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    • 75. 发明专利
    • PRODUCTION OF VAPOR DEPOSITION MATERIAL
    • JPH0428858A
    • 1992-01-31
    • JP13256990
    • 1990-05-24
    • MITSUBISHI HEAVY IND LTD
    • TAGUCHI TOSHIOKOBAYASHI TOSHIROHANANAKA KATSUYASUKAMIKAWA SUSUMU
    • C23C14/24
    • PURPOSE:To produce a vapor deposition material capable of efficiently vapor- depositing a thin SiO film with superior quality at a low cost by mixing SiO2 and Si, compacting the resulting mixture, and sintering the resulting green compact in an N2 atmosphere. CONSTITUTION:An SiO2 powder and an Si powder are mixed. As to the mixing ratio, about 30-70% SiO2 and about 70-30% Si by mole ratio are desirable. At this time, it is preferable that, as to the above SiO2, grains of about 0.1mum diameter comprise about 30% of the mixture. After the above powder mixture is compacted, the resulting green compact is sintered in an N2 atmosphere. As to this N2 atmosphere, that of 1-5atms by partial pressure of N2 is suitably used. Further, preferred sintering temp. is 1200-1400 deg.C. By the above sintering, a nitride is formed on the surface of active Si in the compact and the oxidation of Si in the air can be prevented. Nitrogen in this nitride can easily be removed by means of heating in vacuum at the time of vapor deposition. By this method, the inexpensive vapor deposition material capable of vapor-depositing a thin SiO or SiO-like film with superior quality at an evaporation velocity equal to that of SiO as simple substance can be obtained.
    • 76. 发明专利
    • ROTOR
    • JPH045401A
    • 1992-01-09
    • JP10639690
    • 1990-04-24
    • MITSUBISHI HEAVY IND LTD
    • FUKAYA YASUHIROMATSUMOTO TAKAHIROKOBAYASHI TOSHIROOSAWA HARUSHIGE
    • F01D5/06
    • PURPOSE:To obtain a rotor with high function strength indestructible during its high speed rotation by creating, in a concentrically circular form, annular void sections on the inside perimetrical surface sides of adjacent contact planes of plural disks. CONSTITUTION:A rotation axis 1a and disks 1b1, 1c1 and 1d1 are put together on the same line by engaging a protruding engagement section 3 arranged in the center of both the disk 1c1 and the rotation axis 1a with a fellow recess engagement section. Since a rotor 1 forms a spigot joint and there are also differences in disk structures, their shearing stresses are concentrated on the inside perimetrical surface sides of adjacent contact planes of disks. Accordingly, the shearing stress is diminished by creating, in a concentrically circular form, annular void sections 4 on the inside perimetrical surface sides of adjacent contact planes of respective disks. In this way, a junction strength can be enhanced and a rotor indestructible during it high speed can be obtained.
    • 77. 发明专利
    • VACUUM VAPOR DEPOSITION METHOD OF AL
    • JPH03153862A
    • 1991-07-01
    • JP29001789
    • 1989-11-09
    • MITSUBISHI HEAVY IND LTD
    • YOSHIDA YASUYUKIKOBAYASHI TOSHIRONAKAGAWA YOSHIKIYOHANANAKA KATSUYASU
    • C23C14/14
    • PURPOSE:To prevent a graphite crucible from being attacked by Al and is thereby consumed in a short period of time by adding specific ratios of Zr and Ti to the molten Al in the graphite crucible, melting the molten Al added with this Zr and Ti at a specific temp. and depositing the Al by evaporation at the time of vacuum vapor deposition of the Al by utilizing the graphite crucible. CONSTITUTION:The molten Al in the graphite crucible is used as the vapor deposition source at the time of subjecting the surface of plastic films for packaging food, building materials, steel sheets for household electric appliances, etc., to vacuum vapor deposition of the thin film of the Al. The metal elements, such as Zr and Ti are added into the molten Al in the graphite crucible to form the compsn. consisting of 78 to 97vol.% grade of the Al in the molten metal and Zr and Ti as the balance in this case. This Al alloy is heated and melted to the m. p. of the alloy to 1500 deg.C to cause the vapor deposition of the Al. The Zr and Ti has the higher affinity to graphite than the Al and preferentially forms ZrC and TiC which deposit and stick to the inside surface of the graphite crucible. The attack of the graphite by the Al is thus suppressed and the service life of the graphite crucible is greatly prolonged.
    • 79. 发明专利
    • VACUUM DEPOSITION DEVICE
    • JPH02118072A
    • 1990-05-02
    • JP27094288
    • 1988-10-28
    • MITSUBISHI HEAVY IND LTD
    • TAGUCHI TOSHIOHOSHI YOUNOSUKEKOBAYASHI TOSHIROOKITA HAJIMEKAMIKAWA SUSUMU
    • C23C14/56
    • PURPOSE:To enable vapor depositing operation in a long time by arranging a network vessel equipping a feeder with vapor depositing material introduced thereinto to the side face of a cooling roll with a flexible base plate wound thereon in a vapor deposition chamber and heating the vapor depositing material in the case of vapor-depositing sublimable substance such as inorganic material and high-m.p. metal on the surface of the flexible base plate. CONSTITUTION:In the case of vapor-depositing sublimable substance consisting of both high-m.p. metal such as Ti and inorganic material such as SixOy on the surface of a flexible base plate 1 such as a plastic film, paper and a steel strip, the flexible base plate 1 is supplied into a vacuum deposition chamber 2 via a vacuum sealing chamber 13 evacuated and vacuumized with an exhaust pump unit 11. This base plate 1 is wound on a rotating cooling roll 4 and moved. A network vessel 9 with sublimable vapor depositing material 8 introduced thereinto is arranged to the side face of the cooling roll 4 and heated with a heater 10 to sublimate the material 8. The vapor- deposited film of sublimate vapor depositing material is formed on the surface of the base material 1 wound on the cooling roll 4. The vapor depositing material is supplied to the network vessel 9 from a feeder 12 with large amounts of material 8 introduced thereinto and therefore vapor depositing operation is enabled in a long time.