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61. 发明申请

US20050065272A1 Vinyl alcohol copolymers for use in aqueous dispersions and melt extruded articles 有权
标题翻译：用于水性分散体和熔融挤出制品的乙烯醇共聚物
公开(公告)号：US20050065272A1
公开(公告)日：2005-03-24
申请号：US10946970
申请日：2004-09-21
申请人： Richard Vicari
发明人： Richard Vicari
IPC分类号： C08F2/00 , C08F2/06 , C08F8/12 , C08F218/08 , C08F220/58
CPC分类号： C08F220/58 , C08F8/12 , C08F8/48 , C08F218/08 , C08F2800/20 , C08F8/28 , C08F216/06 , C08F2220/585
摘要： In a method of preparing an aqueous dispersion selected from drilling fluids, hydraulic cement compositions, mineral pigment containing coatings, and papermaking furnishes or in a method of preparing a melt extrudate, the improvement comprising: a) producing a copolymer of vinyl alcohol (VOH) and 2-acrylamido-2-methyl propane sulfonic acid or a salt of such acid (AMPS) by steps including continuously feeding with agitation, vinyl acetate (VAM) and AMPS as comonomers, a free radical yielding polymerization initiator, and a solvent for said comonomers, initiator, and copolymer resulting from the copolymerization of said comonomers, maintaining the resulting reaction mass in said first reaction zone under polymerization conditions for a residence time sufficient for a major proportion of AMPS fed to said first reaction zone to polymerize, continuously feeding reaction mass from said first reaction zone with an additional supply of AMPS to a second reaction zone, maintaining the reaction mass in the second reaction zone for a residence time sufficient to polymerize a major proportion of the AMPS added to the second reaction zone, continuously withdrawing reaction mass from the second reaction zone, separating copolymer of VAM and AMPS from the latter reaction mass, and saponifying by hydrolysis and/or alcoholysis a major proportion of the acetate groups in said copolymer to form a copolymer of VOH and AMPS; and b) incorporating the saponified copolymer into the aqueous dispersion or melt extrudate.
摘要翻译：在制备选自钻井液，水硬性水泥组合物，含矿物颜料的涂料和造纸配料的水性分散体的制备方法中，或在制备熔融挤出物的方法中，改进包括：a）制备乙烯醇（VOH）和2-丙烯酰胺基-2-甲基丙磺酸或这种酸的盐（AMPS），其中包括连续进料搅拌，乙酸乙烯酯（VAM）和AMPS作为共聚单体，产生自由基的聚合引发剂和用于所述由共聚单体的共聚产生的共聚单体，引发剂和共聚物，在聚合条件下将所得到的反应物质保持在所述第一反应区中，停留时间足以使进料至所述第一反应区的大部分AMPS聚合，连续进料反应质量从所述第一反应区与附加的AMPS供应到第二反应区，维持反应m 在第二反应区中的絮凝物的停留时间足以聚合添加到第二反应区中的主要部分的AMPS，连续地从第二反应区抽出反应物质，将VAM和AMPS的共聚物与后一反应物质分离，并皂化通过水解和/或醇解所述共聚物中主要部分的乙酸酯基团以形成VOH和AMPS的共聚物; 和b）将皂化的共聚物掺入水性分散体或熔融挤出物中。

62. 发明授权

US5464941A Biphenyl pyrazine compounds 失效
标题翻译：联苯吡嗪化合物
公开(公告)号：US5464941A
公开(公告)日：1995-11-07
申请号：US326103
申请日：1994-10-19
申请人： Richard Vicari , George Kvakovszky , Olan S. Fruchey , Hans J. Metz
发明人： Richard Vicari , George Kvakovszky , Olan S. Fruchey , Hans J. Metz
IPC分类号： C07D241/12 , C07D241/18 , C07D403/14 , C09B33/044 , C09B35/039 , C07C245/08 , C07D241/00 , C09B35/03
CPC分类号： C07D241/12 , C07D241/18 , C07D403/14 , C09B33/044 , C09B35/039
摘要： The present invention provides novel substituted biphenyl pyrazines or pyrazine derivatives ("BPD") which are functional and have useful application as a monomer for a variety of high performance polymers such as polyester, polyarylate, polycarbonate, polyetherketones, epoxides, polyimides, polyamides, and polyamides-imides; and as pigments for coating compositions such as paints. These BPD have the formula: ##STR1##
摘要翻译：本发明提供新的取代的联吡啶或吡嗪衍生物（“BPD”），它们是有用的，可用作各种高性能聚合物如聚酯，聚芳酯，聚碳酸酯，聚醚酮，环氧化物，聚酰亚胺，聚酰胺和聚酰胺酰亚胺以及用作涂料组合物如颜料的颜料。这些BPD具有以下公式：（I）

63. 发明授权

US5459266A Substituted pyrazines 失效
标题翻译：取代吡嗪
公开(公告)号：US5459266A
公开(公告)日：1995-10-17
申请号：US191848
申请日：1994-02-04
申请人： George Kvakovszky , Richard Vicari , Ahamed M. Tafesh , Kathleen N. Juneau , Olan S. Fruchey , Joseph A. McDonough , Debasish Kuila
发明人： George Kvakovszky , Richard Vicari , Ahamed M. Tafesh , Kathleen N. Juneau , Olan S. Fruchey , Joseph A. McDonough , Debasish Kuila
IPC分类号： C07D241/12 , C08G59/32 , C08G65/40 , C08G75/23 , C07D241/16 , C07D241/18 , C07D403/10
CPC分类号： C07D241/12 , C08G59/3245 , C08G65/4025 , C08G75/23
摘要： The present invention provides novel substituted pyrazines or pyrazine derivatives ("NPD") which are functional and have useful application as a monomer for a variety of high performance polymers such as polyester, polyarylate, polycarbonate, polyetherketones, epoxides, polyimides, polyamides, and polyamides-imides. These NPD have the general formula: ##STR1## wherein R.sub.1, R.sub.2, R.sub.3, and R.sub.4 are defined herein.
摘要翻译：本发明提供了新颖的取代吡嗪或吡嗪衍生物（“NPD”），它们是功能性的并且可用作各种高性能聚合物如聚酯，聚芳酯，聚碳酸酯，聚醚酮，环氧化物，聚酰亚胺，聚酰胺和聚酰胺的单体这些。这些NPD具有通式：其中R 1，R 2，R 3和R 4在本文中定义。

64. 发明授权

US5393860A Polymer compositions containing substituted pyrazines 失效
标题翻译：含有取代吡嗪的聚合物组合物
公开(公告)号：US5393860A
公开(公告)日：1995-02-28
申请号：US191682
申请日：1994-02-04
申请人： George Kvakovszky , Richard Vicari , Olan S. Fruchey , Ahmed M. Tafesh , Charles B. Hilton
发明人： George Kvakovszky , Richard Vicari , Olan S. Fruchey , Ahmed M. Tafesh , Charles B. Hilton
IPC分类号： C07D241/12 , C08G59/26 , C08G65/40 , C08G75/23 , C09K19/34
CPC分类号： C07D241/12 , C08G59/26 , C08G65/4037 , C08G75/23 , C09K19/3452 , C09K19/3472 , C09K19/348
摘要： The present invention provides new polymer compositions which contain novel substituted pyrazines or pyrazine derivatives ("NPD") which are functional and have useful application as a monomer (co-monomer) for a variety of high performance polymers such as polyester, polyarylate, polycarbonate, polyetherketones, epoxides, polyimides, polyamides, and polyamides-imides. These NPD have the general formula: ##STR1## wherein R.sub.1, R.sub.2, R.sub.3, and R.sub.4 are defined herein.
摘要翻译：本发明提供了新的聚合物组合物，其包含新的取代的吡嗪或吡嗪衍生物（“NPD”），它们是功能性的并且可用作单体（共聚单体），用于各种高性能聚合物如聚酯，聚芳酯，聚碳酸酯，聚醚酮，环氧化物，聚酰亚胺，聚酰胺和聚酰胺 - 酰亚胺。这些NPD具有通式：其中R 1，R 2，R 3和R 4在本文中定义。

65. 发明授权

US5362843A Process for preparing highly branched macromolecule polymers 失效
标题翻译：制备高支化高分子聚合物的方法
公开(公告)号：US5362843A
公开(公告)日：1994-11-08
申请号：US125441
申请日：1993-09-22
申请人： Richard Vicari , Michael P. Bodman
发明人： Richard Vicari , Michael P. Bodman
IPC分类号： C08G63/123 , C08G63/60 , C08G69/44 , C08G63/00
CPC分类号： C08G63/123 , C08G63/605 , C08G69/44
摘要： The present invention provides novel one-step processes for preparing highly branched macromolecule polymers that have highly controlled molecular architectures. The process comprise the reaction of a branching monomer such as a substituted phenyl compound having the formula: ##STR1## wherein R.sub.1, R.sub.2, and R.sub.3 are defined herein, with a second monomer (a core monomer) such as a dihydric phenol for a sufficient period of time and at a sufficient temperature to directly produce the highly branched polymer, characterized by having a single core, in a single processing step.
摘要翻译：本发明提供了制备具有高度可控的分子结构的高支化高分子聚合物的新颖的一步法。该方法包括将支化单体如具有下式的取代的苯基化合物（其中R1，R2和R3如本文所定义）与第二单体（核心单体）如二元酚反应足够的一段时间并在足够的温度下直接生产高度支化的聚合物，其特征在于在单一加工步骤中具有单个核心。

66. 发明授权

US5004796A Preparation of poly(arylate) using a non-solvent 失效
标题翻译：使用非溶剂制备聚（芳基化合物）
公开(公告)号：US5004796A
公开(公告)日：1991-04-02
申请号：US464395
申请日：1990-01-12
申请人： Richard Vicari , John R. Costanza , Ronald R. Lamonte , Ralph M. Miano
发明人： Richard Vicari , John R. Costanza , Ronald R. Lamonte , Ralph M. Miano
IPC分类号： C08G63/195 , C08G63/19 , C08G63/20 , C08G63/66 , C08G63/672 , C08G63/78 , C08G63/82 , C08G65/00 , C08G65/48
CPC分类号： C08G63/78 , C08G63/19 , C08G63/82
摘要： A polyarylate is formed by reacting a mixture of a diester of a dihydric phenol, at least one aromatic dicarboxylic acid and an inert diluent comprising a poly(fluorinated alkylene oxide). Polyarylates of improvided color can be formed and the diluent can be easily separated from the polyarylate and reaction byproducts.
摘要翻译：通过使二元酚的二酯，至少一种芳族二羧酸和包含聚（氟化环氧烷）的惰性稀释剂的混合物反应形成多芳基化合物。可以形成成色的多芳基化合物，并且稀释剂可以容易地从多芳基化合物和反应副产物中分离出来。

67. 发明授权

US4929694A Copolymers of p-mercaptostyrene and its esters 失效
标题翻译：对巯基苯乙烯及其酯的共聚物
公开(公告)号：US4929694A
公开(公告)日：1990-05-29
申请号：US348337
申请日：1989-05-04
申请人： Mohammad Aslam , Richard Vicari , Kenneth G. Davenport
发明人： Mohammad Aslam , Richard Vicari , Kenneth G. Davenport
IPC分类号： C08F20/02 , C08F22/36 , C08F212/00 , C08F212/14 , C08F222/00 , C08F222/02 , C08F222/06 , C08F222/40
CPC分类号： C08F212/14
摘要： There are provided novel copolymers of a p-mercaptostyrene ester, e.g., the acetate, with at least one comonomer selected from the group consisting of styrene, N-methylmaleimide, maleic anhydride and p-acetoxystyrene. These copolymers may be hydrolyzed to produce corresponding copolymers of p-mercaptostyrene with at least one comonomer selected from the group consisting of styrene, N-methylmaleimide, maleic acid and p-vinylphenol. The copolymers have application as heavy metal sequestering agents in various forms and structures.

68. 发明授权

US4927956A 3,5-disubstituted-4-acetoxystyrene and process for its production 失效
标题翻译： 3,5-二取代-4-乙酰氧基苯乙烯及其制备方法
公开(公告)号：US4927956A
公开(公告)日：1990-05-22
申请号：US360803
申请日：1989-06-02
申请人： Richard Vicari , Mohammad Aslam , Wilson B. Ray , Kenneth G. Davenport , Ralph Dammel , Juergen Lingnau , Karl-Friedrich Doessel
发明人： Richard Vicari , Mohammad Aslam , Wilson B. Ray , Kenneth G. Davenport , Ralph Dammel , Juergen Lingnau , Karl-Friedrich Doessel
IPC分类号： C07C39/373 , C07C45/54 , C07C45/63 , C07C49/825 , C07C69/157 , G03F7/038
CPC分类号： G03F7/038 , C07C39/373 , C07C45/54 , C07C45/63 , C07C49/825
摘要： 3-substituted-4-hydroxy- and 4-acetoxystyrene compounds, especially 3,5-di(methyl, bromo or chloro)-4-acetoxystyrene as well as a process for its preparation. 2,6-dimethylphenol is acylated with acetic anhydride and HF catalyzed to produce 3,5-dimethyl-4-hydroxy-acetophenone. After subsequent esterification with acetic anhydride and catalyzed hydrogenation to form 1-(3',5'-dimethyl-4'-acetoxyphenyl)ethanol, this intermediate is then dehydrated with an acid and a polymerization inhibitor to produce 3,5-dimethyl-4-acetoxystyrene.
摘要翻译： 3-取代-4-羟基 - 和4-乙酰氧基苯乙烯化合物，特别是3,5-二（甲基，溴或氯）-4-乙酰氧基苯乙烯以及其制备方法。 2,6-二甲基苯酚用乙酸酐进行酰化，HF催化反应生成3,5-二甲基-4-羟基苯乙酮。在用乙酸酐进行酯化和催化氢化后，形成1-（3'，5'-二甲基-4'-乙酰氧基苯基）乙醇，然后将该中间体用酸和阻聚剂脱水，得到3,5-二甲基-4 乙酰氧基苯乙烯

69. 发明授权

US4661611A Polyfunctional acylsilane crosslinking agents and photocrosslinking systems comprising the same 失效
标题翻译：多官能酰基硅烷交联剂和包含其的光交联体系
公开(公告)号：US4661611A
公开(公告)日：1987-04-28
申请号：US805537
申请日：1985-12-06
申请人： Subhash C. Narang , Richard Vicari , Juesheng Gu
发明人： Subhash C. Narang , Richard Vicari , Juesheng Gu
IPC分类号： C07F1/02 , C07F7/08 , C08K5/5415 , C08K5/544
CPC分类号： C07F7/0818 , C07F1/02 , C08K5/5415 , C08K5/544
摘要： Polyfunctional acyl silanes of the formula ##STR1## are disclosed as novel crosslinking agents. Composition and processes involving the same are also disclosed.
摘要翻译：公开了式（1）的多官能酰基硅烷作为新型交联剂。还公开了涉及其的组成和方法。

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