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71. 发明授权

US5756691A Water--insoluble azo colorants based on N-acetoacetyldehydrothiotoluidine 失效
标题翻译：基于N-乙酰乙酰基脱硫硫代甲苯胺的水不溶性偶氮着色剂
公开(公告)号：US5756691A
公开(公告)日：1998-05-26
申请号：US874961
申请日：1997-06-13
申请人： Joachim Weber , Hans Joachim Metz
发明人： Joachim Weber , Hans Joachim Metz
IPC分类号： C09B29/09 , C09B29/01 , C09B29/33 , C09B29/36 , C09D7/00 , C09D11/037 , G03G9/09 , C09B67/20 , C09D11/00 , D06P3/79
CPC分类号： C09D11/037 , C09B29/0003 , C09B29/337 , C09D7/007 , G03G9/091
摘要： Water-insoluble azo colorant based on N-acetoacetyldehydrothiotoluidine Compound of the formula (I) ##STR1## in which R.sub.1 and R.sub.2 independently of one another are a hydrogen atom, C.sub.1 -C.sub.4 -alkyl, C.sub.5 -C.sub.6 -cycloalkyl, a benzyl group, an unsubstituted phenyl group or a substituted phenyl group with 1 to 5, preferably 1 to 3, substituents from the group consisting of C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, halogen, nitro, cyano, hydroxyl, CF.sub.3, CONH.sub.2, CONH(C.sub.5 -C.sub.6 -cycloalkyl), CON(C.sub.1 -C.sub.4 -alkyl).sub.2, CONH(C.sub.1 -C.sub.4 -alkyl), COO(C.sub.1 -C.sub.4 -alkyl), COO(C.sub.5 -C.sub.6 -cycloalkyl) and CONH(phenyl), R.sub.3 is a hydrogen atom, C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, halogen, nitro, cyano, hydroxyl, CF.sub.3, COO(C.sub.1 -C.sub.4 -alkyl) or COO(C.sub.5 -C.sub.6 -cycloalkyl) and n is 1 or 2.
摘要翻译：基于N-乙酰乙酰基脱硫硫代甲苯胺的水不溶性偶氮着色剂，式（I）的化合物是氢原子，C1-C4烷基，C5-C6-环烷基，苄基，未取代的苯基或取代的苯基具有1至5个，优选1至3个取代基，由C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基，卤素，硝基，氰基，羟基，CF 3，CONH 2，CONH（C 5 -C 6环烷基），CON （C 1 -C 4 - 烷基）2，CONH（C 1 -C 4 - 烷基），COO（C 1 -C 4 - 烷基），COO（C 5 -C 6环烷基）和CONH（苯基），R 3是氢原子， - 烷基，C 1 -C 4 - 烷氧基，卤素，硝基，氰基，羟基，CF 3，COO（C 1 -C 4 - 烷基）或COO（C 5 -C 6环烷基），n为1或2。

72. 发明授权

US5747566A Water-insoluble azo colorants based on aminoquinazolinediones 失效
标题翻译：基于氨基喹唑啉的水不溶性偶氮着色剂
公开(公告)号：US5747566A
公开(公告)日：1998-05-05
申请号：US694162
申请日：1996-08-08
申请人： Joachim Weber
发明人： Joachim Weber
IPC分类号： C09B29/44 , C07D239/46 , C07D239/60 , C08K5/3442 , C08K5/3462 , C08K5/3465 , C08L23/00 , C09B29/00 , C09B29/036 , C09B29/36 , C09B29/52 , C09D5/03 , C09D5/46 , C09D7/00 , C09D11/037 , G03G9/09 , C08K5/3495 , C03C17/00 , C09D5/00
CPC分类号： C09D11/037 , C09B29/0051 , C09B29/3673 , C09D5/035 , C09D7/007 , G03G9/091
摘要： Compound of the general formula (I) ##STR1## in which X is an O or S atom or an imino group, Y is an O atom or an imino group, R.sub.1 and R.sub.2 are a hydrogen atom, C.sub.1 -C.sub.4 -alkyl, an unsubstituted phenyl group or a substituted phenyl group having 1 to 5 substituents from the group consisting of C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, halogen, nitro, cyano, hydroxyl, CF.sub.3, CONH.sub.2, CONH(C.sub.5 -C.sub.6 -cycloalkyl), CON(C.sub.1 -C.sub.4 -alkyl).sub.2, CONH(C.sub.1 -C.sub.4)-alkyl, COO(C.sub.1 -C.sub.4)-alkyl, COO(C.sub.5 -C.sub.6 -cycloalkyl) and CONH(phenyl), with the proviso that at least one of the radicals R.sub.1 or R.sub.2 has one of the meanings mentioned which differ from hydrogen, R.sub.3 is a hydrogen atom, a trifluoromethyl group, a halogen atom or a C.sub.1 -C.sub.4 -alkyl, a C.sub.1 -C.sub.4 -alkoxy, a nitro or a cyano group and R.sub.4 and R.sub.5 independently of one another are a hydrogen atom, C.sub.1 -C.sub.4 -alkyl, phenyl or a substituted phenyl group having 1 to 5 substituents from the group consisting of C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, halogen, nitro, cyano, hydroxyl, CF.sub.3, CONH.sub.2, CONH(C.sub.5 -C.sub.6 -cycloalkyl), CON(C.sub.1 -C.sub.4 -alkyl).sub.2, CONH(C.sub.1 -C.sub.4)-alkyl, COO(C.sub.1 -C.sub.4)-alkyl, COO(C.sub.5 -C.sub.6 -cycloalkyl) and CONH(phenyl).
摘要翻译： X为O或S原子或亚氨基的通式（I）的化合物，其中X为O原子或亚氨基，R 1和R 2为氢原子，C 1 -C 4 - 烷基，未取代的苯基或具有1至5个选自C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基，卤素，硝基，氰基，羟基，CF 3，CONH 2，CONH（C 5 -C 6）环烷基），CON（C 1 -C 4 - 烷基）2，CONH（C 1 -C 4） - 烷基，COO（C 1 -C 4） - 烷基，COO（C 5 -C 6环烷基）和CONH（苯基）基团R 1或R 2中的至少一个具有与氢不同的所述含义之一，R 3为氢原子，三氟甲基，卤素原子或C 1 -C 4烷基，C 1 -C 4 - 烷氧基，硝基或氰基，R 4和R 5彼此独立地是氢原子，C 1 -C 4 - 烷基，苯基或具有1至5个选自C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基的取代基的取代苯基，卤素，硝基，氰基，羟基，CF 3，CONH 2，CONH（C 5 -C 6环烷基），CON（C 1 -C 4-烷基）2，CONH（C 1 -C 4） - 烷基，COO（C 1 -C 4） - 烷基，COO（C 5 -C 6环烷基）和CONH（苯基）。

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