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71. 发明专利

JP2009280555A Method and apparatus for producing mono(lower alkyl)monoalkanolamine 审中-公开
标题翻译：制备单（低级烷基）单烷基胺的方法和装置
公开(公告)号：JP2009280555A
公开(公告)日：2009-12-03
申请号：JP2008137277
申请日：2008-05-26
申请人： Mitsubishi Heavy Ind Ltd , 三菱重工業株式会社
发明人： TACHIBANA SHINYA , TSUJIUCHI TATSUYA , OISHI GOJI
IPC分类号： C07C213/04 , B01J29/40 , C07B61/00 , C07C213/10 , C07C215/08
CPC分类号： C07C213/04 , C07C215/08
摘要： PROBLEM TO BE SOLVED: To provide a method and apparatus for producing mono(lower alkyl)monoalkanolamine in an energy saving way.
SOLUTION: The apparatus for producing a mono(lower alkyl)monoalkanolamine is constituted of a reaction/distillation column 12 to which a raw material mixture 11 consisting of a mono(lower alkyl)amine (AA: a raw material I) and an alkylene oxide (AO: a raw material II) is fed by a raw-material main feed line L
0 , and a purification/distillation column 19 for separating a reaction product 13 separated in a liquid form into an intended reaction product 20 (a monomer) and a residue 21 (a dimer) by distillation. Unreacted raw materials 16 are separated from the top 12a of the column via a line L
1 , and the reaction product 13 is separated from the bottom 12b of the column via a line L
2 .
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：待解决的问题：提供以节能的方式制备单（低级烷基）单烷醇胺的方法和装置。解决方案：单（低级烷基）单链烷醇胺的制造装置由反应/蒸馏塔12构成，原料混合物11由单（低级烷基）胺（AA：原料I）和通过原料主供给管线L S供给环氧烷（AO：原料II）和用于将液态分离的反应产物13分离的净化/蒸馏塔19 预期的反应产物20（单体）和残余物21（二聚体）。未反应的原料16经由管线L 从塔的顶部12a分离，并且反应产物13经由管线L 2从柱的底部12b分离， SB>。版权所有（C）2010，JPO＆INPIT

72. 发明专利

JP2008133144A Hydrogen production system and exhaust-heat recovery method using the same 有权
标题翻译：氢生产系统和使用其的排热恢复方法
公开(公告)号：JP2008133144A
公开(公告)日：2008-06-12
申请号：JP2006318690
申请日：2006-11-27
申请人： Mitsubishi Heavy Ind Ltd , 三菱重工業株式会社
发明人： TANAKA YUKIO , TACHIBANA SHINYA , FUJIMOTO YOSHIMASA , KOBAYASHI KAZUTO
IPC分类号： C01B3/38
CPC分类号： Y02P20/124 , Y02P20/129
摘要： PROBLEM TO BE SOLVED: To provide a hydrogen production system which is improved in the efficiency of exhaust-heat recovery by enabling exhaust-heat recovery so as to reduce the fuel consumption amount in a boiler. SOLUTION: The hydrogen production system 10A comprises: a desulfurizer 101 for removing sulfur contained in a raw material gas G containing hydrocarbons as main components; and a hydrogen production apparatus 105 for reforming the hydrocarbons in the desulfurized raw material gas G by using a reforming catalyst and taking out formed hydrogen by selectively separating only the formed hydrogen. Further, the hydrogen production system 10A comprises: a humidifier 11A for humidifying the raw material gas G in a raw material gas supply line L 1-1 for supplying the raw material gas G to the hydrogen production apparatus 105 from the desulfurizer 10; and a hydrogen supply line L 4-1 for supplying hydrogen formed in the hydrogen production apparatus 105 to the humidifier 11A. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：解决的问题：提供一种氢气生产系统，其通过使排气热回收提高废热回收的效率，从而降低锅炉中的燃料消耗量。解决方案：氢气生产系统10A包括：用于除去含有烃作为主要成分的原料气体G中所含的硫的脱硫器101; 以及用于通过使用重整催化剂重整脱硫原料气体G中的烃并通过仅选择性分离形成的氢而取出形成的氢的氢气制备装置105。此外，氢气制备系统10A包括：用于将用于将原料气体G供应到氢气制备装置105的原料气体供应管线L 1-1 中的原料气体G加湿的加湿器11A 来自脱硫器10; 以及用于将形成在氢气制备装置105中的氢气供应到加湿器11A的氢气供应管线L 4-1 。版权所有（C）2008，JPO＆INPIT

73. 发明专利

JP2007277161A Method and apparatus for producing mono lower alkyl monoalkanol amine 有权
标题翻译：生产单一低级烷基单烷基胺的方法和装置
公开(公告)号：JP2007277161A
公开(公告)日：2007-10-25
申请号：JP2006105632
申请日：2006-04-06
申请人： Mitsubishi Heavy Ind Ltd , Nippon Nyukazai Kk , 三菱重工業株式会社 , 日本乳化剤株式会社
发明人： TACHIBANA SHINYA , YOSHIYAMA TAKASHI , KOBAYASHI KAZUTO , MITA HIDEHISA , SHINJO RYOSUKE , SAITO KENJI
IPC分类号： C07C213/04 , B01J29/40 , C07B61/00 , C07C215/08
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a method and an apparatus for producing a mono lower alkyl monoalkanol amine in a high yield. SOLUTION: This method for producing the mono lower alkyl monoalkanol amine, comprising reacting a mono lower alkyl amine with an alkylene oxide in the presence of a catalyst comprising crystalline metallosilicate, is characterized by forming a reaction zone in the presence of the catalyst in multi-stages, and serially supplying the mono lower alkyl amine to the multi-stage reaction zone to flow in the rear stage reaction zone through the front stage reaction zone, and supplying the alkylene oxide to the front flow of each reaction zone in the multi-stage reaction zones in parallel to mitigate the rise of temperature due to the reaction in each reaction zone. The apparatus is characterized by forming a reactor charged with the catalyst at multi-stages reactor to connect a flow route for supplying the mono lower alkyl amine in multi-stage reactors, and branching flow routes for supplying the alkylene oxide to connect in parallel in the front reactor of each reactor of the multi-stage reactors. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：待解决的问题：提供以高产率制备单低级烷基单烷醇胺的方法和设备。解决方案：制备单低级烷基单链烷醇胺的方法包括在含有结晶金属硅酸盐的催化剂存在下使单低级烷基胺与烯化氧反应，其特征在于在催化剂存在下形成反应区在多级反应区中连续供给单级低级烷基胺至多级反应区，通过前段反应区在后段反应区中流通，并将烯化氧供给至各反应区的前流多级反应区并联以缓解由于每个反应区中的反应导致的温度上升。该装置的特征在于在多级反应器中形成装有催化剂的反应器，以连接用于在多级反应器中供应单低级烷基胺的流动路线，以及用于供应烯化氧以在多级反应器的每个反应器的前反应器。版权所有（C）2008，JPO＆INPIT

74. 发明专利

JP2007217344A Method and apparatus for producing mono lower alkyl monoalkanol amine 有权
标题翻译：生产单一低级烷基单烷基胺的方法和装置
公开(公告)号：JP2007217344A
公开(公告)日：2007-08-30
申请号：JP2006039605
申请日：2006-02-16
申请人： Mitsubishi Heavy Ind Ltd , Nippon Nyukazai Kk , 三菱重工業株式会社 , 日本乳化剤株式会社
发明人： TACHIBANA SHINYA , YOSHIYAMA TAKASHI , KOBAYASHI KAZUTO , MITA HIDEHISA , SHINJO RYOSUKE , SAITO KENJI
IPC分类号： C07C213/04 , B01J29/40 , C07B61/00 , C07C215/08
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a method and an apparatus for continuously producing a mono lower alkyl monoalkanol amine in a high yield. SOLUTION: This method for reacting a mono lower alkyl amine with an alkylene oxide in the presence of a catalyst containing a crystalline metallosilicate to produce the mono lower alkyl monoalkanol amine is characterized by including an unreacted raw material recovery process for separating the unreacted mono lower alkyl amine, the alkylene oxide, and the reaction product from the reaction mixture discharged from a reaction zone in the presence of the catalyst by a distillation method and then returning the separated and recovered unreacted mono lower alkyl amine and the separated and recovered unreacted alkylene oxide to the reaction zone, and a purification process for separating the produced mono lower alkyl monoalkanol amine and the produced mono lower alkyl dialkanol amine by a distillation method to recover the mono lower alkyl monoalkanol amine. COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：待解决的问题：提供以高产率连续生产单低级烷基单烷醇胺的方法和装置。解决方案：在含有结晶金属硅酸盐的催化剂存在下使单低级烷基胺与烯化氧反应以制备单低级烷基单链烷醇胺的方法的特征在于包括用于分离未反应的未反应的原料回收方法单烷基低级烷基胺，烯化氧，以及在催化剂存在下通过蒸馏法从反应区排出的反应混合物的反应产物，然后使分离回收的未反应的单低级烷基胺和未反应的未反应的环氧烷与反应区的反应，以及通过蒸馏法分离生产的单低级烷基一链烷醇胺和所制备的单低级烷基二链烷醇胺以回收单低级烷基单链烷醇胺的纯化方法。版权所有（C）2007，JPO＆INPIT

75. 发明专利

JP2007139259A Simple boiler, and hydrogen manufacturing device using it 审中-公开
标题翻译：简单的锅炉和使用它的氢气制造设备
公开(公告)号：JP2007139259A
公开(公告)日：2007-06-07
申请号：JP2005331140
申请日：2005-11-16
申请人： Mitsubishi Heavy Ind Ltd , 三菱重工業株式会社
发明人： FUJIMOTO YOSHIMASA , TANAKA YUKIO , TACHIBANA SHINYA , KOBAYASHI KAZUTO
IPC分类号： F22B35/00 , B01D53/22 , C01B3/38
摘要： PROBLEM TO BE SOLVED: To provide a simple type boiler suppressing the fluctuation of a vapor pressure during operation.
SOLUTION: The simple boiler 4 has a first pressure detecting means 21 for detecting a first pressure being a minimum pressure in the boiler, and a second pressure being a maximum pressure, and water vapor is produced by pilot combustion and main combustion. A second pressure detecting means 22 is provided for detecting a third pressure in a first pressure neighborhood, and a fourth pressure in a second pressure neighborhood, between the first pressure and the second pressure. When the pressure in the boiler becomes higher than the third pressure, the main combustion is stopped, and when the pressure in the boiler becomes lower than the fourth pressure, the main combustion is carried out.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供一种抑制运行时蒸汽压波动的简单型锅炉。解决方案：简单的锅炉4具有第一压力检测装置21，用于检测锅炉中的最小压力的第一压力，第二压力是最大压力，并且通过先导燃烧和主燃烧产生水蒸汽。提供第二压力检测装置22，用于在第一压力和第二压力之间检测第一压力附近的第三压力和第二压力附近的第四压力。当锅炉中的压力高于第三压力时，主燃烧停止，当锅炉中的压力低于第四压力时，进行主燃烧。版权所有（C）2007，JPO＆INPIT

76. 发明专利

JP2007117843A Fluid-permeable thin film structure body and its manufacturing method 审中-公开
标题翻译：流体透气薄膜结构体及其制造方法
公开(公告)号：JP2007117843A
公开(公告)日：2007-05-17
申请号：JP2005311349
申请日：2005-10-26
申请人： Mitsubishi Heavy Ind Ltd , 三菱重工業株式会社
发明人： NAKAJIMA HIROSHI , KAJIWARA TETSUO , TACHIBANA SHINYA
IPC分类号： B01D69/12 , B01D53/22 , B01D69/10 , B01D71/02 , C01B3/38 , C01B3/56
摘要： PROBLEM TO BE SOLVED: To provide a fluid-permeable thin film structure body which can form a fluid-permeable thin film including hydrogen-permeable metallic foil to be thinner than hydrogen-permeable metallic foil of conventional structure to improve fluid permeability and which prevents drop in fluid permeability due to a reaction with an impure fluid different from a raw material fluid such as a raw material gas, and to provide its manufacturing method.
SOLUTION: The fluid-permeable thin film structure body 100 is formed by connecting fluid-permeable thin films 1a and 1b, which have fluid-permeable capability, with a metallic reinforcement plate 2 having a plurality of aperture parts on its surface. In this case, a plurality of fluid-permeable thin films 1a and 1b are stacked, and the junction planes 7 of the fluid-permeable thin films 1a and 1b are bonded to each other.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供一种流体可渗透的薄膜结构体，其可以形成包含透氢性金属箔的流体渗透性薄膜，其比常规结构的透氢性金属箔薄，以提高流体渗透性，能够防止由于与原料气体等原料流体不同的不纯的液体的反应引起的流体渗透性的降低，提供其制造方法。解决方案：透液薄膜结构体100通过将具有流体渗透性的流体可渗透薄膜1a和1b与其表面上具有多个孔部的金属加强板2连接而形成。在这种情况下，堆叠多个透液性薄膜1a和1b，并且流体渗透薄膜1a和1b的接合面7彼此接合。版权所有（C）2007，JPO＆INPIT

77. 发明专利

JP2006111472A System and method for producing hydrogen 审中-公开
标题翻译：用于生产氢的系统和方法
公开(公告)号：JP2006111472A
公开(公告)日：2006-04-27
申请号：JP2004298339
申请日：2004-10-13
申请人： Mitsubishi Heavy Ind Ltd , 三菱重工業株式会社
发明人： TANAKA YUKIO , KOBAYASHI KAZUTO , FUJIMOTO YOSHIMASA , TACHIBANA SHINYA
IPC分类号： C01B3/38 , H01M8/06
CPC分类号： Y02E60/50
摘要： PROBLEM TO BE SOLVED: To provide a system for producing hydrogen, which exhibits improved thermal efficiency and in which the problem related to the waste water treatment is solved and apparatus itself can be made compact; and to provide a method for producing hydrogen.
SOLUTION: In a hydrogen producing system, which produces hydrogen by performing steam reforming reaction using hydrocarbons or oxygen-containing hydrocarbons as raw materials in a hydrogen separation-type reformer 1 having a hydrogen permeation section partitioned by a hydrogen separation membrane 5 in a reaction tube filled with a reforming catalyst 3 and a combustion gas passage at the outside of the reaction tube, a pressure reducing means 7 for reducing the pressure of an exhaust gas 6 of the reformer 1 and an exhaust gas reformer 8 for reforming the exhaust gas 6 having passed through the pressure reducing means 7 are provided, and the exhaust gas 6 having passed through the exhaust gas reformer 8 is burnt by a combustor 10 of the hydrogen separation-type reformer 1.
COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：提供一种表现出改善的热效率并且其中与废水处理相关的问题得到解决并且可以使设备本身变得紧凑的生产氢气的系统; 并提供生产氢的方法。解决方案：在氢分离型重整器1中通过使用烃或含氧烃作为原料进行蒸汽重整反应产生氢气的氢气生产系统中，氢分离型重整器1具有由氢分离膜5分隔的氢气渗透部分填充有重整催化剂3的反应管和在反应管外侧的燃烧气体通道，用于降低重整器1的排气6的压力的减压装置7和用于重整排气的废气重整器8 设有通过减压装置7的气体6，并且通过排气重整器8的废气6被氢分离型重整器1的燃烧器10燃烧。版权所有（C）2006 ，JPO＆NCIPI

78. 发明专利

JP2006096623A Primary reformer integrated with thermal desulfurizer 审中-公开
标题翻译：主要改造器与热脱硫器集成
公开(公告)号：JP2006096623A
公开(公告)日：2006-04-13
申请号：JP2004285568
申请日：2004-09-30
申请人： Mitsubishi Heavy Ind Ltd , 三菱重工業株式会社
发明人： TACHIBANA SHINYA , KOBAYASHI KAZUTO , TANAKA YUKIO
IPC分类号： C01B3/38
CPC分类号： Y02P20/129
摘要： PROBLEM TO BE SOLVED: To provide an apparatus used in a system for producing hydrogen from a feedstock containing hydrocarbons, being capable of removing sulfur compounds such as carbonyl sulfide, and reduced in heat loss. SOLUTION: The primary reformer 3 integrated with a thermal desulfurizer is one equipped with a reaction vessel 30 which contains a thermal desulfurizer section 31 packed with a thermal desulfurizing agent and a primary reforming section 32 packed with a primary reforming catalyst, wherein heat exchange between the thermal desulfurization section 31 and the primary reforming section 32 is possible. A hydrogen production system 1 is also equipped with an ordinary temperature adsorption desulfurizer 2, the primary reformer integrated with the thermal desulfurizer, and a hydrogen separation type reformer 4. COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：提供一种用于从含有烃的原料生产氢的系统中使用的装置，其能够除去硫化合物如硫化羰，并减少热损失。＆lt;解决方案＆gt;与热脱硫器一体化的一次重整器3是配备有反应容器30的反应容器30，反应容器30包含填充有热脱硫剂的热脱硫部31和填充有初级重整催化剂的一次重整部32，热脱硫部31与一次重整部32之间的交换是可能的。氢气生产系统1还配备有常温吸附脱硫器2，与热脱硫器一体化的一次重整器和氢分离型重整器4.版权所有（C）2006，JPO＆NCIPI

79. 发明专利

JP2006096622A Hydrogen production system 审中-公开
标题翻译：氢生产系统
公开(公告)号：JP2006096622A
公开(公告)日：2006-04-13
申请号：JP2004285567
申请日：2004-09-30
申请人： Mitsubishi Heavy Ind Ltd , 三菱重工業株式会社
发明人： TACHIBANA SHINYA , KOBAYASHI KAZUTO , TANAKA YUKIO
IPC分类号： C01B3/38
摘要： PROBLEM TO BE SOLVED: To provide a hydrogen production system capable of producing hydrogen from a feedstock gas rich in 2C or higher hydrocarbons, such as naphtha or kerosene.
SOLUTION: The hydrogen production system 1 is one equipped with a desulfurizer 2 that removes sulfur from a feedstock based on hydrocarbons, a preheater 10 that raises the temperature of the hydrocarbons in the desulfurized feedstock, a primary reformer 3 that at least partially reforms the hydrocarbons in the feedstock preheated by the preheater with the aid of a reforming catalyst, and a hydrogen separation type reformer 4 that further reforms the hydrocarbons leaving the primary reformer and selectively separating and recovering only the formed hydrogen, wherein the preheater 10 is equipped with a combustion chamber gas feed line 8 that feeds the gas in the combustion chamber 43 of the hydrogen separation type reformer.
COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：提供一种能够从富含2C或更高级烃的原料气体如石脑油或煤油中产生氢气的氢气生产系统。解决方案：氢气生产系统1是配备有脱硫剂2的脱硫剂2，其基于烃除去来自原料的硫，预热器10，其提高脱硫原料中的烃的温度;初级重整器3，其至少部分地借助于重整催化剂改进由预热器预热的原料中的烃，以及氢分离型重整器4，其进一步改造离开一次重整器的烃并选择性地分离和回收仅形成的氢，其中预热器10配备具有在氢分离型重整器的燃烧室43中供给气体的燃烧室气体供给管线8。版权所有（C）2006，JPO＆NCIPI

80. 发明专利

JP2005015262A Hydrogen production system 审中-公开
标题翻译：氢生产系统
公开(公告)号：JP2005015262A
公开(公告)日：2005-01-20
申请号：JP2003180491
申请日：2003-06-25
申请人： Mitsubishi Heavy Ind Ltd , 三菱重工業株式会社
发明人： TACHIBANA SHINYA , KOBAYASHI KAZUTO , TANAKA YUKIO
IPC分类号： C01B3/38 , C10G29/16 , C10G45/08 , H01M8/06
CPC分类号： Y02E60/50
摘要： PROBLEM TO BE SOLVED: To provide a hydrogen production system capable of highly efficiently producing hydrogen by using a ≥2C hydrocarbon as a raw material with less deterioration of the performance. SOLUTION: The hydrogen production system includes: a desulfurizer 2 for removing sulfur which is contained in the raw material consisting essentially of the ≥2C hydrocarbon; a primary reformer 3 for reforming at least partially the desulfurized raw material by using a reforming catalyst; and a hydrogen separation type reformer 4 for further reforming the raw material which has passed through the primary reformer by the reforming catalyst and selectively separating and taking out only the produced hydrogen. COPYRIGHT: (C)2005,JPO&NCIPI

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