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71. 发明授权

US06355113B1 Multiple solvent cleaning system 失效
标题翻译：多溶剂清洗系统
公开(公告)号：US06355113B1
公开(公告)日：2002-03-12
申请号：US09186932
申请日：1998-11-06
申请人： David Nalewajek , Rajat Subhra Basu , David Paul Wilson , Michael Van Der Puy , Ellen Louise Swan , Peter Brian Logsdon , Gary J. Zyhowski , Hepburn Ingham , Daniel Franklin Harnish , Joel Edward Rodgers
发明人： David Nalewajek , Rajat Subhra Basu , David Paul Wilson , Michael Van Der Puy , Ellen Louise Swan , Peter Brian Logsdon , Gary J. Zyhowski , Hepburn Ingham , Daniel Franklin Harnish , Joel Edward Rodgers
IPC分类号： B08B308
CPC分类号： C11D7/5018 , C11D7/24 , C11D7/28 , C23G5/02 , C23G5/024 , H05K3/26 , H05K2203/0766 , H05K2203/0783 , H05K2203/1518
摘要： A non-aqueous cleaning process uses an organic solvent for removing soil or surface contamination from contaminated articles such as printed circuit boards which are cleaned by immersion into a sump compartment of a cleaning tank containing the organic cleaning solvent. The organic solvent is preferably a hydrocarbon solvent. The cleaned articles, now coated with the organic cleaning solvent, are then disposed in a rinsing sump containing a fluorocarbon based rinsing solvent having an affinity for the organic cleaning solvent. The organic solvent is thus removed from the articles which are then dried without waste water as in a conventional solvent vapor degreasing solvent process.
摘要翻译：非水清洗方法使用有机溶剂去除被污染物品（例如印刷电路板）污染的土壤或表面污染物，其通过浸入含有有机清洗溶剂的清洗槽的贮槽室中清洗。有机溶剂优选为烃溶剂。然后将现在涂覆有机清洁溶剂的清洁物品置于含有对有机清洁溶剂具有亲和性的基于碳氟化合物的漂洗溶剂的漂洗池中。因此，有机溶剂从制品中除去，然后如常规溶剂蒸汽脱脂溶剂法那样无需废水干燥。

72. 发明授权

US6133472A Fluorinated oxyvinyl compounds and methods of preparing and using same 失效
标题翻译：氟化氧乙烯基化合物及其制备和使用方法
公开(公告)号：US6133472A
公开(公告)日：2000-10-17
申请号：US9110
申请日：1998-01-20
申请人： David Nalewajek , David Bradley , John Schabel , Robert Blomquist
发明人： David Nalewajek , David Bradley , John Schabel , Robert Blomquist
IPC分类号： G02B6/00 , C07C43/17 , C07C43/172 , C07C69/63 , C07C309/63 , C07C309/73 , C08F8/18 , C08F16/12 , C09D11/02 , C09D11/10 , C09D129/10 , C09J4/00 , C09J129/10 , G02B6/12 , G11B7/2531 , G11B7/2533 , G11B7/2542 , C07C69/00
CPC分类号： C09J129/10 , C07C309/73 , C07C43/17 , C07C43/172 , C07C69/63 , C08F8/18 , C09D11/101 , C09D129/10 , C09J4/00 , G11B7/2531 , G11B7/2533 , G11B7/2542 , G11B7/256
摘要： Fluorine containing oxyvinyl compounds characterized by having one or more oxyvinyl groups separated from fluorine containing groups by at least one alkylene group having 2-8 carbon atoms and by at least one oxygen atom in addition to the oxygen on the oxyvinyl. In general the compounds of the invention have the generic formula:Rz(L).sub.a (Ry).sub.b OROCH.dbd.CH.sub.2.Where L is .dbd.CHCOOROCH.dbd.CH.sub.2 ; a is number of 0 to about 1; R.sub.y is --CO--; b is a number of 0 to about 1; R is cycloalkane or (CH.sub.2).sub.x --, where x is a number of about 2 through about 10; R.sub.z is R.sub.f C.sub.n H.sub.m where R.sub.f is a fluorinated alkylene moiety of about 1 to about 12 carbon atoms which may be linear or branch chained and may contain a further --OROCH.dbd.CH.sub.2 group; n is an integer of about 1 through about 6; and m is an integer of n to 2n. The compounds are suitable for use in optical devices such as fibers and waveguides, are readily radiation curable and curable by other means, and can be formulated to be of low viscosity when applied. The compounds are also suited for coatings, inks and adhesive and other applications. The invention includes methods for preparing and using the compounds and products employing the compounds. Intermediates to prepare the compounds and methods to prepare the intermediates are also included.
摘要翻译：含氟氧基乙烯基化合物的特征在于具有一个或多个氧基乙烯基，其含氟基团通过至少一个具有2-8个碳原子的亚烷基和至少一个氧原子与氧基乙烯基上的氧分开。通常，本发明的化合物具有以下通式：Rz（L）a（Ry）bOROCH = CH 2。其中L = CHCOOROCH = CH 2; a是0到1的数字; Ry是-CO-; b是0到1的数; R是环烷烃或（CH 2）x - ，其中x是约2至约10的数; Rz是RfCnHm，其中Rf是约1至约12个碳原子的氟化亚烷基部分，其可以是直链或支链，并且可以含有另外的-OROCH = CH 2基团; n为约1至约6的整数; m为n〜2n的整数。该化合物适用于诸如纤维和波导的光学装置，易于辐射固化并且可通过其它方法固化，并且可以在施用时配制成具有低粘度。这些化合物也适用于涂料，油墨和粘合剂等应用。本发明包括制备和使用化合物和使用该化合物的产品的方法。还包括制备化合物的中间体和制备中间体的方法。

73. 发明授权

US5868799A Surfactants and drying and drycleaning compositions which utilize said surfactants 失效
标题翻译：使用所述表面活性剂的表面活性剂和干燥和干洗组合物
公开(公告)号：US5868799A
公开(公告)日：1999-02-09
申请号：US761043
申请日：1996-12-05
申请人： Gary John Zyhowski , David Nalewajek , Leonard Michael Stachura
发明人： Gary John Zyhowski , David Nalewajek , Leonard Michael Stachura
IPC分类号： D06L1/04 , C11D1/34 , C11D1/62
CPC分类号： D06L1/04
摘要： Novel surfactants and drying, drycleaning and soil repellency compositions containing such surfactants which utilize such surfactants. The surfactants are fluorine containing quaternary ammonium salts, and the drying, drycleaning and soil repellency compositions contain at least one halocarbon component and at least one of the fluorine containing surfactants. These compositions have the ability to remove water or aqueous films from the surfaces of a broad range of substrates and impart soil repellency to fabrics.
摘要翻译：新型表面活性剂和含有这种表面活性剂的干燥，干洗和防污性组合物。表面活性剂是含氟季铵盐，干燥，干洗和防污组合物含有至少一种卤代烃组分和至少一种含氟表面活性剂。这些组合物具有从宽范围的基材的表面除去水或水性膜的能力，并赋予织物防污性。

74. 发明授权

US5856286A Surfactants for use in drying and dry cleaning compositions 失效
标题翻译：用于干燥和干洗组合物的表面活性剂
公开(公告)号：US5856286A
公开(公告)日：1999-01-05
申请号：US881179
申请日：1997-06-23
申请人： David Nalewajek , Leonard Michael Stachura , Gary John Zyhowski
发明人： David Nalewajek , Leonard Michael Stachura , Gary John Zyhowski
IPC分类号： C07F9/09 , C07F9/12 , C11D1/00 , C11D3/24 , D06L1/04 , C11D3/28
CPC分类号： D06L1/04 , C07F9/098 , C07F9/12 , C11D1/006 , C11D3/24 , C11D3/245 , C11D3/43
摘要： The invention provides a fluorinated surfactant for use with halocarbon and hydrofluoroether solvents. Additionally, the invention provides drying, dry cleaning, and soil repellency compositions containing a halocarbon or hydrofluoroether and a fluorinated surfactant.
摘要翻译：本发明提供一种与卤代烃和氢氟醚溶剂一起使用的氟化表面活性剂。此外，本发明提供了含有卤代烃或氢氟醚和氟化表面活性剂的干燥，干洗和防污组合物。

75. 发明授权

US5800729A Mixtures of pentafluoropropane and a hydrofluorocarbon having 3 to 6 carbon atoms 失效
标题翻译：五氟丙烷与碳原子数为3〜6的氢氟烃的混合物
公开(公告)号：US5800729A
公开(公告)日：1998-09-01
申请号：US685821
申请日：1996-07-25
申请人： David P. Wilson , Rajiv R. Singh , Rajat S. Basu , Ellen L. Swan , David Nalewajek
发明人： David P. Wilson , Rajiv R. Singh , Rajat S. Basu , Ellen L. Swan , David Nalewajek
IPC分类号： C08G18/79 , C08G101/00 , C08J9/14 , C09K3/00 , C09K5/04
CPC分类号： C08J9/14 , C09K5/045 , C09K2205/22 , C09K2205/32 , Y10S521/902 , Y10S521/91
摘要： The invention discloses novel azeotrope-like mixtures of fluorinated compounds which are useful for heating and cooling as heat transfer agents and/or refrigerants. The azeotrope-like mixture comprises: (a) pentafluoropropane; and (b) a hydrofluorocarbon of the formula: C.sub.x F.sub.y H.sub.z, wherein x is 3, 4, 5, or 6 and y and z are each independently 1 or a positive whole number such that the result of y/(y+z) is greater than 0.67.
摘要翻译：本发明公开了可用作加热和冷却作为传热剂和/或制冷剂的氟化化合物的类似新颖的混合物。共沸混合物包含：（a）五氟丙烷; 和（b）下式的氢氟烃，其中x为3,4,5或6，y和z各自独立地为1或正整数，使得y /（y + z）的结果更大大于0.67。

76. 发明授权

US5696307A Hydrofluoroalkanes as cleaning and degreasing solvents 失效
标题翻译：氢氟烷作为清洗和脱脂溶剂
公开(公告)号：US5696307A
公开(公告)日：1997-12-09
申请号：US184810
申请日：1994-01-21
申请人： Michael Van Der Puy , Rajat Subhra Basu , David Nalewajek , Lois A. Ellis
发明人： Michael Van Der Puy , Rajat Subhra Basu , David Nalewajek , Lois A. Ellis
IPC分类号： C07C19/08 , C11D7/50 , C23G5/028 , C07C23/06
CPC分类号： C07C19/08 , C11D7/5018 , C23G5/02803
摘要： Hydrofluoroalkanes useful as solvents, especially for vapor degreasing and solvent cleaning, are one or many of the following formulae: CHF.sub.2 --X--(CHF).sub.n --X--Y wherein X is selected from the group consisting of CHF, CF.sub.2 and CH.sub.2, Y is CH.sub.3, and n is 0, 1 or 2.
摘要翻译：可用作溶剂，特别是用于蒸气脱脂和溶剂清洗的溶剂的氢氟烷烃是下列一种或多种：CHF 2 -X-（CHF）n X-Y，其中X选自CHF，CF 2和CH 2，Y是CH 3， n为0,1或2。

77. 发明授权

US5534176A Refrigeration lubricants prepared by polymerizing alkene having a perfluoroalkyl group on one end thereof 失效
标题翻译：通过在其一端聚合具有全氟烷基的烯烃制备的制冷润滑剂
公开(公告)号：US5534176A
公开(公告)日：1996-07-09
申请号：US380470
申请日：1995-01-30
申请人： David Nalewajek , Richard E. Eibeck , Raymond H. P. Thomas
发明人： David Nalewajek , Richard E. Eibeck , Raymond H. P. Thomas
IPC分类号： C09K5/04 , C10M107/38 , C10M171/00
CPC分类号： C09K5/045 , C10M107/38 , C10M171/008 , C09K2205/124 , C09K2205/24 , C10M2211/022 , C10M2211/06 , C10M2213/02 , C10M2213/062 , C10N2240/00 , C10N2240/22 , C10N2240/30 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66
摘要： The present invention provides a composition for use in refrigeration and air-conditioning comprising: (a) at least one refrigerant selected from the group consisting of hydrofluorocarbon, hydrochlorofluorocarbon, fluorocarbon, and chlorofluorocarbon; and (b) a sufficient amount to provide lubrication of at least one lubricant prepared by polymerizing alkene having a perfluoroalkyl group on one end thereof. The lubricant has a molecular weight of about 300 to about 3,000 and a viscosity of about 5 to about 150 centistokes at 37.degree. C. The lubricant is miscible in combination with the refrigerant in the range between about -40.degree. C. and at least about +20.degree. C.
摘要翻译：本发明提供一种用于制冷和空调的组合物，包括：（a）至少一种选自氢氟碳化合物，氢氯氟烃，氟碳化合物和氯氟烃的制冷剂; 和（b）足够的量来提供通过在其一端聚合具有全氟烷基的烯烃制备的至少一种润滑剂的润滑。润滑剂的分子量为约300至约3,000，在37℃下的粘度为约5至约150厘沲。润滑剂可与制冷剂混合在约-40℃至约约 +20℃

78. 发明授权

US5315048A Preparation of 1,1,1,2,3-pentafluoropropane by reduction of 1,2,3-trichloropentafluropropane 失效
标题翻译：通过还原1,2,3-三氯丙基丙烷制备1,1,1,2,3-五氟丙烷
公开(公告)号：US5315048A
公开(公告)日：1994-05-24
申请号：US130083
申请日：1993-09-30
申请人： Michael Van Der Puy , David Nalewajek
发明人： Michael Van Der Puy , David Nalewajek
IPC分类号： C07C17/23 , C07C19/08 , C07C17/24 , C07C19/02
CPC分类号： C07C19/08 , C07C17/23
摘要： The present invention relates to a process for the reductive dechlorination of ClCF.sub.2 CFClCF.sub.2 Cl to CF.sub.3 CHFCH.sub.2 F comprising the step of contacting 1,2,3-trichloropentafluoropropane and H.sub.2 in the presence of a catalyst selected from the group consisting of palladium, platinum, ruthenium, rhodium, iridium and mixtures thereof supported on alumina under reaction conditions sufficient to produce a product stream containing 1,1,1,2,3-pentafluoropropane.
摘要翻译：本发明涉及将ClCF 2 CFClCF 2 Cl还原脱氯至CF 3 CHFCH 2 F的方法，包括在选自钯，铂，钌，铑，铱的催化剂存在下使1,2,3-三氯五氟丙烷与H 2接触的步骤和其混合物在足以产生含有1,1,1,2,3-五氟丙烷的产物流的反应条件下负载在氧化铝上。

79. 发明授权

US4770797A Carbon fluoride chloride lubricant 失效
标题翻译：碳氟化碳润滑剂
公开(公告)号：US4770797A
公开(公告)日：1988-09-13
申请号：US846547
申请日：1986-03-31
申请人： Allan V. Syracuse , Lynn E. McCurry , David Nalewajek
发明人： Allan V. Syracuse , Lynn E. McCurry , David Nalewajek
IPC分类号： C10M111/04 , C10M125/02 , C10M125/18
CPC分类号： C10M111/04 , C10M2201/00 , C10M2201/003 , C10M2201/0403 , C10M2201/041 , C10M2201/0413 , C10M2201/042 , C10M2201/0423 , C10M2201/0433 , C10M2201/053 , C10M2201/061 , C10M2201/066 , C10M2201/16 , C10M2201/18 , C10M2205/00 , C10M2205/04 , C10M2205/043 , C10M2209/00 , C10M2209/02 , C10M2209/10 , C10M2209/1003 , C10M2209/101 , C10M2209/1013 , C10M2209/1023 , C10M2211/06 , C10M2213/00 , C10M2213/02 , C10M2213/023 , C10M2213/043 , C10M2213/0606 , C10M2213/062 , C10M2213/0623 , C10M2217/0403 , C10M2217/0415 , C10M2217/042 , C10M2217/0425 , C10M2217/043 , C10M2217/0435 , C10M2217/0443 , C10M2217/0453 , C10M2217/0465 , C10N2250/121
摘要： The application of carbon fluoride chloride in dry lubricant compositions is disclosed. The material offers a substantial improvement in lubricating properties over prior art carbon fluoride dry lubricants.The improved lubricant is comprised of carbon fluoride chloride of the general formula (C.sub.y F.sub.x Cl.sub.z).sub.n wherein y is 1 or 2, x is greater than 0 to 1.2, z is 0.1 and n defines an infinitely large two dimensional array of repeating units occurring in this molecule of high molecular weight. The resulting lubricant has improved lubricating properties over graphite, MoS.sub.2 and carbon monofluoride.
摘要翻译：公开了氟化氯在干润滑剂组合物中的应用。与现有技术的氟化碳干润滑剂相比，该材料提供了润滑性能的显着改进。改进的润滑剂由通式（CyFxClz）n的氟化碳氯化物组成，其中y为1或2，x大于0至1.2，z为0.1，n定义了无限大的二维重复单元阵列高分子量分子。所得到的润滑剂具有比石墨，MoS2和一氟化碳更好的润滑性能。

80. 发明授权

US4695522A Aqueous battery with (C.sub.y F.sub.x Cl.sub.z).sub.n cathode 失效
标题翻译：带有（Cy Fx Clz）n阴极的水性电池
公开(公告)号：US4695522A
公开(公告)日：1987-09-22
申请号：US900280
申请日：1986-08-26
申请人： David Nalewajek , Jung T. Kim , Lynn E. McCurry
发明人： David Nalewajek , Jung T. Kim , Lynn E. McCurry
IPC分类号： H01M4/58 , H01M6/04
CPC分类号： H01M4/5835 , H01M6/04
摘要： A novel high energy density aqueous cell exhibiting superior electrochemical properties is described. The use of the novel cathode composition, (C.sub.y F.sub.x Cl.sub.z).sub.n, permits the construction of a novel high energy density aqueous cell comprised of an anode, an alkaline electrolyte and a cathode, said cathode comprised of carbon fluoride chloride of the type (C.sub.y F.sub.x Cl.sub.z).sub.n : wherein y is 1 or 2; x is greater than 0 up to about 1.2; z is greater than 0 up to 0.1; and n denotes an infinitely large two dimensional array of C.sub.y F.sub.x Cl.sub.z units.The carbon fluoride chloride is composed of carbon, fluorine and chlorine, wherein the carbon can be chosen from the group consisting of graphite, coke, needle coke, charcoal, activated carbon, carbon blacks and the like. The carbon fluoride chloride described herein can be made in several ways, e.g. carbon can be reacted with chlorine monofluoride, ClF, to produce (C.sub.y F.sub.x Cl.sub.z).sub.n or with mixtures of chlorine, Cl.sub.2, and fluorine, F.sub.2, to produce (C.sub.y F.sub.x Cl.sub.z).sub.n.
摘要翻译：描述了一种具有优异电化学特性的新型高能密度水溶液电池。新型阴极组合物（CyFxClz）n的使用允许构建由阳极，碱性电解质和阴极组成的新型高能密度水溶液电池，所述阴极由（CyFxClz）n型碳氟化物：其中y为1或2; x大于0至约1.2; z大于0至0.1; n表示CyFxClz单位的无限大的二维阵列。碳氟化碳由碳，氟和氯组成，其中碳可选自石墨，焦炭，针状焦炭，活性碳，炭黑等。本文所述的氟化碳氟化物可以以几种方式制备，例如，碳可以与一氟化物ClF反应以产生（CyFxClz）n或与氯，Cl2和氟的混合物F2，以产生（CyFxClz）n。

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