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71. 发明授权

US4699916A Substituted furazan pesticides 失效
标题翻译：取代呋咱农药
公开(公告)号：US4699916A
公开(公告)日：1987-10-13
申请号：US820508
申请日：1986-01-21
申请人： Wilhelm Sirrenberg , Erich Klauke , Gerhard Zoebelein , Benedikt Becker , Wilhelm Stendel
发明人： Wilhelm Sirrenberg , Erich Klauke , Gerhard Zoebelein , Benedikt Becker , Wilhelm Stendel
IPC分类号： A01N47/36 , C07D271/08 , C07D319/00 , C07D413/12 , C07D521/00 , H05B6/64
CPC分类号： C07D521/00 , A01N47/36 , C07D271/08 , C07D413/12 , H05B6/6408
摘要： Substituted furazans of the formula ##STR1## in which R and R.sup.1 are identical or different and represent optionally substituted aromatic or heteroaromatic radicals,R.sup.2 represents hydrogen, an OH or COOH grouping or an optionally substituted radical from the series comprising alkyl, alkoxy, cycloalkyl, cycloalkenyl, alkoxycarbonyl, alkoxythiocarbonyl, alkylsulphonyl, arylsulphonyl and aralkyl,Y represents oxygen or an S(O).sub.m, --CR.sup.3 R.sup.4, CO or NR.sup.5 grouping,in whichm represents the number 0, 1 or 2 andR.sup.3, R.sup.4 and R.sup.5 are identical or different and represent hydrogen or alkyl,n represents the number 0 or 1 andX represents oxygen or sulphur,and wherein, ifR represents phenyl,R.sup.1 represents phenyl,R.sup.2 represents hydrogen andX represents oxygen or sulphur,thenn represents the number 1,or ifn represents the number 0,R represents 4-bromophenyl,R.sup.1 represents 4-chlorophenyl andR.sup.2 represents hydrogen,thenX represents sulphur,which possess pesticidal activity.
摘要翻译： R 1和R 1相同或不同且代表任意取代的芳族或杂芳族基团的取代呋喃酮，其中R 1表示氢，OH或COOH基团或任选取代的包含烷基，烷氧基，环烷基，环烷基，烷氧基羰基，烷氧基硫代羰基，烷基磺酰基，芳基磺酰基和芳烷基，Y代表氧或S（O）m，-CR3R4，CO或NR5基团，其中m代表数字0,1或2，且R3，R4和R5相同或不同，表示氢或烷基，n表示数字0或1，X表示氧或硫，并且其中，如果R表示苯基，则R1表示苯基，R2表示氢，X表示氧或硫，则n表示数字1 ，或者如果n表示数字0，则R表示4-溴苯基，R 1表示4-氯苯基，R 2表示氢，则X表示具有杀虫活性的硫。

72. 发明授权

US4665217A (Meth)-acrylic acid esters and their use 失效
标题翻译：（甲基）丙烯酸酯及其用途
公开(公告)号：US4665217A
公开(公告)日：1987-05-12
申请号：US852600
申请日：1986-04-16
申请人： Jurgen Reiners , Jens Winkel , Erich Klauke , Carlhans Suling , Wolfgang Podszun
发明人： Jurgen Reiners , Jens Winkel , Erich Klauke , Carlhans Suling , Wolfgang Podszun
IPC分类号： C08F20/00 , A61K6/083 , A61K6/09 , C07C67/00 , C07C69/54 , C07C239/00 , C07C271/16 , C08F20/10 , C08F20/30 , C08F20/34 , C08F20/36 , C07C125/06 , C07C69/52
CPC分类号： A61K6/083 , A61K6/0017 , A61K6/0023 , A61K6/09 , C08F20/30
摘要： (Meth)-acrylic acid esters of the formula ##STR1## in which R.sup.1 and R.sup.2 are identical or different and denote hydrogen, chlorine, fluorine or a C.sub.1 - to C.sub.4 -alkyl radical andR.sup.3 and R.sup.4 are identical or different and represent the group ##STR2## wherein R.sup.5 and R.sup.6 are identical or different and denote hydrogen or methyl,Z denotes a straight-chain or branched C.sub.2 - to C.sub.8 -alkylene chain andn denotes values from 1 to 4. Such (meth)-acrylic acid esters can be used as dental fillers or to coat teeth.
摘要翻译：（甲基）丙烯酸酯，其中R 1和R 2相同或不同，表示氢，氯，氟或C 1〜C 4 - 烷基，R 3和R 4相同或不同，表示基团其中R 5和R 6相同或不同，表示氢或甲基，Z表示直链或支链的C 2 -C 8 - 亚烷基链，n表示1至4的数值。这种（甲基）丙烯酸酯可以用作牙齿填料或涂抹牙齿。

73. 发明授权

US4588837A Process for the preparation of fluorocarboxylic acids 失效
标题翻译：氟代羧酸的制备方法
公开(公告)号：US4588837A
公开(公告)日：1986-05-13
申请号：US632135
申请日：1984-07-18
申请人： Bernd Baasner , Erich Klauke , Reinhard Lantzsch
发明人： Bernd Baasner , Erich Klauke , Reinhard Lantzsch
IPC分类号： C07C53/15 , C07C51/00 , C07C51/097 , C07C67/00 , C07C53/18
CPC分类号： C07C51/097
摘要： Fluorocarboxylic acids are prepared by metering fluoronitroaliphatic compounds into a mineral acid which has been initially introduced.
摘要翻译：氟代羧酸是通过将氟代芳族脂肪族化合物计量为最初引入的无机酸来制备的。

74. 发明授权

US4564478A Fluorinated thiocarbonic acid ester-fluorides 失效
标题翻译：氟化硫代碳酸酯 - 氟化物
公开(公告)号：US4564478A
公开(公告)日：1986-01-14
申请号：US670693
申请日：1984-11-13
申请人： Erich Klauke , Engelbert Kuhle
发明人： Erich Klauke , Engelbert Kuhle
IPC分类号： C07C323/52 , A01N37/02 , C07C67/00 , C07C313/00 , C07C325/00 , C07C327/00 , C07C329/00 , C07C329/02 , C07C333/02 , C07C153/017 , C07C148/00 , C07C153/023
CPC分类号： C07C329/00 , C07C323/00
摘要： Novel fluorinated thiocarbonic acid ester-fluorides of the formula ##STR1## in which R.sup.1 represents alkyl, cycloalkyl or optionally substituted aryl andR.sup.2 and R.sup.3 independently of one another represent hydrogen or alkyl, orR.sup.1 and R.sup.2 together represent an alkylene chain,a new process for the preparation of the new compounds and their use as intermediates for the preparation of compounds having herbicidal properties.Novel intermediates of the formulae ##STR2## in which R.sup.2 and R.sup.3 have the above-mentioned meaning,R.sup.4 is optionally substituted aryl,R.sup.5 is alkyl or cycloalkyl, andX is fluorine or chlorine, at least one X representing chlorine.
摘要翻译：式（I）的新型氟代硫代碳酸酯 - 氟化物，其中R 1表示烷基，环烷基或任选取代的芳基，R 2和R 3彼此独立地表示氢或烷基，或者R 1和R 2一起表示亚烷基链，用于制备新化合物的新方法及其作为制备具有除草性的化合物的中间体的用途。其中R 2和R 3具有上述含义的式“IMAGE”的新型中间体，R 4是任选取代的芳基，R 5是烷基或环烷基，X是氟或氯，至少一个X代表氯。

75. 发明授权

US4533676A 2,5-Dihalogenobenzoyl-(thio)urea insecticides 失效
标题翻译： 2,5-二卤代苯甲酰 - （硫）脲类杀虫剂
公开(公告)号：US4533676A
公开(公告)日：1985-08-06
申请号：US487799
申请日：1983-04-22
申请人： Wilhelm Sirrenberg , Erich Klauke , Ingeborg Hammann
发明人： Wilhelm Sirrenberg , Erich Klauke , Ingeborg Hammann
IPC分类号： A01N47/34 , C07C67/00 , C07C275/54 , C07C309/66 , C07C313/00 , C07C317/42 , C07C323/19 , C07C323/20 , C07C323/44 , C07C325/00 , C07C335/26 , C07D317/46 , C07D319/08 , C07D319/20 , C07C127/22
CPC分类号： C07D319/08 , A01N47/34 , C07C275/54 , C07C309/66 , C07C317/42 , C07C323/19 , C07C323/20 , C07C323/44 , C07D317/46 , C07D319/20
摘要： A 2,5-dihalogenobenzoyl-(thio)urea of the formula ##STR1## in which X represents sulphur or oxygen,X.sup.1 and X.sup.2 are identical or different and represent fluorine, chlorine, bromine or iodine,R.sup.1 represents hydrogen, halogen, or optionally substituted radicals from the series comprising alkyl, alkoxy and alkylthio,R.sup.2 represents hydrogen, halogen, cyano, nitro or optionally substituted radicals from the series comprising alkyl, alkylthio, alkylsulphonyl, alkoxy, aryloxy, alkylcarbonyl, alkoxycarbonyl, alkoxycarbonylalkyl and alkoxycarbonylalkylthio,R.sup.1 and R.sup.2 together represent an optionally substituted alkylenedioxy radical or represent --CF.sub.2 --O--CF.sub.2 --O--,R.sup.3 represents hydrogen, halogen, or an optionally substituted alkyl, alkoxy or aryloxy radical, andR.sup.4 represents hydrogen, halogen, or optionally substituted radicals from the series comprising alkyl, alkylthio and alkoxy, with the exception of those cases in which X represents oxygen, X.sup.1 and X.sup.2 represent chlorine and (a) R.sup.1 represents chlorine, R.sup.2 represents OCF.sub.2 CHFCL and R.sup.3 and R.sup.4 represent hydrogen, or (b) R.sup.1 represents chlorine, R.sup.2 represents OCF.sub.3 and R.sup.3 and R.sup.4 represent hydrogen, or (c) R.sup.2 represents OCF.sub.3 and R.sup.1, R.sup.3 and R.sup.4 represent hydrogen, which possesses insecticidal activity.
摘要翻译：其中X表示硫或氧，X1和X2的式“IMAGE”的2,5-二卤代苯甲酰基（硫代）脲相同或不同，表示氟，氯，溴或碘，R1表示氢，卤素或任选地取代基包括烷基，烷氧基和烷硫基，R2代表氢，卤素，氰基，硝基或任选取代的基团，其中包括烷基，烷硫基，烷基磺酰基，烷氧基，芳氧基，烷基羰基，烷氧基羰基，烷氧基羰基烷基和烷氧羰基烷硫基，R1和R2 一起代表任选取代的亚烷基二氧基或代表-CF2-O-CF2-O-，R3代表氢，卤素或任选取代的烷基，烷氧基或芳氧基，R4代表氢，卤素或任选取代的基团包括烷基，烷硫基和烷氧基，除了其中X表示氧，X1和X2表示氯的那些情况，（a）R1代表氯 R表示OCF2CHFCL，R3和R4表示氢，或（b）R1表示氯，R2表示OCF3，R3和R4表示氢，或（c）R2表示OCF3，R1，R3和R4表示氢，具有杀虫活性。

76. 发明授权

US4513003A Process for protecting wood using N-(dichlorofluoromethylthio)-3,6-endomethylene-.DELTA..sup.4 -tetrahydrophthalimide 失效
标题翻译：使用N-（二氯氟甲硫基）-3,6-三亚甲基-DTA4-四氢邻苯二甲酰亚胺保护木材的方法
公开(公告)号：US4513003A
公开(公告)日：1985-04-23
申请号：US399632
申请日：1982-07-19
申请人： Engelbert Kuhle , Erich Klauke , Wilfried Paulus , Hermann Genth
发明人： Engelbert Kuhle , Erich Klauke , Wilfried Paulus , Hermann Genth
IPC分类号： A01N47/04 , C07D209/76 , C07D209/48 , A61K31/40
CPC分类号： C07D209/76 , A01N47/04
摘要： The novel N-(dichlorofluoromethylthio)-3,6-endomethylene-.DELTA..sup.4 -tetrahydrophthalimides can be prepared from 3,6-endomethylene-.DELTA..sup.4 -tetrahydrophthalimide with dichlorofluoromethanesulphenyl chloride in the presence of an acid-binding agent in solution. They can be used as microbicidal agents.
摘要翻译：新型N-（二氯氟甲硫基）-3,6-三亚甲基-DTA4-四氢邻苯二酰亚胺可以在溶液中存在酸结合剂的情况下由3,6-己亚甲基-DTA4-四氢邻苯二甲酰亚胺与二氯氟甲磺酰氯制备。它们可以用作杀菌剂。

77. 发明授权

US4348323A Intermediates and derivatives thereof 失效
标题翻译：中间体及其衍生物
公开(公告)号：US4348323A
公开(公告)日：1982-09-07
申请号：US226289
申请日：1981-01-19
申请人： Rainer Fuchs , Erich Klauke , Ingeborg Hammann , Bernhard Homeyer , Wolfgang Behrenz , Wilhelm St-Noel , Reinhard Lantzsch , Albrecht Harhold
发明人： Rainer Fuchs , Erich Klauke , Ingeborg Hammann , Bernhard Homeyer , Wolfgang Behrenz , Wilhelm St-Noel , Reinhard Lantzsch , Albrecht Harhold
IPC分类号： A01N37/00 , A01N37/10 , A01N37/38 , A01N43/24 , A01N43/30 , A01N43/32 , A01N47/02 , A01N53/00 , C07C59/64 , C07C69/612 , C07C255/53 , C07D317/46 , C07D319/20
CPC分类号： C07C255/00 , A01N37/10 , A01N37/38 , A01N43/30 , A01N43/32 , A01N47/02 , A01N53/00 , C07C323/00 , C07C59/64 , C07D317/46 , C07D319/20
摘要： Fluorine-containing phenylacetic acid esters of the formula ##STR1## in which R represents the radical of an alcohol customary in the case of pyrethroids,R.sup.1 represents C.sub.2-4 -alkyl, C.sub.2-4 -alkenyl or cyclopropyl,X represents H, halogen, alkyl, alkoxy, OCHF.sub.2, SCHF.sub.2, SCClF.sub.2 or SCF.sub.3 andX.sup.1 can vary widely or form a fused ring with X, the overall compound necessarily containing a fluorine atom, which compounds possess arthropodicidal properties. Intermediates therefor and an overall synthesis from an alcohol of the formula ROH and a toluene of the formula ##STR2## are also shown.
摘要翻译：式（I）的含氟苯乙酸酯其中R表示在拟除虫菊酯类中常用的醇的基团，R 1表示C 2-4烷基，C 2-4链烯基或环丙基，X表示H ，卤素，烷基，烷氧基，OCHF 2，SCHF 2，SCClF 2或SCF 3和X 1可以广泛变化或与X形成稠环，所述化合物必须含有氟原子，该化合物具有节肢动物学特性。还示出了其中间体和来自式ROH的醇和式“IMAGE”的甲苯的总体合成。

78. 发明授权

US4330366A Process for the preparation of halogenated benzoyl fluorides 失效
标题翻译：制备卤代苯甲酰氟的方法
公开(公告)号：US4330366A
公开(公告)日：1982-05-18
申请号：US170448
申请日：1980-07-21
申请人： Albrecht Marhold , Erich Klauke
发明人： Albrecht Marhold , Erich Klauke
IPC分类号： C07C63/70 , C07C29/147 , C07C51/00 , C07C51/58 , C07C67/00
CPC分类号： C07C51/58 , C07C29/147
摘要： A process for the preparation of a halogenated benzoyl fluoride, which comprises contacting a halogenated benzotrifluoride of the formula ##STR1## in which m and n independently of one another represent an integer from 0 to 5, the sum of m and n being 5, with at least one sulphur compound of the formula ##STR2## in which X denotes fluorine, chlorine or hydroxyl andY represents hydroxyl, orX and Y together denote an oxygen atom linked to the sulphur atom by a double bond,at an elevated temperature, and after reaction with the halogenated benzotrifluoride, removing the sulphur compound from the reaction mixture in the form of a compound of the formula ##STR3## in which X has the meaning given andHal represents fluorine or chlorine, the reaction product is further reacted with potassium fluoride at an elevated temperature and under increased pressure.
摘要翻译：一种制备卤代苯甲酰氟的方法，其包括使式（I）的卤化苯并三氟化物与其中m和n彼此独立地表示0至5的整数，m和n的和为5，与至少一种式“IMAGE”的硫化合物，其中X表示氟，氯或羟基，Y表示羟基，或X和Y一起表示在高温下与硫原子连接的氧原子，以及在与卤化的三氟甲苯反应后，从反应混合物中除去硫化合物，其形式为：其中X具有给定的含义，Hal表示氟或氯，反应产物进一步与氟化钾反应在升高的温度和增加的压力下。

79. 发明授权

US4322442A Combating fungi with 1-halo-1-propyn-3-ols 失效
标题翻译：抗真菌与1-卤代-1-丙炔-3-醇
公开(公告)号：US4322442A
公开(公告)日：1982-03-30
申请号：US184694
申请日：1980-09-08
申请人： Gerhard Jager , Erich Klauke , Wilhelm Brandes , Paul-Ernst Frohberger
发明人： Gerhard Jager , Erich Klauke , Wilhelm Brandes , Paul-Ernst Frohberger
IPC分类号： A01N31/02 , A01N31/04 , A01N31/14 , A01N33/20 , A01N43/06 , A01N43/40 , A01N43/56 , C07C27/00 , C07C29/62 , C07C33/48 , C07C41/30 , C07C43/295 , C07C67/00 , C07C201/00 , C07C205/19 , C07C213/00 , C07C215/68 , C07C253/00 , C07C255/53 , C07C313/00 , C07C323/19 , C07D213/30 , C07D231/10 , C07D231/12 , C07D307/42 , C07D333/16
CPC分类号： C07D213/30 , A01N31/04 , A01N31/14 , A01N33/20 , A01N43/06 , A01N43/40 , A01N43/56 , C07C205/26 , C07C29/62 , C07C33/486 , C07C41/30 , C07C43/23 , C07C43/295 , C07D231/12 , C07D307/42 , C07D333/16
摘要： 1-Halo-1-propyn-3-ols of the formula ##STR1## in which R is optionally substituted phenyl, pyridyl, furyl, thienyl or pyrazolyl,R' is optionally substituted phenyl, andX is halogen,which possess fungicidal properties.
摘要翻译：其中R为任选取代的苯基，吡啶基，呋喃基，噻吩基或吡唑基，R'为任选取代的苯基，X为卤素，具有杀真菌性质。

80. 发明授权

US4322237A Preserving cut flowers with N-(trifluoromethyl)-N-(dichlorofluoromethylsulphenyl)-aminobenzoic acids 失效
标题翻译：用N-（三氟甲基）-N-（二氯氟甲基亚磺酰基） - 氨基苯甲酸保存切花
公开(公告)号：US4322237A
公开(公告)日：1982-03-30
申请号：US185829
申请日：1980-09-10
申请人： Johannes Niggemann , Engelbert Kuhle , Erich Klauke
发明人： Johannes Niggemann , Engelbert Kuhle , Erich Klauke
IPC分类号： A01N3/00 , A01N3/02
CPC分类号： A01N3/00 , A01N3/02
摘要： A method of preserving cut flowers and other parts of plants which have been cut off, comprising placing the flowers or parts of plants in water containing an N-(trifluoromethyl)-N-(dichlorofluoromethylsulphenyl)-aminobenzoic acid, or salt thereof, of the formula ##STR1## in which M is hydrogen or 1 equivalent of an alkali metal atom or of an alkaline earth metal atom, andR is hydrogen, methyl, methoxy, trifluoro-methyl, chlorine or nitro.The active material can be employed in the form of a composition also containing water, a carbohydrate and a salt of magnesium, boron or aluminum. It can be held as a dry concentrate on a carrier such as kieselguhr, a natural or synthetic zeolite or alumina.
摘要翻译：一种保存切割的切花和植物的其他部分的方法，包括将植物的花或部分置于含有N-（三氟甲基）-N-（二氯氟甲基磺酰基） - 氨基苯甲酸或其盐的水中式中，M为氢或1当量碱金属原子或碱土金属原子，R为氢，甲基，甲氧基，三氟甲基，氯或硝基。活性物质可以以还含有水，碳水化合物和镁，硼或铝的盐的组合物的形式使用。它可以作为干燥浓缩物保持在诸如硅藻土，天然或合成沸石或氧化铝的载体上。

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