherein R 5 , R 6 , R 7 , R 8 , R 9 , R 10 , and R 11 has the same meanings as the above) with hydrogen in the presence of asymmetric cobalt complex.

74. 发明授权

EP2044013B1 PROCESS FOR PRODUCING 2-HYDROXY-4-(METHYLTHIO)BUTYRATE COMPOUNDS AND INTERMEDIATES THEREOF 有权
标题翻译：用于生产2-羟基-4-（甲硫基）BUTYRATVERBINDUNGEN及其中间体
公开(公告)号：EP2044013B1
公开(公告)日：2013-05-29
申请号：EP07768484.3
申请日：2007-07-20
申请人： Sumitomo Chemical Company, Limited
发明人： HAGIYA, Koji
IPC分类号： C07C323/22 , C07C319/20 , C07C323/50
CPC分类号： C07C319/20 , C07C323/22 , C07C323/52

75. 发明授权

EP1698606B1 FLUORINATING AGENT AND METHOD FOR PRODUCING FLUORINE-CONTAINING COMPOUND USING SAME 有权
标题翻译：氟化和方法用于生产含福陆连接按及其应用
公开(公告)号：EP1698606B1
公开(公告)日：2013-02-20
申请号：EP04808022.0
申请日：2004-12-21
申请人： Sumitomo Chemical Company, Limited
发明人： HAGIYA, Koji
IPC分类号： C07C17/20 , C07C17/093 , C07C19/08 , C07C22/08 , C07C205/12 , C07D233/58 , C07D213/61 , C07B39/00 , C07D233/56 , C07D233/64
CPC分类号： C07D233/64 , C07B39/00 , C07C17/093 , C07C17/202 , C07C201/12 , C07D213/61 , C07D233/56 , C07C19/08 , C07C22/08 , C07C205/12

76. 发明授权

EP1790628B1 METHOD FOR PRODUCING UNSATURATED VICINAL DIOL COMPOUND 有权
标题翻译： METHOD FOR生产不饱和邻二醇化合物
公开(公告)号：EP1790628B1
公开(公告)日：2012-08-01
申请号：EP05783582.9
申请日：2005-09-09
申请人： Sumitomo Chemical Company, Limited
发明人： HAGIYA, Koji
IPC分类号： C07C29/10 , B01J29/035 , B01J29/90 , B01J38/00 , C07C33/035
CPC分类号： B01J23/30 , B01J23/28 , B01J29/0308 , B01J29/04 , B01J29/041 , B01J35/1061 , C07C29/106 , C07C33/035
摘要： Disclosed is a method for producing an unsaturated vicinal diol compound represented by the formula (2) below which is characterized in that an unsaturated epoxy compound represented by the formula (1) below is reacted with water in the presence of a silicate which contains at least one element selected from the group consisting of group V elements and group VI elements of the long form periodic table as a constituent. (1) (In the formula (1), R1, R2, R3, R4, R5 and R6 may be the same as or different from one another and respectively represent a hydrogen atom; an alkyl group having 1-20 carbon atoms which may be substituted by a halogen atom, an alkoxy group having 1-6 carbon atoms, an alkoxycarbonyl group having 2-7 carbon atoms, an aryl group having 6-10 carbon atoms or a carboxyl group; or an aryl group having 6-10 carbon atoms which may be substituted by a halogen atom, an alkoxy group having 1-6 carbon atoms, an aryl group having 6-10 carbon atoms or a carboxyl group.) (2) (In the formula (2), R1, R2, R3, R4, R5 and R6 are as defined above.)

77. 发明公开

EP2404897A1 METHOD FOR PRODUCING HALOGEN-SUBSTITUTED BENZENE DIMETHANOL 审中-公开
标题翻译： VERFAHREN ZUR HERSTELLUNG VON HALOGENSUBSTITUIERTEM BENZENDIMETHANOL
公开(公告)号：EP2404897A1
公开(公告)日：2012-01-11
申请号：EP10748888.4
申请日：2010-03-04
申请人： Sumitomo Chemical Company, Limited
发明人： HAGIYA, Koji , AOYAGI, Yasutaka
IPC分类号： C07C237/42 , C07C29/147 , C07C33/46 , C07C231/08 , C07B61/00
CPC分类号： C07C269/00 , C07C29/147 , C07C231/08 , C07C269/04 , C07C33/46 , C07C271/66 , C07C233/65
摘要： A method for producing a halogen-substituted benzene dimethanol, the method including:
a first step of reacting a compound represented by formula (1) with a compound represented by formula (2) to obtain a dicarboxamide compound represented by formula (3), and
a second step of reducing the dicarboxamide compound using a borohydride compound to obtain a halogen-substituted benzene dimethanol represented by formula (4).
摘要翻译：一种制备卤素取代的苯二甲醇的方法，所述方法包括：使由式（1）表示的化合物与式（2）表示的化合物反应得到由式（3）表示的二羧酰胺化合物的第一步骤，以及使用硼氢化合物还原二羧酰胺化合物以获得由式（4）表示的卤素取代的苯二甲醇的第二步骤。

78. 发明授权

EP2066798B1 PROCESS FOR THE PREPARATION OF 2-HYDROXY CARBOXYLIC ACIDS EMPLOYING BACTERIA OF THE GENUS PSEUDOMONAS, RHODOCOCCUS OR BACILLUS 有权
标题翻译：工艺制备2-羟基羧酸利用细菌假单胞菌属，红球菌或芽孢杆菌属
公开(公告)号：EP2066798B1
公开(公告)日：2010-12-29
申请号：EP07828867.7
申请日：2007-09-21
申请人： Sumitomo Chemical Company, Limited
发明人： ASAKO, Hiroyuki , HAGIYA, Koji
IPC分类号： C12P11/00
CPC分类号： C12P11/00
摘要： There is provided is a process for producing a sulfur-containing α-hydroxycarboxylic acid compound represented by the formula (2): wherein R1 represents hydrogen, C1-8 alkyl, or C6-20 aryl, which comprises subjecting a sulfur-containing ketol represented by the formula (1): wherein R1 is the same as defined above, to the action of microbial cells of a microorganism belonging to the genus Pseudomonas, Rhodococcus or Bacillus capable of converting the ketol into a corresponding α-hydroxycarboxylic acid compound, or a treated material thereof, thereby producing the sulfur-containing α-hydroxycarboxylic acid without using a hydroxynitrile compound as a starting material.

79. 发明授权

EP1748042B1 PROCESS FOR PRODUCING ADIPIC ACID 有权
标题翻译：用于生产ADIPIC
公开(公告)号：EP1748042B1
公开(公告)日：2010-12-29
申请号：EP04733681.3
申请日：2004-05-18
申请人： Sumitomo Chemical Company, Limited
发明人： HIROTA, Masaji , HAGIYA, Koji
IPC分类号： C07C51/285 , C07C55/14 , C07C51/31 , B01J23/30
CPC分类号： C07C51/313 , B01J23/30 , C07C51/487 , C07C55/14
摘要： A process for producing adipic acid, characterized in that a wastewater containing hydroxycaproic acid and discharged from the step of oxidizing cyclohexane with molecular oxygen in a liquid phase is reacted with hydrogen peroxide in the presence of a tungsten catalyst in the pH range of 0 to 6.

80. 发明公开

EP2192087A1 ALKALI METAL FLUORIDE DISPERSION, AND PROCESS FOR PRODUCTION OF FLUORINATED ORGANIC COMPOUND USING THE SAME 审中-公开
标题翻译：碱金属氟化物分散液及其制备方法具有氟化有机结合
公开(公告)号：EP2192087A1
公开(公告)日：2010-06-02
申请号：EP08828723.0
申请日：2008-08-27
申请人： Sumitomo Chemical Company, Limited
发明人： HAGIYA, Koji
IPC分类号： C01D3/02 , C07B39/00 , C07C17/20 , C07C22/08 , C07C51/58 , C07C63/72 , C07C67/14 , C07C69/82 , C07C201/12 , C07C205/11
CPC分类号： C07B39/00 , C01D3/02 , C07C17/208 , C07C51/00 , C07C51/58 , C07C51/60 , C07C67/14 , C07C201/12 , C07C63/30 , C07C69/76 , C07C205/12
摘要： An alkali metal fluoride dispersion essentially consisting of an alkali metal fluoride and an aprotic organic solvent obtainable by conducting the following Step (A), subsequently conducting the following Step (B) at least once, and then conducting the following Step(C);
Step (A) : a step of separating a liquid phase from an alkali metal fluoride dispersion comprising at least one alcohol solvent selected from the group consisting of methanol, ethanol and isopropanol and an alkali metal fluoride, and mixing the separated liquid phase with an aprotic organic solvent having a boiling point of 85°C or higher at normal pressure to obtain a mixture containing the alkali metal fluoride;
Step (B) : a step of obtaining a mixture containing the alkali metal fluoride comprising the following Steps (b1) to (b3);
Step (b1) : a step of concentrating the mixture containing the alkali metal fluoride obtained in Step (A) or Step (b3) to obtain a concentrated fraction and a concentrated residue;
Step (b2) : a step of mixing a residue of the alkali metal fluoride dispersion obtained by separating the liquid phase in Step (A) or a residue of the mixture obtained by separating a liquid phase in Step (b3) with the concentrated fraction obtained in Step (b1) to obtain a mixture containing an alkali metal fluoride; and
Step (b3) : a step of separating a liquid phase from the mixture containing an alkali metal fluoride obtained in Step (b2) and mixing the separated liquid phase with the concentrated residue obtained in Step (b1) to obtain a mixture containing an alkali metal fluoride; and

Step (C) : a step of removing the alcohol solvent fromthemixture containing the alkali metal fluoride, which is obtained in Step (B), to obtain the alkali metal fluoride dispersion essentially consisting of the alkali metal fluoride and the aprotic organic solvent.
摘要翻译：碱金属氟化物分散液实质上通过进行下述工序（A）中，随后进行下面的工序（B）至少一次，然后进行随后的步骤（C）由以下组成的碱金属氟化物和非质子性有机溶剂而得到的A; 步骤（A）：从在碱金属氟化物分散液，其包含至少一种醇中分离出液相的步骤选自甲醇，乙醇和异丙醇以及碱金属氟化物的由......组成选择的溶剂，并且所述分离的液相与在非质子传递混合在常压下的85℃或更高的沸点，得到含有碱金属氟化物的混合物中有机溶剂中; 步骤（B）：得到含有碱金属氟化物，包括以下步骤（b1）至混合物的步骤（B3）; 工序（b1）：含有碱金属氟化物的工序（A）或工序（b3）中得到以获得浓缩馏分和浓缩的残留物浓缩混合物的步骤; 步骤（b2）：获得与浓缩馏分混合通过分离在步骤（A）的液相得到的碱金属氟化物分散液的残基或通过分离在步骤（b3）中的液相中获得的混合物的残基的一个步骤在工序（b1），以获得的碱金属氟化物包含的混合物; 和工序（b3）：分离从含有超过碱金属氟化物在步骤（b2）中得到的混合物的液相，并与在步骤（b1）中得到的浓缩残余物中分离出的液相混合的步骤，得到含有经碱的混合物金属氟化物; 和步骤（C）：除去醇溶剂fromthemixture含有碱金属氟化物，所有这些都在步骤（B）得到的步骤，以获得碱金属氟化物分散液基本上由碱金属氟化物和非质子性有机溶剂。

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