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    • 63. 发明申请
    • PRODUCTION OF SELENIUM-72 AND ARSENIC-72
    • 硒-72和ARSENIC-72的生产
    • WO1993004768A1
    • 1993-03-18
    • PCT/US1992007347
    • 1992-09-04
    • UNITED STATES DEPARTMENT OF ENERGY
    • UNITED STATES DEPARTMENT OF ENERGYPHILLIPS, Dennis, Ray
    • B01D59/00
    • G21G4/08G21G2001/0026Y10S423/07
    • Methods and apparatus for producing selenium-72, separating it from its daughter isotope arsenic-72, and generating multiple portions of a solution containing arsenic-72 from a reusable parent substance comprised of selenium-72. The invention provides apparatus which can be located at a site where arsenic-72 is used, for purposes such as PET imaging, to produce arsenic-72 as needed, since the half-life of arsenic-72 is very short. A solution containing arsenic-72 is placed into reactor (100). Hydrazine dihydrochloride and a carrier comprised of selenium are added through additive funnel (103) and conduit (102). The contents of reactor (100) are heated by electrical heating jacket (106). After reaction, the material in reactor (100) is passed to separation means (101), where the solution containing As-72 is separated from the solid comprised of Se-72. The solution is returned to reactor (100) by means of conduit (112). Product solution is treated to remove hydrazinium ion and then removed from reactor (100) by means of conduit (110). An HCl/H2O2 solution is then heated in reactor (100) and circulated through filter means (101) in order to dissolve the precipitated Se. This solution is removed through conduit (110) and is stored to allow As-72 to grow-in and H2O2 to decompose.
    • 67. 发明申请
    • OXIDATION OF GALLIUM ARSENIDE
    • 氧化阿魏酸钠的氧化
    • WO1992009108A1
    • 1992-05-29
    • PCT/US1991007941
    • 1991-11-01
    • UNITED STATES DEPARTMENT OF ENERGY
    • UNITED STATES DEPARTMENT OF ENERGYHOFFBAUER, Mark, A.CROSS, Jon, B.
    • H01L29/20
    • H01L21/31654
    • A compound material (34) is oxidized by exposing the surface of the material to a high kinetic energy beam (32) of atomic oxygen. In particular, GaAs has been oxidized at room temperature by exposure to a 2.8 eV beam of atomic oxygen. Oxide layers of 300-500 ANGSTROM have been produced with no evidence of elemental As in the oxide layer or at the interface with the GaAs substrate. The oxide is of uniform Ga/As stoichiometry with complete oxidation of the Ga and As. The layer has been shown to passivate the GaAs surface, to be insulating, and to form a capacitor with an overlying layer. These characteristics indicate that discrete electronic components may be formed using the properties of the GaAs oxide layer formed herein.
    • 复合材料(34)通过将材料的表面暴露于原子氧的高动能束(32)而被氧化。 特别地,GaAs通过暴露于2.8eV的原子氧束在室温下被氧化。 已经生产了300-500安培的氧化层,没有在氧化物层或与GaAs衬底的界面处有元素As的迹象。 氧化物具有Ga / As均匀的化学计量,完全氧化Ga和As。 该层已经显示为钝化GaAs表面,被绝缘,并形成具有上覆层的电容器。 这些特征表明可以使用本文形成的GaAs氧化物层的性质来形成分立的电子部件。
    • 70. 发明申请
    • COAL BENEFICIATION AND UTILIZATION PROCESS
    • 煤炭利益和利用过程
    • WO1991006618A1
    • 1991-05-16
    • PCT/US1990006224
    • 1990-11-02
    • UNITED STATES DEPARTMENT OF ENERGY
    • UNITED STATES DEPARTMENT OF ENERGYHUCKO, Richard, Edmond
    • C10L10/00
    • B03B5/442C10L9/00C10L9/10
    • A method of beneficiating a particulate carbonaceous material such as coal, including formation of a slurry of the material in an aqueous salt solution. The slurry is separated in a cyclone into a low-density fraction and a high-density fraction with the low-density fraction having particulate carbonaceous material with a lower sulfur content and lower ash content than the particulate carbonaceous material in the high-density fraction. The particulate carbonaceous material with a lower sulfur content and lower ash content is separated from the low-density fraction but a residue of the aqueous salt solution is left thereon. The separated particulate carbonaceous material with a residual portion of the salt is used as a fuel in a process producing carbonaceous gases with at least a portion of the lower sulfur content gettered in solid form by the residual salt or further lowered in a process producing superclean coal. Potassium salts as well as calcium and nickel salts are disclosed.
    • 一种选择诸如煤的颗粒状碳质材料的方法,包括在盐水溶液中形成材料的浆料。 将浆料在旋风分离器中分离为低密度馏分和高密度馏分,其中低密度馏分具有颗粒状碳质材料,硫含量较低,灰分含量低于高密度馏分中的颗粒状碳质材料。 从低密度馏分中分离出具有较低硫含量和较低灰分含量的颗粒状碳质材料,但残留的盐水溶液残留在其上。 将具有残留盐的分离的颗粒状含碳材料用作生产含碳气体的方法中的燃料,其中至少一部分较低硫含量的固体形式被残留的盐吸收或在生产超清洁煤的方法中进一步降低 。 公开了钾盐以及钙和镍盐。