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61. 发明授权

US06284843B1 Fluorochemical oligomer and use thereof 有权
公开(公告)号：US06284843B1
公开(公告)日：2001-09-04
申请号：US09677396
申请日：2000-09-29
申请人： Chetan P. Jariwala , Thomas P. Klun
发明人： Chetan P. Jariwala , Thomas P. Klun
IPC分类号： C08F25908
CPC分类号： C08K5/435 , C07C323/52 , C08L101/00 , Y10T428/3154 , C08L2666/04
摘要： The present invention provides a novel fluorochemical oligomer, and polymer composition comprising the fluorochemical oligomeric compound and a thermoplastic or thermoset polymer. The polymer composition is useful in preparing shaped articles such as fibers and films which have desirable oil- and water repellency properties.

62. 发明授权

US6127485A High temperature-stable fluorochemicals as hydrophobic and oleophobic additives to synthetic organic polymers 失效
标题翻译：高温稳定的含氟化合物作为合成有机聚合物的疏水和疏油添加剂
公开(公告)号：US6127485A
公开(公告)日：2000-10-03
申请号：US901363
申请日：1997-07-28
申请人： Thomas P. Klun , Alton J. Gasper , John A. Temperante
发明人： Thomas P. Klun , Alton J. Gasper , John A. Temperante
IPC分类号： B32B5/26 , C08J5/18 , C08J9/36 , C08K5/10 , C08K5/20 , D01F1/10 , D04H1/42 , D04H3/16 , C08F5/02 , B32B27/00 , C08F14/18 , C08F27/12
CPC分类号： D01F1/10 , C08J5/18 , Y10T428/29 , Y10T428/2913 , Y10T428/2915 , Y10T428/2967 , Y10T428/2969
摘要： This invention describes hydrophobic and oleophobic fibers, films and molded articles comprising synthetic organic polymer wherein dispersed within the fiber, fabric or molded article and present at the surface of the fiber, fabric or molded article are fluorochemical compounds. Method of preparing such fibers, films and molded articles, as well as articles made therefrom also are disclosed.
摘要翻译：本发明描述了疏水和疏油纤维，包含合成有机聚合物的膜和模塑制品，其中分散在纤维，织物或模塑制品中并存在于纤维，织物或模塑制品的表面是含氟化合物。还公开了制备这种纤维，膜和模制品以及由其制成的制品的方法。

63. 发明授权

US5628952A Precisely shaped particles and method of making the same 失效
标题翻译：精确成型的颗粒及其制造方法
公开(公告)号：US5628952A
公开(公告)日：1997-05-13
申请号：US668786
申请日：1996-06-24
申请人： Gary L. Holmes , Scott R. Culler , David H. Hardy , William A. Hendrickson , Thomas P. Klun , Kimberly K. Harmon , Robert V. Heiti , Kathryn M. Spurgeon , Charles J. Studiner, III
发明人： Gary L. Holmes , Scott R. Culler , David H. Hardy , William A. Hendrickson , Thomas P. Klun , Kimberly K. Harmon , Robert V. Heiti , Kathryn M. Spurgeon , Charles J. Studiner, III
IPC分类号： B24D3/00 , B24D3/28 , B24D11/00 , B24D18/00 , C09K3/14 , D06N7/04 , C08J5/00
CPC分类号： B24D18/00 , B24D11/00 , B24D3/28 , C09K3/1409 , Y10T428/24372 , Y10T428/2438 , Y10T428/24405 , Y10T428/24413 , Y10T428/24421 , Y10T428/2982 , Y10T428/2991 , Y10T428/2998 , Y10T442/198 , Y10T442/2115
摘要： Precisely shaped composites and methods for making these composites are disclosed. The method of this invention comprises the steps of:(a) providing a production tool comprising a plurality of cavities;(b) providing a dispensing means capable of introducing a binder precursor comprising a thermosetting resin into the cavities;(c) providing a means, for at least partially curing the binder precursor;(d) introducing said binder precursor into at least a portion of at least two of the cavities;(e) continuously moving the production tool through a curing zone to at least partially cure the binder precursor;(f) removing the solidified binder from the production tool; and(g) converting the solidified binderinto precisely shaped composites. Steps (f) and (g) can be conducted simultaneously. The composites can be bonded together to form a shaped mass, e.g., a wheel; alternatively, the composites can be bonded to a backing to form a coated abrasive article; or the composites can be bonded into a fibrous, nonwoven substrate to form a non-woven abrasive article.
摘要翻译：公开了精确成型的复合材料和制备这些复合材料的方法。本发明的方法包括以下步骤：（a）提供包括多个空腔的生产工具; （b）提供能够将包含热固性树脂的粘合剂前体引入所述空腔中的分配装置; （c）提供用于至少部分固化粘合剂前体的装置; （d）将所述粘合剂前体引入至少两个空腔的至少一部分中; （e）连续移动生产工具通过固化区至少部分固化粘合剂前体; （f）从生产工具中去除固化的粘合剂; 和（g）将固化的粘合剂转化成精确成型的复合材料。步骤（f）和（g）可以同时进行。复合材料可以结合在一起以形成成形块，例如轮; 或者，复合材料可以结合到背衬以形成涂覆的磨料制品; 或者复合材料可以结合到纤维状非织造基材中以形成无纺布磨料制品。

64. 发明授权

US5549962A Precisely shaped particles and method of making the same 失效
标题翻译：精确成型的颗粒及其制造方法
公开(公告)号：US5549962A
公开(公告)日：1996-08-27
申请号：US085638
申请日：1993-06-30
申请人： Gary L. Holmes , Scott R. Culler , David H. Hardy , Kimberly K. Harmon , Robert V. Heiti , William A. Hendrickson , Thomas P. Klun , Kathryn M. Spurgeon , Charles J. Studiner, III
发明人： Gary L. Holmes , Scott R. Culler , David H. Hardy , Kimberly K. Harmon , Robert V. Heiti , William A. Hendrickson , Thomas P. Klun , Kathryn M. Spurgeon , Charles J. Studiner, III
IPC分类号： B24D3/00 , B24D3/28 , B24D11/00 , B24D18/00 , C09K3/14 , D06N7/04
CPC分类号： B24D18/00 , B24D11/00 , B24D3/28 , C09K3/1409 , Y10T428/24372 , Y10T428/2438 , Y10T428/24405 , Y10T428/24413 , Y10T428/24421 , Y10T428/2982 , Y10T428/2991 , Y10T428/2998 , Y10T442/198 , Y10T442/2115
摘要： A coated abrasive article comprising:(a) a backing;(b) at least one layer comprising a plurality of precisely shaped abrasive particles that comprise abrasive grits and a free-radically polymerized binder, wherein said precisely shaped particles have vertexes and(c) a bonding medium which serves to adhere said precisely shaped particles to said backing;wherein the precisely shaped particles are randomly disposed on the backing such that at least a portion of said particles are oriented with said vertexes pointing toward said backing.
摘要翻译：一种涂覆的磨料制品，包括：（a）背衬; （b）至少一层包括多个精确成形的磨料颗粒，其包含磨粒和自由基聚合的粘合剂，其中所述精确成形的颗粒具有顶点和（c）粘合介质，其用于将所述精确成形的颗粒粘附到说支持其中所述精确成形的颗粒被随机地设置在所述背衬上，使得所述颗粒的至少一部分被定向成使所述顶点指向所述背衬。

65. 发明授权

US09777407B2 Hydrophilic polyproylene melt additives 有权
公开(公告)号：US09777407B2
公开(公告)日：2017-10-03
申请号：US13260589
申请日：2010-03-25
申请人： Matthew T. Scholz , Michael R. Berrigan , Thomas P. Klun
发明人： Matthew T. Scholz , Michael R. Berrigan , Thomas P. Klun
IPC分类号： D01F6/06 , A61L15/24 , A61L15/48 , A61L31/04 , A61L31/14 , D01F1/10
CPC分类号： D01F6/06 , A61L15/24 , A61L15/48 , A61L31/048 , A61L31/14 , D01F1/10 , C08L23/00
摘要： Melt additive ionic and non-ionic surfactants to impart stable durable hydrophilicity to thermoplastic polymers or blends thereof.

66. 发明授权

US08816029B2 Compositions and articles comprising polymerizable ionic liquid mixture, and methods of curing 有权
标题翻译：包含可聚合离子液体混合物的组合物和制品以及固化方法
公开(公告)号：US08816029B2
公开(公告)日：2014-08-26
申请号：US13380267
申请日：2010-08-26
申请人： Yizhong Wang , Joel D. Oxman , Larry R. Krepski , Peiwang Zhu , Kevin M. Lewandowski , Brian N. Holmes , Richard L. Severance , Joseph D. Rule , Thomas P. Klun
发明人： Yizhong Wang , Joel D. Oxman , Larry R. Krepski , Peiwang Zhu , Kevin M. Lewandowski , Brian N. Holmes , Richard L. Severance , Joseph D. Rule , Thomas P. Klun
IPC分类号： C08F26/00 , C08F12/30 , C08F118/02 , A61K6/00
CPC分类号： C08F28/02 , A61K6/083 , C07D233/58 , C07D233/60 , C07D233/61 , C08F22/22 , C08F26/02 , C08K5/3445 , C09D4/06 , C09D133/066 , C09D139/00 , C09D141/00 , Y10T428/31725 , Y10T428/31786 , Y10T428/31935
摘要： Presently described are curable compositions comprising a mixture of at least one (e.g. free-radically) polymerizable ionic liquid and at least one other ethylenically unsaturated monomer, oligomer, or polymer. The polymerizable ionic liquid is characterized as having an air to nitrogen curing exotherm ratio of at least 0.70. Also described are articles and methods of making articles from such curable compositions. A monofunctional polymerizable ionic liquid is also described comprising a non-polymerizable substituted imidazolium cationic group and a polymerizable sulfonate anion.
摘要翻译：目前描述的是包含至少一种（例如自由基）可聚合离子液体和至少一种其它烯属不饱和单体，低聚物或聚合物的混合物的可固化组合物。可聚合离子液体的特征在于具有至少0.70的空气至氮固化放热比。还描述了从这种可固化组合物制备制品的制品和方法。还描述了单官能可聚合离子液体，其包含不可聚合的取代的咪唑鎓阳离子基团和可聚合的磺酸根阴离子。

67. 发明授权

US08383694B2 Polymerizable composition comprising perfluoropolyether material having ethylene oxide repeat unit segment 有权
公开(公告)号：US08383694B2
公开(公告)日：2013-02-26
申请号：US13396158
申请日：2012-02-14
申请人： Thomas P. Klun , Richard J. Pokorny , Joan M. Noyola
发明人： Thomas P. Klun , Richard J. Pokorny , Joan M. Noyola
IPC分类号： C08G18/67
CPC分类号： C08G18/2885 , C08G18/283 , C08G18/672 , C08G18/73 , C09D175/16 , G02B1/105 , G02B1/14 , Y10T428/31507 , Y10T428/31511 , Y10T428/3154 , Y10T428/31544 , Y10T428/31547 , Y10T428/31551 , Y10T428/31786
摘要： Presently is described a free-radically polymerizable composition comprising a mixture of reaction products of i) at least one polyisocyanate; ii) at least one isocyanate reactive perfluoropolyether compound; iii) at least one isocyanate reactive compound comprising greater than 6 repeat units of ethylene oxide; and iv) at least one isocyanate reactive non-fluorinated crosslinker comprising at least two free-radically polymerizable groups.

68. 发明申请

US20130004773A1 POLYMERIZABLE COMPOSITION COMPRISING PERFLUOROPOLYETHER MATERIAL HAVING ETHYLENE OXIDE REPEAT UNIT SEGMENT 有权
标题翻译：包含具有乙烯氧化物重复单元部分的全氟聚醚材料的可聚合组合物
公开(公告)号：US20130004773A1
公开(公告)日：2013-01-03
申请号：US13615688
申请日：2012-09-14
申请人： Thomas P. Klun , Richard J. Pokorny , Joan M. Noyola
发明人： Thomas P. Klun , Richard J. Pokorny , Joan M. Noyola
IPC分类号： B32B27/08 , B32B5/02 , B32B27/34 , B32B27/30 , B32B27/40 , B32B27/36
CPC分类号： C08G18/2885 , C08G18/283 , C08G18/672 , C08G18/73 , C09D175/16 , G02B1/105 , G02B1/14 , Y10T428/31507 , Y10T428/31511 , Y10T428/3154 , Y10T428/31544 , Y10T428/31547 , Y10T428/31551 , Y10T428/31786
摘要： Presently is described a free-radically polymerizable composition comprising a mixture of reaction products of i) at least one polyisocyanate; ii) at least one isocyanate reactive perfluoropolyether compound; iii) at least one isocyanate reactive compound comprising greater than 6 repeat units of ethylene oxide; and iv) at least one isocyanate reactive non-fluorinated crosslinker comprising at least two free-radically polymerizable groups.
摘要翻译：本发明描述了一种可自由基聚合的组合物，其包含i）至少一种多异氰酸酯的反应产物的混合物; ii）至少一种异氰酸酯反应性全氟聚醚化合物; iii）至少一种包含大于6个重复单元的环氧乙烷的异氰酸酯反应性化合物; 和iv）至少一种包含至少两个可自由基聚合的基团的异氰酸酯反应性非氟化交联剂。

69. 发明授权

US08329830B2 Surface treatment process and treated article 有权
标题翻译：表面处理工艺和处理制品
公开(公告)号：US08329830B2
公开(公告)日：2012-12-11
申请号：US12792153
申请日：2010-06-02
申请人： Yu Yang , George G. I. Moore , Thomas P. Klun
发明人： Yu Yang , George G. I. Moore , Thomas P. Klun
IPC分类号： C08F283/00 , C08G77/62
CPC分类号： C08L83/04 , B05D3/0254 , B05D5/083 , B05D2202/25 , C08G77/24 , C08G77/62 , C08L83/16 , C08L83/00
摘要： A surface treatment process comprises (a) providing at least one substrate having at least one major surface; (b) combining (1) at least one curable oligomeric or polymeric polysilazane comprising at least one chemically reactive site, and (2) at least one fluorochemical compound comprising (i) at least one organofluorine or heteroorganofluorine moiety that comprises at least about six perfluorinated carbon atoms, and (ii) at least one functional group that is capable of reacting with the polysilazane through at least one of the chemically reactive sites; (c) allowing or inducing the polysilazane and the fluorochemical compound to react to form at least one curable organofluorine-modified polysilazane; (d) applying the curable organofluorine-modified polysilazane or its precursors to at least a portion of at least one major surface of the substrate; and (e) curing the curable organofluorine-modified polysilazane to form a surface treatment.
摘要翻译：表面处理方法包括（a）提供至少一个具有至少一个主表面的基材; （b）组合（1）包含至少一个化学反应位点的至少一种可固化的低聚或聚合的聚硅氮烷，和（2）至少一种含氟化合物，其包含（i）至少一种有机氟或杂有机氟部分，其包含至少约六个全氟化碳原子，和（ii）能够通过至少一个化学反应性位点与聚硅氮烷反应的至少一个官能团; （c）允许或诱导聚硅氮烷和含氟化合物反应以形成至少一种可固化的有机氟改性的聚硅氮烷; （d）将可固化的有机氟改性的聚硅氮烷或其前体施加到基材的至少一个主表面的至少一部分上; 和（e）固化可固化的有机氟改性聚硅氮烷以形成表面处理。

70. 发明申请

US20120270980A1 COATING COMPOSITIONS COMPRISING NON-IONIC SURFACTANT EXHIBITING REDUCED FINGERPRINT VISIBILITY 有权
标题翻译：包含非离子表面活性剂的涂料组合物展示降低指纹可视性
公开(公告)号：US20120270980A1
公开(公告)日：2012-10-25
申请号：US13526800
申请日：2012-06-19
申请人： Richard J. Pokorny , Thomas P. Klun , Christopher B. Walker, JR. , David B. Olson , Joan M. Noyola , Michelle L. Toy , Evan L. Schwartz
发明人： Richard J. Pokorny , Thomas P. Klun , Christopher B. Walker, JR. , David B. Olson , Joan M. Noyola , Michelle L. Toy , Evan L. Schwartz
IPC分类号： C09D175/16 , C08K5/06 , C08K5/103 , C08F20/06
CPC分类号： C09D5/1618 , C08F220/34 , C08F2222/1026 , C08G18/283 , C08G18/5015 , C08G18/8116 , C09D4/06 , C09D7/63 , C08F2220/346 , C08F220/24 , C08F220/40 , C08F220/20
摘要： Presently described are coating compositions comprising a polymerizable resin composition and a non-ionic unpolymerizable surfactant. In some embodiments, the coating comprises greater than 10 wt-% of non-ionic unpolymerizable surfactant. In other embodiments, the coating composition comprises an an additive comprising a silicone group or a fluorinated group and a hydrophobic group. Also described are articles comprising the cured coating compositions. In one embodiment, an article is described comprising a cured coating wherein the cured coating exhibits a property of an initially visible simulated fingerprint reducing in visibility in 1-20 minutes. Also described is a method of determining the fingerprint visibility of a coating composition and a polyacylate composition useful as an additive. In another embodiment a coated surface is described comprising a polymeric organic material comprising a plurality of pores wherein a portion of the pores are interconnected and comprise a lipophilic liquid.
摘要翻译：目前描述的是包含可聚合树脂组合物和非离子不可聚合表面活性剂的涂料组合物。在一些实施方案中，涂层包含大于10重量％的非离子不可聚合表面活性剂。在其它实施方案中，涂料组合物包含包含硅氧烷基团或氟化基团和疏水基团的添加剂。还描述了包含固化的涂料组合物的制品。在一个实施方案中，描述了包含固化涂层的制品，其中固化的涂层表现出在1-20分钟内可见度的最初可见的模拟指纹的性质降低。还描述了确定涂料组合物和可用作添加剂的聚丙烯酸酯组合物的指纹可见性的方法。在另一个实施方案中，描述了涂覆的表面，其包括包含多个孔的聚合有机材料，其中一部分孔相互连接并且包含亲油性液体。

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