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61. 发明授权

US4547542A Sulfonated polymer and compositions thereof 失效
标题翻译：磺化聚合物及其组合物
公开(公告)号：US4547542A
公开(公告)日：1985-10-15
申请号：US564719
申请日：1983-12-23
申请人： Robert D. Lundberg , Warren A. Thaler
发明人： Robert D. Lundberg , Warren A. Thaler
IPC分类号： C08F8/36 , C08L23/32 , C08K5/09 , C08K5/21 , C08L51/08 , C08L81/08
CPC分类号： C08L23/32 , C08F8/36
摘要： This invention relates to unique and novel compositions based on chemically combining a sulfonated polymer and an amine terminated polylactone composition. The resulting amine neutralized sulfonated polymer compositions have a variety of uses including those as diverse as adhesive agents, thermoplastic elastomers, additive uses wherein these materials can be utilized to compatibilize two different polymers which are normally incompatible. These compositions can also be blended with fillers and/or oils when the sulfonated polymer is elastomeric. The materials display thermoplastic character.
摘要翻译：本发明涉及基于化学组合磺化聚合物和胺封端的聚内酯组合物的独特且新颖的组合物。所得胺中和的磺化聚合物组合物具有多种用途，包括各种用途，包括粘合剂，热塑性弹性体，添加剂用途，其中这些材料可用于使通常不相容的两种不同聚合物相容。当磺化聚合物是弹性体时，这些组合物也可与填料和/或油混合。材料显示热塑性。

62. 发明授权

US4480012A Contact adhesive and adhesive system for EPDM and related elastomers 失效
标题翻译：用于EPDM和相关弹性体的粘合剂和粘合剂系统
公开(公告)号：US4480012A
公开(公告)日：1984-10-30
申请号：US588848
申请日：1984-03-12
申请人： John W. Fieldhouse
发明人： John W. Fieldhouse
IPC分类号： C08G14/06 , C08J5/12 , C08L23/32 , C09J123/32 , C09J161/06 , C09J161/34 , B32B25/16 , B32B31/12
CPC分类号： C08J5/12 , C08G14/06 , C09J123/32 , C09J161/06 , C09J161/34 , C08J2323/16 , C08L23/32 , Y10T428/31877 , Y10T428/31931
摘要： An adhesive composition for bonding cured layers of EPDM together is provided which comprises a neutralized sulfonated EPDM elastomeric terpolymer, an organic hydrocarbon solvent or mixture of an organic hydrocarbon solvent and an aliphatic alcohol, a para-alkylated phenol formaldehyde tackifying resin and an alkylphenol or ethoxylated alkylphenol. A method for bonding the cured layers of EPDM together utilizing the adhesive composition is also provided.
摘要翻译：提供一种用于将EPDM的固化层粘合在一起的粘合剂组合物，其包含中和的磺化EPDM弹性体三元共聚物，有机烃溶剂或有机烃溶剂和脂族醇的混合物，对烷基化酚醛增塑树脂和烷基酚或乙氧基化烷基酚。还提供了一种利用粘合剂组合物将EPDM的固化层粘合在一起的方法。

63. 发明授权

US4285851A Process for controlled gelation of polymeric solution (C-974) 失效
标题翻译：聚合溶液（C-974）的控制凝胶化方法
公开(公告)号：US4285851A
公开(公告)日：1981-08-25
申请号：US136834
申请日：1980-04-03
申请人： Henry S. Makowski , Robert D. Lundberg
发明人： Henry S. Makowski , Robert D. Lundberg
IPC分类号： C09D7/00 , C09D123/32 , C09J123/32 , C09K8/035 , C09K8/24 , C09K8/588 , C08L23/32
CPC分类号： C09K8/588 , C09D123/32 , C09D7/002 , C09J123/32 , C09K8/035 , C09K8/24 , C08L23/32 , Y10S260/31 , Y10S524/916
摘要： The present invention relates to a process for forming a polymeric solution or gel having a viscosity of at least about 50,000 cps which includes the steps of dissolving an amine terminated polyalkylene oxide neutralized sulfonated polymer in a solvent to form a polymeric solution, a concentration of the amine terminated polyalkylene oxide neutralized sulfonated polymer in the solution being about 0.1 to about 20 wt. %, a viscosity of the solution being less than about 20,000 cps; and adding about 1 to about 500 vol. % water to the polymeric solution having a viscosity less than about 20,000 cps, the water being immiscible with the solvent and the polymeric solution, the viscosity of said polymeric solution increasing rapidly upon the addition of said water from less than 20,000 cps to greater than 50,000 cps.
摘要翻译：本发明涉及形成具有至少约50,000cps的粘度的聚合物溶液或凝胶的方法，其包括将胺封端的聚亚烷基氧化物中和的磺化聚合物溶解在溶剂中以形成聚合物溶液的步骤，浓度为胺封端的聚环氧烷中和的磺化聚合物在溶液中为约0.1至约20wt。％，溶液的粘度小于约20,000cps; 并加入约1至约500体积％％的水溶于具有小于约20,000cps的粘度的聚合物溶液中，水与溶剂和聚合物溶液不混溶，所述聚合物溶液的粘度在将所述水从小于20,000cps加到大于50,000时迅速增加 cps。

64. 发明授权

US4162241A Polyvinyl chloride thermoplastic blend compositions having improved glass transition tempratures 失效
标题翻译：具有改进的玻璃化转变温度的聚氯乙烯热塑性共混组合物
公开(公告)号：US4162241A
公开(公告)日：1979-07-24
申请号：US787368
申请日：1977-04-14
申请人： Nathan H. Canter , Neville G. Thame
发明人： Nathan H. Canter , Neville G. Thame
IPC分类号： C08L23/32 , C08L27/06 , C08L23/16
CPC分类号： C08L27/06 , C08L23/32
摘要： This patent relates to thermoplastic blend compositions having improved stiffness and increased glass transition temperature, wherein a major portion of polar thermoplastic resin is compounded with a minor portion of a neutralized sulfonated polymer. The neutralized sulfonated polymers of the present invention included sulfonated polystyrene butadiene copolymers, sulfonated butyl rubber, sulfonated EPDM and other sulfonated elastomeric polymers. The thermoplastic polar resins having a halogen-carbon bond include polyvinyl chloride.
摘要翻译：该专利涉及具有改善的刚性和增加的玻璃化转变温度的热塑性共混组合物，其中极大的热塑性树脂的主要部分与少部分中和的磺化聚合物混合。本发明的中和磺化聚合物包括磺化聚苯乙烯丁二烯共聚物，磺化丁基橡胶，磺化EPDM和其它磺化弹性体聚合物。具有卤素 - 碳键的热塑性极性树脂包括聚氯乙烯。

65. 发明授权

US4151137A Blend compositions 失效
标题翻译：混合组合物
公开(公告)号：US4151137A
公开(公告)日：1979-04-24
申请号：US855728
申请日：1977-11-29
申请人： Ilan Duvdevani , Jan Bock
发明人： Ilan Duvdevani , Jan Bock
IPC分类号： C08L23/32 , C08L91/00
CPC分类号： C08L23/32 , Y10S260/31
摘要： This invention relates to injection moldable and extrusion type elastomeric compositions having a viscosity at 200.degree. C. at 0.73 sec.sup.-1 of less than about 8.times.10.sup.5 poises. The compositions used for elastomeric articles include 100 parts of a neutralized sulfonated EPDM terpolymer; less than about 200 parts per hundred of a paraffinic, low polarity process oil; about 25 to about 200 parts per hundred of an amorphous silica filler treated or untreated; and a preferential plasticizer at about less than 50 parts per hundred based on 100 parts of the sulfonated elastomeric polymer. The composition may also include a crystalline polyolefinic thermoplastic at less than about 100 parts per hundred by weight per 100 parts of sulfonated polymer.These blend compositions can be readily processed due to their superior rheological properties on conventional plastic fabrication equipment, especially on low and high pressure injection molding or extrusion equipment into elastomeric articles having excellent physical properties and desirable rubbery characteristics.
摘要翻译：本发明涉及在200℃，0.73秒-1时粘度小于约8×10 5泊的注射成型和挤压型弹性体组合物。用于弹性制品的组合物包括100份中和的磺化EPDM三元共聚物; 小于约200份/ 100份石蜡，低极性工艺油; 每百份无定形二氧化硅填料处理或未处理约25至约200份; 和基于100份磺化弹性体聚合物的约百分之50的优选增塑剂。该组合物还可以包含每100份磺化聚合物小于约100份/ 100重量份的结晶聚烯烃热塑性塑料。

66. 发明授权

US2719139A Polyvinyl chloride-polysulfone resin 失效
公开(公告)号：US2719139A
公开(公告)日：1955-09-27
申请号：US2719139D
IPC分类号： C08G75/22 , C08L27/06 , C08L81/06
CPC分类号： C08L27/06 , C08G75/22 , C08L81/06 , C08L23/32 , C08L2666/14 , C08L2666/04

67. 发明公开

KR1020160079366A 비할로겐계 난연성 폴리프로필렌 수지의 제조방법, 이에 의해 제조된 폴리프로필렌 수지 및 이를 포함하는 난연성 고분자 수지 조성물 有权
标题翻译：非卤化物阻燃剂聚丙烯树脂，其制备的聚丙烯树脂及其阻燃聚合物树脂组合物的制备方法
公开(公告)号：KR1020160079366A
公开(公告)日：2016-07-06
申请号：KR1020140190625
申请日：2014-12-26
申请人： 경북대학교 산학협력단
发明人： 김한도 , 김민관
IPC分类号： C08F8/40 , C08F10/06 , C08L23/32
CPC分类号： C08F8/40 , C08F10/06 , C08L23/32 , C08L2201/02 , C08L2201/22 , C08L2666/84
摘要： 본발명은난연성폴리프로필렌(Flame retardant polypropylene, FRPP) 수지의제조에관한것으로, 상세하게는비할로겐계난연성폴리프로필렌수지의제조방법, 이에의하여제조되는난연성폴리프로필렌수지및 이를포함하는난연성고분자수지조성물에관한것이다. 본발명에따르면, 유기용매에말레익무수물이그라프트된폴리프로필렌수지를용해시킨후, 염기성반응촉매를투입하여, 상기그라프트된말레익무수물을숙신산으로전환시켜, 숙신산으로관능화된폴리프로필렌수지용액을제조하는제1 단계; 및상기폴리프로필렌수지용액에라디칼계반응촉매및 인계난연제를첨가하여라디칼부가반응을시킴으로써, 인계난연제가부가결합된폴리프로필렌수지를제조하는제2 단계를포함하는것을특징으로하는, 인계난연제가공유결합된비할로겐계난연성폴리프로필렌수지의제조방법이개시된다.
摘要翻译：本发明涉及非卤素阻燃聚丙烯（FRPP）树脂的制备。特别地，本发明涉及一种制备非卤素FRPP树脂，由此制备的FRPP树脂的方法和包含该FRPP树脂的阻燃聚合物树脂组合物。根据本发明，公开了一种制备磷基阻燃剂共价结合的非卤素FRPP树脂的方法，包括以下步骤：将接枝有马来酸酐的聚丙烯树脂溶解在有机溶剂中，引入碱性反应催化剂以将接枝的马来酸酐转化成琥珀酸，从而提供琥珀酸官能化的聚丙烯树脂溶液; 并向聚丙烯树脂溶液中添加自由基反应催化剂和磷系阻燃剂进行自由基添加，由此提供通过添加与磷系阻燃剂结合的聚丙烯树脂。

68. 发明授权

KR101443375B1 부틸 고무 이오노머 나노복합물 有权
标题翻译：丁基橡胶离子纳米复合材料
公开(公告)号：KR101443375B1
公开(公告)日：2014-09-24
申请号：KR1020070107020
申请日：2007-10-24
申请人： 아란세오 캐나다 인코퍼레이티드
发明人： 레센데스,뤼 , 앳키슨,다나
IPC分类号： C08L9/00 , C08K7/00
CPC分类号： C08F210/12 , C08L23/32 , C08L91/00 , C08L2312/00 , C08L91/06 , C08F236/08
摘要： 본 발명은 다중올레핀 단량체(예: 이소프렌)로부터 유도된 반복 단위 3.5 몰％ 이상을 갖는 부틸 고무 이오노머를 포함하는 나노복합물 및 그의 제조 방법에 관한 것이다. 더 구체적으로, 본 발명은 고 종횡비의 충전제를 포함하는 부틸 고무 이오노머 나노복합물에 관한 것이다. 본 발명의 하나의 바람직한 양상에서, 나노복합물은 나노복합물을 형성하는 동안 동일 반응계내 생성되는 이오노머를 포함하여, 이오노머에 나노복합물이 삽입된다. 본 발명에 따른 나노복합물은 통상적인 브롬화 부틸 고무를 사용하여 제조된 종래 기술의 나노복합물에 비하여 개선된 불투과성 및 인장 특성을 나타낸다.
나노복합물, 부틸 고무, 이오노머, 종횡비

69. 发明授权

US09193680B2 Method for the preparation of poly(disulfide) polymers and gels 有权
标题翻译：制备聚（二硫化物）聚合物和凝胶的方法
公开(公告)号：US09193680B2
公开(公告)日：2015-11-24
申请号：US14016511
申请日：2013-09-03
申请人： Judit E. Puskas , Emily Q. Rosenthall
发明人： Judit E. Puskas , Emily Q. Rosenthall
IPC分类号： C08G75/14 , C08G75/04 , C07C321/04 , C07C323/52 , C08F8/34 , C08G63/688 , C08G63/87 , C08G75/12 , C08L23/32 , C08L81/02 , C08F6/06 , C08F8/06 , C08J3/03 , C08J3/05
CPC分类号： C07C321/04 , C07C323/52 , C08F8/34 , C08G63/688 , C08G63/87 , C08G75/04 , C08G75/12 , C08L23/32 , C08L81/02
摘要： High molecular weight disulfide polymers are synthesized in aqueous media by exposing dithiol compounds to a mild oxidizing environment in the presence of a tertiary amine catalyst. The unique oxidizing system polymerizes monomers through the formation of sulfur-sulfur bonds between dithiol compounds. The same oxidizing system may be used to make disulfide-crosslinked gels from compounds containing multiple thiol groups. The oxidizing system is comprised of oxygen at atmospheric concentration and dilute hydrogen peroxide. A filler such as carbon black may be incorporated into the polymer or cross-linked gel during polymerization. A polydisulfide polymer is provided having a weight average molecular weight of greater than about 100,000 g/mol and a polydispersity index of about 2 or less. A tetrathiol composition results from a reaction of a diacrylate with a trithiol. The tetrathiol composition may be subjected to an oxidizing environment with a tertiary amine catalyst to provide a polytetrathiol polymer network.
摘要翻译：通过在叔胺催化剂存在下将二硫醇化合物暴露于温和的氧化环境下，在水性介质中合成高分子量二硫化物聚合物。独特的氧化体系通过在二硫醇化合物之间形成硫 - 硫键聚合单体。可以使用相同的氧化体系从含有多个硫醇基的化合物制备二硫键交联的凝胶。氧化系统由大气浓度的氧和稀释的过氧化氢组成。在聚合过程中，可以在聚合物或交联凝胶中引入填充剂如炭黑。提供重均分子量大于约100,000g / mol且多分散指数为约2或更小的聚二硫化物聚合物。四硫醇组合物来自二丙烯酸酯与三硫醇的反应。四硫醇组合物可以用叔胺催化剂进行氧化环境以提供聚四硫醇聚合物网络。

70. 发明申请

US20140066589A1 Method For The Preparation of Poly(Disulfide) Polymers and Gels 有权
标题翻译：聚（二硫化物）聚合物和凝胶的制备方法
公开(公告)号：US20140066589A1
公开(公告)日：2014-03-06
申请号：US14016511
申请日：2013-09-03
申请人： Judit E. Puskas , Emily Q. Rosenthall
发明人： Judit E. Puskas , Emily Q. Rosenthall
IPC分类号： C08G75/12 , C07C321/04
CPC分类号： C07C321/04 , C07C323/52 , C08F8/34 , C08G63/688 , C08G63/87 , C08G75/04 , C08G75/12 , C08L23/32 , C08L81/02
摘要： High molecular weight disulfide polymers are synthesized in aqueous media by exposing dithiol compounds to a mild oxidizing environment in the presence of a tertiary amine catalyst. The unique oxidizing system polymerizes monomers through the formation of sulfur-sulfur bonds between dithiol compounds. The same oxidizing system may be used to make disulfide-crosslinked gels from compounds containing multiple thiol groups. The oxidizing system is comprised of oxygen at atmospheric concentration and dilute hydrogen peroxide. A filler such as carbon black may be incorporated into the polymer or cross-linked gel during polymerization. A polydisulfide polymer is provided having a weight average molecular weight of greater than about 100,000 g/mol and a polydispersity index of about 2 or less. A tetrathiol composition results from a reaction of a diacrylate with a trithiol. The tetrathiol composition may be subjected to an oxidizing environment with a tertiary amine catalyst to provide a polytetrathiol polymer network.
摘要翻译：通过在叔胺催化剂存在下将二硫醇化合物暴露于温和的氧化环境下，在水性介质中合成高分子量二硫化物聚合物。独特的氧化体系通过在二硫醇化合物之间形成硫 - 硫键聚合单体。可以使用相同的氧化体系从含有多个硫醇基的化合物制备二硫键交联的凝胶。氧化系统由大气浓度的氧和稀释的过氧化氢组成。在聚合过程中，可以在聚合物或交联凝胶中引入填充剂如炭黑。提供重均分子量大于约100,000g / mol且多分散指数为约2或更小的聚二硫化物聚合物。四硫醇组合物来自二丙烯酸酯与三硫醇的反应。四硫醇组合物可以用叔胺催化剂进行氧化环境以提供聚四硫醇聚合物网络。

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