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71. 发明授权

US08273680B2 Process for producing geometric shaped catalyst bodies 有权
标题翻译：用于生产几何形状的催化剂体的方法
公开(公告)号：US08273680B2
公开(公告)日：2012-09-25
申请号：US12557021
申请日：2009-09-10
申请人： Andreas Raichle , Catharina Horstmann , Frank Rosowski , Klaus Joachim Mueller-Engel , Jochen Petzoldt , Ulrich Cremer
发明人： Andreas Raichle , Catharina Horstmann , Frank Rosowski , Klaus Joachim Mueller-Engel , Jochen Petzoldt , Ulrich Cremer
IPC分类号： B01J21/00
CPC分类号： C07C51/252 , B01J23/002 , B01J23/8885 , B01J35/0006 , B01J35/023 , B01J37/0036 , B01J37/0221 , B01J37/34 , B01J2523/00 , C07C45/35 , C07C45/37 , C07C253/26 , Y02P20/52 , C07C47/22 , C07C57/04 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/69 , B01J2523/842 , B01J2523/845 , C07C255/08
摘要： A process for producing geometric shaped catalyst bodies K whose active material is a multielement oxide of stoichiometry [BiaZ1bOx]p[BicMo12FedZ2eZ3fZ4gZ5hZ6iOy]1, in which a finely divided oxide BiaZ1bOx and, formed from element sources, a finely divided mixture of stoichiometry BicMo12FedZ2eZ3fZ4gZ5hZ6i are mixed in a ratio of p:1, this mixture is used to form shaped bodies and these are treated thermally, where 0
摘要翻译：用于生产几何形状的催化剂体K的方法，其活性材料是化学计量的多元素氧化物[BicMo12FedZ2eZ3fZ4gZ5hZ6iOy] 1，其中细分的氧化物BiaZ1bOx和由元素源形成的细分的化学计量比BicMo 12 FedZ 2eZ 3 fZ 4 gZ 5hZ 6i的混合物混合以p：1的比例，将该混合物用于形成成形体，并将它们热处理，其中0

72. 发明授权

US08153825B2 Preparation of phthalic anhydride by gas phase oxidation of o-xylene 有权
标题翻译：通过邻二甲苯的气相氧化制备邻苯二甲酸酐
公开(公告)号：US08153825B2
公开(公告)日：2012-04-10
申请号：US12301352
申请日：2007-05-18
申请人： Thomas Mackewitz , Frank Rosowski , Andreas Tenten
发明人： Thomas Mackewitz , Frank Rosowski , Andreas Tenten
IPC分类号： C07D307/89
CPC分类号： C07D307/89 , C07C51/265 , C07C63/16
摘要： A process is described for preparing phthalic anhydride by catalytic gas phase oxidation of o-xylene, in, in a main reactor, a gaseous mixture of o-xylene and an oxygenous gas is passed through at least two reaction zones whose temperature can be controlled independently, and converted to a gaseous intermediate reaction product which comprises unconverted o-xylene, phthalic anhydride underoxidation products and phthalic anhydride, and the intermediate reaction product is introduced into a postreactor, wherein the temperature of the reaction zones in the main reactor is regulated in such a way that the concentration of unconverted o-xylene in the intermediate reaction product is at least 0.5% by weight. The process allows an increase in the overall yield of phthalic anhydride without or without significant deterioration in the product quality.
摘要翻译：描述了通过邻二甲苯的催化气相氧化制备邻苯二甲酸酐的方法，在主反应器中，邻二甲苯和氧气的气态混合物通过至少两个温度可独立控制的反应区并转化为包含未转化的邻二甲苯，邻苯二甲酸酐未氧化产物和邻苯二甲酸酐的气态中间反应产物，将中间反应产物引入后反应器中，其中主反应器中的反应区的温度如此调节在中间反应产物中未转化的邻二甲苯的浓度为至少0.5重量％的方式。该方法允许邻苯二甲酸酐的总产率提高，而不会产生质量的显着劣化。

73. 发明申请

US20120077998A1 USE OF STRUCTURED CATALYST BEDS FOR PREPARING ETHYLENE OXIDE 有权
标题翻译：用于制备乙烯氧化物的结构化催化剂床的用途
公开(公告)号：US20120077998A1
公开(公告)日：2012-03-29
申请号：US13376879
申请日：2010-06-09
申请人： Georg Seeber , Torsten Mäurer , Gerhard Theis , Dieter Köffer , Frank Rosowski
发明人： Georg Seeber , Torsten Mäurer , Gerhard Theis , Dieter Köffer , Frank Rosowski
IPC分类号： C07D301/10
CPC分类号： C07D301/10
摘要： The present invention relates to a process for preparing ethylene oxide by reaction of ethylene with oxygen in the presence of at least one silver-comprising catalyst, wherein the reaction takes place in a reactor which has a catalyst packed bed having at least two zones (i) and (ii) and the silver content of the catalyst in zone (i) is lower than the silver content of the catalyst in zone (ii). The catalyst packed bed preferably has a further zone (a) with which the reaction mixture comes into contact before the zones (i) and (ii). According to the invention, the silver content of the catalyst in the zone (a) is higher than the silver content of the catalyst in zone (i).
摘要翻译：本发明涉及通过乙烯与氧在至少一种含银催化剂存在下反应来制备环氧乙烷的方法，其中该反应在具有至少两个区域的催化剂填充床（i ）和（ii），并且（i）区域中的催化剂的银含量低于区域（ii）中的催化剂的银含量。催化剂填充床优选具有另外的区域（a），反应混合物在区域（i）和（ii）之前与其接触。根据本发明，区域（a）中催化剂的银含量高于区域（i）中催化剂的银含量。

74. 发明申请

US20110250124A1 CATALYST FOR THE OXIDATION OF SO2 TO SO3 有权
标题翻译： SO2氧化SO3的催化剂
公开(公告)号：US20110250124A1
公开(公告)日：2011-10-13
申请号：US13084934
申请日：2011-04-12
申请人： Michael Kramer , Markus Schubert , Thomas Lautensack , Thomas Hill , Reinhard Korner , Frank Rosowski , Jurgen Zuhlke
发明人： Michael Kramer , Markus Schubert , Thomas Lautensack , Thomas Hill , Reinhard Korner , Frank Rosowski , Jurgen Zuhlke
IPC分类号： C01B17/79 , B01J37/04 , B01J37/02 , B01J27/055
CPC分类号： B01J27/055 , B01J21/08 , B01J23/22 , B01J35/023 , B01J37/0018 , B01J37/0201 , C01B17/79
摘要： The invention relates to a catalyst for the oxidation of SO2 to SO3 and also a process for producing it and its use in a process for the oxidation of SO2 to SO3.
摘要翻译：本发明涉及一种用于将SO2氧化成SO 3的催化剂，还涉及其生产方法及其在SO2氧化成SO 3的方法中的应用。

75. 发明授权

US07985705B2 Three-layered, four-layered, or five-layered catalyst systems for producing phthalic anhydride 有权
标题翻译：用于生产邻苯二甲酸酐的三层，四层或五层催化剂体系
公开(公告)号：US07985705B2
公开(公告)日：2011-07-26
申请号：US12708181
申请日：2010-02-18
申请人： Sebastian Storck , Jürgen Zühlke , Samuel Neto , Frank Rosowski
发明人： Sebastian Storck , Jürgen Zühlke , Samuel Neto , Frank Rosowski
IPC分类号： B01J31/36 , C07D307/89
CPC分类号： C07C51/313 , B01J23/002 , B01J23/22 , B01J27/198 , B01J35/0006 , B01J35/10 , B01J35/1009 , B01J35/1014 , B01J2523/00 , C07C51/265 , C07C63/16 , B01J2523/15 , B01J2523/47 , B01J2523/53 , B01J2523/55 , B01J2523/51
摘要： Catalyst systems for preparing phthalic anhydride by means of gas-phase oxidation of o-xylene and/or naphthalene, and a process for preparing phthalic anhydride using the catalyst systems.
摘要翻译：通过邻二甲苯和/或萘的气相氧化制备邻苯二甲酸酐的催化剂体系，以及使用催化剂体系制备邻苯二甲酸酐的方法。

76. 发明申请

US20100210857A1 Three-Layered or Four-Layered Catalyst Systems for Producing Phthalic Anhydride 有权
标题翻译：用于生产邻苯二甲酸酐的三层或四层催化剂体系
公开(公告)号：US20100210857A1
公开(公告)日：2010-08-19
申请号：US12708181
申请日：2010-02-18
申请人： Sebastian Storck , Jürgen Zühlke , Samuel Neto , Frank Rosowski
发明人： Sebastian Storck , Jürgen Zühlke , Samuel Neto , Frank Rosowski
IPC分类号： C07D307/89
CPC分类号： C07C51/313 , B01J23/002 , B01J23/22 , B01J27/198 , B01J35/0006 , B01J35/10 , B01J35/1009 , B01J35/1014 , B01J2523/00 , C07C51/265 , C07C63/16 , B01J2523/15 , B01J2523/47 , B01J2523/53 , B01J2523/55 , B01J2523/51
摘要： Catalyst systems for preparing phthalic anhydride by means of gas-phase oxidation of o-xylene and/or naphthalene, and a process for preparing phthalic anhydride using the catalyst systems
摘要翻译：通过邻二甲苯和/或萘的气相氧化制备邻苯二甲酸酐的催化剂体系，以及使用催化剂体系制备邻苯二甲酸酐的方法

77. 发明申请

US20080312450A1 Method for Start-Up of Oxidation Catalysts 审中-公开
标题翻译：氧化催化剂启动方法
公开(公告)号：US20080312450A1
公开(公告)日：2008-12-18
申请号：US11994516
申请日：2006-06-30
申请人： Samuel Neto , Frank Rosowski , Sebastian Storck , Juergen Zuehlke , Hans-Martin Allmann , Thomas Lautensack , Rainer Steeg
发明人： Samuel Neto , Frank Rosowski , Sebastian Storck , Juergen Zuehlke , Hans-Martin Allmann , Thomas Lautensack , Rainer Steeg
IPC分类号： C07D213/79 , C07C27/10 , C07D307/60 , C07D307/89 , C07C51/16
CPC分类号： C07D307/34 , B01J23/002 , B01J2523/00 , C07C51/265 , C07C51/313 , C07C63/16 , B01J2523/15 , B01J2523/47 , B01J2523/53 , B01J2523/55 , B01J2523/824
摘要： Methods comprising: providing an oxidation catalyst bed; and starting up the oxidation catalyst at a temperature of 360° C. to 400° C. with an amount of air of 1.0 to 3.5 standard m3/h and a hydrocarbon loading of 20 to 65 g/standard m3, such that a hot spot having a temperature of 390° C. to
摘要翻译：方法包括：提供氧化催化剂床; 并在360℃至400℃的温度下启动氧化催化剂，空气量为1.0-3.5标准立方米/小时，烃装载量为20至65克/标准立方米，使得热点在催化剂床的前7-20％中形成温度为390℃至<450℃的温度。

78. 发明申请

US20080214863A1 PROCESS FOR PREPARING A CATALYST CONSISTING OF A SUPPORT BODY AND A CATALYTICALLY ACTIVE COMPOSITION APPLIED ON THE SURFACE OF THE SUPPORT BODY 有权
标题翻译：制备支持体的催化剂的方法和应用于支持体的表面的催化活性组合物
公开(公告)号：US20080214863A1
公开(公告)日：2008-09-04
申请号：US12039231
申请日：2008-02-28
申请人： Ulrich CREMER , Andreas Raichle , Frank Rosowski , Ulrich Hammon , Klaus Joachim Mueller-Engel
发明人： Ulrich CREMER , Andreas Raichle , Frank Rosowski , Ulrich Hammon , Klaus Joachim Mueller-Engel
IPC分类号： C07C51/235 , B01J23/22 , B01J23/28
CPC分类号： B01J23/002 , B01J23/28 , B01J23/8885 , B01J37/0219 , B01J37/0221 , B01J2523/00 , C07C51/252 , C07C57/04 , B01J2523/17 , B01J2523/55 , B01J2523/68 , B01J2523/69
摘要： A process for preparing a coated catalyst in which a finely divided mixture of a multielement oxide comprising the elements Mo and V and a molybdenum oxide or a molybdenum oxide former is applied to the surface of a support body as an active composition.
摘要翻译：一种制备涂覆催化剂的方法，其中将包含元素Mo和V的多元素氧化物和氧化钼或氧化钼形成剂的细碎混合物施加到作为活性组合物的载体的表面。

79. 发明申请

US20080146846A1 Direct Amination of Hydrocarbons 审中-公开
标题翻译：碳氢化合物的直接胺化
公开(公告)号：US20080146846A1
公开(公告)日：2008-06-19
申请号：US11722774
申请日：2005-12-20
申请人： Harald Dialer , Matthias Frauenkron , Holger Evers , Ekkehard Schwab , Johann-Peter Melder , Frank Rosowski , Frederik Van Laar , Joachim-Thierry Anders , Sven Crone , Wolfgang Mackenroth
发明人： Harald Dialer , Matthias Frauenkron , Holger Evers , Ekkehard Schwab , Johann-Peter Melder , Frank Rosowski , Frederik Van Laar , Joachim-Thierry Anders , Sven Crone , Wolfgang Mackenroth
IPC分类号： C07C209/02
CPC分类号： C07C209/02 , B01J23/755 , B01J23/76 , B01J23/885 , B01J23/8892 , B01J23/8933 , B01J23/94 , B01J27/24 , B01J27/28 , B01J37/03 , B01J37/04 , B01J38/08 , B01J38/18 , Y02P20/584 , C07C211/46
摘要： The invention relates to a process for preparing nitrogen-containing catalysts, comprising: a) preparation of an oxidic species comprising the following components: at least one metal M selected from groups Ib to VIIb and VIII of the Periodic Table of the Elements, it being possible for the same metal to be present in different oxidation states; if appropriate one or more promoters P selected from groups Ib to VIIb and VIII of the Periodic Table of the Elements, the lanthanides, and from groups IIIa to VIa of the Periodic Table of the Elements, excluding oxygen and sulfur; if appropriate one or more elements R selected from hydrogen, alkali metals and alkaline earth metals; if appropriate one or more elements Q selected from chloride and sulfate; oxygen, the molar proportion of oxygen being determined by the valency and frequency of the elements in the oxidic species other than other oxygen; b) reaction of the oxidic species with an amine component selected from ammonia, primary and secondary amines and ammonium salts, the nitrogen-containing catalyst being formed with the formation of water, and to nitrogen-containing catalysts preparable by this process. The invention further relates to a process for aminating hydrocarbons using the inventive nitrogen-containing catalyst and to the use of an oxidic species in a process for the direct amination of hydrocarbons.
摘要翻译：本发明涉及一种制备含氮催化剂的方法，包括：a）制备包含以下组分的氧化物质：至少一种选自元素周期表Ib至VIIb和VIII族的金属M，它是可能使相同的金属以不同的氧化态存在; 如果合适的话，可以选择元素周期表Ib-VIIb和VIII族中的一种或多种助催化剂P，元素周期表IIIa至VIa族，不包括氧和硫; 如果合适，则选自氢，碱金属和碱土金属的一种或多种元素R; 如果适当，选自氯化物和硫酸盐的一种或多种元素Q; 氧，氧的摩尔比例由氧化物中除了其它氧以外的元素的化合价和频率决定; b）氧化物质与选自氨，伯胺和仲胺和铵盐的胺组分的反应，形成水的含氮催化剂，以及可通过该方法制备的含氮催化剂。本发明还涉及使用本发明的含氮催化剂胺化烃的方法以及在直接胺化烃的方法中使用氧化物质的方法。

80. 发明申请

US20070135302A1 Mehtod for the production of a catalyst for gas-phase oxidations by the coating of support materials in a fluid bed apparatus 审中-公开
标题翻译： Mehtod用于通过在流化床装置中涂覆支撑材料来生产用于气相氧化的催化剂
公开(公告)号：US20070135302A1
公开(公告)日：2007-06-14
申请号：US10573480
申请日：2004-09-24
申请人： Samuel Neto , Wolfgang Rummel , Sebastien Storck , Jurgen Zuhlke , Frank Rosowski
发明人： Samuel Neto , Wolfgang Rummel , Sebastien Storck , Jurgen Zuhlke , Frank Rosowski
IPC分类号： B01J23/00
CPC分类号： B01J2/16 , B01J2/006 , B01J23/22 , B01J35/0006 , B01J35/002 , B01J35/1014 , B01J37/0009 , B01J37/0221 , B01J37/0232 , B01J37/0244
摘要： The invention relates to a process for producing a catalyst for gas-phase oxidations, which comprises weighing a particulate inert support having a total mass of Msupport into a fluidized-bed apparatus, providing an aqueous suspension of a catalytically active material or sources therefor and a binder having a binder content of Bsusp, fluidizing the inert support by introduction of a gas stream heated to a temperature of Tgas at a flow rate of Qgas, and spraying the suspension at a rate of Qsusp onto the fluidized inert support. When Qgas, Qsusp, Bsusp, Msupport and Tgas are selected within the ranges 3000≦Qgas [m3/h]≦9000, 1000≦Qsusp [g/min]≦3500, 2≦Bsusp [% by weight]≦18, 60≦Msupport [kg]≦240. 75≦Tgas [° C.]≦120 so that a parameter K defined as K=0.020 Qgas−0.055 Qsusp+7.500 Bsusp−0.667 Msupport+2.069 Tgas−7satisfies the relationship 127.5≦K≦202, high-quality coatings can be produced and the formation of twins made up of support particles adhering to one another can be avoided.
摘要翻译：本发明涉及一种用于生产气相氧化催化剂的方法，该方法包括将具有总质量的载体的颗粒惰性载体称重到流化床装置中，提供水悬浮液催化活性材料或其来源以及具有粘合剂含量为B susp susp susp susp susp a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a Q气体的流速，并以悬浮液的速度将悬浮液喷雾到流化的惰性载体上。当气体气体时，Q 1，B 2，B 3，M 3，N 2，在3000以下范围内选择气体[m 3 / h] <= 9000,1000 <= Q [g / min ] <= 3500，2 <= B [重量％] <= 18,60 <= M [kg] = 240。 75 <= T [°C] <= 120，使得定义为<？in-line-formula description =“In-Line Formulas”end =“lead”？> K = 0.020 Q气体-0.055 Q + +7.500 B＆lt;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp; 气体-7 <？在线公式描述=“在线公式”end =“tail”？>满足关系127.5 <= K <= 202，可以生产高品质涂层并形成可以避免由彼此粘附的支撑颗粒构成的双胞胎。

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