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61. 发明授权

US5731077A Self-lubricating device 失效
标题翻译：自润滑装置
公开(公告)号：US5731077A
公开(公告)日：1998-03-24
申请号：US458703
申请日：1995-06-02
申请人： Kazufumi Ogawa , Norihisa Mino , Mamoru Soga
发明人： Kazufumi Ogawa , Norihisa Mino , Mamoru Soga
IPC分类号： B05D1/18 , B05D5/08 , C09D4/00 , B32B9/04
CPC分类号： B82Y30/00 , B05D1/185 , B82Y40/00 , C09D4/00 , B05D5/08 , Y10T428/261 , Y10T428/266 , Y10T428/268 , Y10T428/31536 , Y10T428/31663
摘要： A chemically adsorbed film having a surface layer containing fluorine groups and a stem layer chemically bonded by siloxane bonds to a substrate is formed on the surface of a frictional portion of a machine part such as a gear or a bearing or on the surface of a game ball. An excellently self-lubricating low frictional resistance machine part or game ball thus can be obtained. A frictional portion of a gear or the like, made of SiO.sub.2 or like ceramic material, is dipped and held in a solution containing a surface active material, e.g., CF.sub.3 (CF.sub.2).sub.7 (CH.sub.2).sub.2 SiCl.sub.3 dissolved in a non-aqueous solvent. A hydrochloric acid removal reaction is brought about between SiCl groups of the material, which contains a fluorocarbon and a chlorosilane group, and hydroxyl groups numerously present on the SiO2 surface, thus forming bonds of CF.sub.3 (CF.sub.2).sub.7 (CH.sub.2).sub.2 Si(O--).sub.3 over the entire frictional portion surface. A fluorine-containing monomolecular film thus is formed, which is chemically bonded to the substrate and has a thickness of about 1.5 nm.
摘要翻译：在机械部件例如齿轮或轴承的摩擦部分的表面上或游戏表面上形成具有含氟基团的表面层和通过硅氧烷键合到基材上的茎层的化学吸附膜球。因此可以获得优异的自润滑低摩擦阻力机器部件或游戏球。将由SiO 2或类似陶瓷材料制成的齿轮等的摩擦部分浸渍并保持在含有溶解在非水溶剂中的表面活性物质例如CF 3（CF 2）7（CH 2）2 ClCl 3）的溶液中。在含有碳氟化合物和氯硅烷的材料的SiCl基团和SiO 2表面上大量存在的羟基之间产生盐酸去除反应，从而形成CF 3（CF 2）7（CH 2）2 Si（O - ）在整个摩擦部分表面上。因此，形成与基板化学键合并且具有约1.5nm的厚度的含氟单分子膜。

62. 发明授权

US5681442A Method of producing an organic device 失效
标题翻译：生产有机装置的方法
公开(公告)号：US5681442A
公开(公告)日：1997-10-28
申请号：US565636
申请日：1995-11-29
申请人： Kazufumi Ogawa , Norihisa Mino
发明人： Kazufumi Ogawa , Norihisa Mino
IPC分类号： H01L51/05 , C08F38/00 , H01L21/368 , H01L51/00 , H01L51/30 , C25D9/02
CPC分类号： H01L51/0075 , H01L51/0094 , H01L51/0545 , H01L51/0036 , H01L51/0062 , Y10S428/901 , Y10T428/24917
摘要： A process for producing an organic device includes forming a first electrode and a second electrode on a substrate having an insulating film formed on a surface thereof, etching out the insulating film with the first electrode and the second electrode being used as masks, forming a monomolecular or built-up monomolecular film containing electrolytically polymerizable unsaturated groups directly or indirectly on the surface of the substrate by a chemical absorption method or the Langmuir-Blodgett method. The process further includes a procedure of spreading a surfactant containing the electrolytically polymerizable unsaturated groups on the surface of a water bath to form a monomolecular film, transferring at least one layer of the monomolecular film into the surface of the substrate, and chemically bonding molecules of the surfactant to form at least one layer of the monomolecular film of the surfactant containing electroconductive conjugated groups, applying a voltage between the first electrode and the second electrode to polymerize the electrolytically polymerizable unsaturated groups, and deriving a third electrode from the substrate such that the substrate acts as the third electrode.
摘要翻译：一种制造有机器件的方法包括：在其表面上形成有绝缘膜的基板上形成第一电极和第二电极，用第一电极和第二电极作为掩模蚀刻绝缘膜，形成单分子或通过化学吸收法或Langmuir-Blodgett法直接或间接地在基材表面上含有电解聚合性不饱和基团的单分子膜。该方法还包括将含有电解可聚合不饱和基团的表面活性剂扩散到水浴表面以形成单分子膜，将至少一层单分子膜转移到基材表面的方法，以及化学键合所述表面活性剂形成至少一层含有导电共轭基团的表面活性剂的单分子膜，在所述第一电极和所述第二电极之间施加电压以聚合所述电解聚合的不饱和基团，并从所述基板导出第三电极，衬底作为第三电极。

63. 发明授权

US5578340A Medical member and method of manufacturing the same 失效
标题翻译：医疗会员及其制造方法
公开(公告)号：US5578340A
公开(公告)日：1996-11-26
申请号：US485787
申请日：1995-06-07
申请人： Kazufumi Ogawa , Norihisa Mino , Mamoru Soga
发明人： Kazufumi Ogawa , Norihisa Mino , Mamoru Soga
IPC分类号： A61L33/00 , B05D1/18 , C09D4/00 , B05D3/06 , B05D3/10 , B05D1/36
CPC分类号： B82Y30/00 , A61L33/0088 , B05D1/185 , B82Y40/00 , B82Y5/00 , C09D4/00 , Y10S623/923
摘要： A medical member having active hydrogen groups such as hydroxyl, amino or imino groups at its surface, is dipped, either directly or after formation of an inner layer on its surface, into a solution. The solution is prepared by dissolving a surface active material, e.g., CF.sub.3 (CF.sub.2).sub.7 (CH.sub.2).sub.2 SiCl.sub.3 in a non-aqueous solvent. A dehydrochlorination reaction is brought about between active hydrogen groups at the surface of the member and SiCl groups of the surface active material, thus producing bonds ofCF.sub.3 (CF.sub.2).sub.7 (CH.sub.2).sub.2 Si(O--).sub.3over the entire surface. A fluorine-containing monomolecular film is formed, which is chemically (or covalently) bonded to the member surface and has a thickness at the nanometer level. Since the chemically adsorbed film is covalently bonded to the member or inner layer, it is chemically stable and difficult to separate. Medical members can be obtained when the invention is applied to an artificial tooth, a joint, a bone, a blood bag, a catheter, a blood transportation tool, a dialysis equipment part, an operation thread, a medical implant and an operation tool.
摘要翻译：在其表面具有羟基，氨基或亚氨基的活性氢基团的医学成分在其表面上直接或内层形成后溶解成溶液。通过将表面活性物质例如CF 3（CF 2）7（CH 2）2 ClCl 3溶解在非水溶剂中来制备溶液。在成员表面的活性氢基团和表面活性材料的SiCl基团之间产生脱氯化氢反应，从而在整个表面上产生CF 3（CF 2）7（CH 2）2 Si（O-）3的键。形成化学（或共价）结合到构件表面并具有纳米级厚度的含氟单分子膜。由于化学吸附的膜共价结合到构件或内层，因此化学稳定且难以分离。当将本发明应用于人造牙齿，关节，骨骼，血袋，导管，血液输送工具，透析设备部件，手术线，医疗植入物和操作工具时，可获得医疗部件。

64. 发明授权

US5552236A Organic magnetic film and method of manufacturing the same 失效
标题翻译：有机磁性膜及其制造方法
公开(公告)号：US5552236A
公开(公告)日：1996-09-03
申请号：US25662
申请日：1993-03-03
申请人： Tadashi Ohtake , Norihisa Mino , Kazufumi Ogawa
发明人： Tadashi Ohtake , Norihisa Mino , Kazufumi Ogawa
IPC分类号： B05D1/18 , G11B5/62 , H01F1/42 , H01F10/00 , G11B5/66 , B05D5/12 , C09J5/02
CPC分类号： B82Y30/00 , B05D1/185 , B82Y10/00 , B82Y40/00 , G11B5/62 , H01F1/42 , H01F10/005 , H01F1/0009 , Y10S428/90
摘要： According to the invention, the surface of a substrate possessing an active hydrogen group is contacted with a chemical adsorbent containing a radical generation precursor group or metal ion capturing group within a molecule--also possessing a reactive functional group such as halosilyl or alkoxy silyl at its end--to form a chemical adsorption film by removing the unreacted chemical adsorbent, radicals are then generated and magnetism is expressed on the chemical adsorption film.
摘要翻译：根据本发明，具有活性氢基团的基材的表面在分子内与含有自由基产生前体基团或金属离子捕获基团的化学吸附剂接触，并且在其分子中也具有反应性官能团如卤代甲硅烷基或烷氧基甲硅烷基通过除去未反应的化学吸附剂形成化学吸附膜，然后产生自由基，并在化学吸附膜上表现磁性。

65. 发明授权

US5536982A Ultra thin polymer film electret 失效
标题翻译：超薄聚合物电极驻极体
公开(公告)号：US5536982A
公开(公告)日：1996-07-16
申请号：US507667
申请日：1995-07-25
申请人： Norihisa Mino , Yoshikazu Yamagata , Kazufumi Ogawa
发明人： Norihisa Mino , Yoshikazu Yamagata , Kazufumi Ogawa
IPC分类号： B29C41/12 , B29L9/00 , B29L31/34 , C08J5/18 , C08J7/00 , H01G7/02 , G11C13/02
CPC分类号： H01G7/023 , B82Y30/00 , B82Y40/00
摘要： The invention concerns an ultra thin polymer film electret comprising a polymer and a substrate having a surface electric charge, wherein a side chain of the polymer and the substrate are physically or chemically bonded. A method of manufacturing an ultra thin polymer film electret comprising: adsorbing a monomolecular film comprising a unsaturated group or a laminated film comprising the monomolecular film on to a substrate surface, irradiating the monomolecular film or the laminated film with an energy beam to polymerize the unsaturated groups and applying a high voltage to the film is also disclosed. Further, a method of manufacturing an ultra thin polymer film electret comprising: physically bonding a side chain of the polymer to a substrate surface to form a thin film and applying a high voltage to the thin film is also disclosed.
摘要翻译：本发明涉及一种包含聚合物和具有表面电荷的基底的超薄聚合物膜驻极体，其中聚合物和基底的侧链物理或化学键合。一种制造超薄聚合物膜驻极体的方法，包括：将包含不饱和基团的单分子膜或包含单分子膜的层压膜吸附到基材表面上，用能量束照射单分子膜或层压膜以聚合不饱和并且还公开了向薄膜施加高电压的组。此外，还公开了一种制造超薄聚合物膜驻极体的方法，其包括：将聚合物的侧链物理结合到基板表面以形成薄膜并向薄膜施加高电压。

66. 发明授权

US5500250A Chemically adsorbed film and method of manufacturing the same 失效
标题翻译：化学吸附膜及其制造方法
公开(公告)号：US5500250A
公开(公告)日：1996-03-19
申请号：US511912
申请日：1995-08-07
申请人： Kazufumi Ogawa , Norihisa Mino , Mamoru Soga
发明人： Kazufumi Ogawa , Norihisa Mino , Mamoru Soga
IPC分类号： A61L33/00 , B05D1/18 , C09D4/00 , B05D3/00
CPC分类号： B82Y30/00 , A61L33/0088 , B05D1/185 , B82Y40/00 , B82Y5/00 , C09D4/00 , Y10T428/31544 , Y10T428/31612 , Y10T428/31699
摘要： Disclosed is an ornament with a thin film formed on the ornament surface. The thin film includes a fluorocarbon-based adsorbed monomolecular film, and the thin film is covalently bonded to the ornament. By contacting the ornament with the non-aqueous solution containing a chlorosilane group at one end and a fluorocarbon chain at the other end, a reaction occurs between hydroxyl groups at the ornament surface and the chlorosilyl groups of the material having a plurality of chlorosilyl grounds. A monomolecular film which is covalently bonded to the ornament surface is thereby obtained. A thin, fluorine-containing, monomolecular film thus can be formed on the ornament such that it is, chemically bonded to the ornament. The film is anti-contaminating, water-and oil-repelling, durable and does not spoil the intrinsic luster of the ornament.
摘要翻译：公开了一种在装饰表面上形成有薄膜的装饰品。薄膜包括氟碳基吸附单分子膜，并且该薄膜与装饰物共价键合。通过将装饰物与其一端含有氯硅烷基的非水溶液和另一端的碳氟化合物链接触，在装饰表面的羟基和具有多个氯代甲硅烷基的材料的氯甲硅烷基之间发生反应。由此获得共价键合到装饰表面的单分子膜。因此，可以在装饰品上形成薄的含氟单分子膜，使其与装饰物化学结合。该胶片具有防污，防水，防油，耐用，不会破坏装饰品的内在光泽。

67. 发明授权

US5474839A Surface-treated apparel material 失效
标题翻译：表面处理服装材料
公开(公告)号：US5474839A
公开(公告)日：1995-12-12
申请号：US165569
申请日：1993-12-13
申请人： Kazufumi Ogawa , Norihisa Mino , Mamoru Soga
发明人： Kazufumi Ogawa , Norihisa Mino , Mamoru Soga
IPC分类号： B05D1/18 , D06M15/657 , D06M23/00 , B32B7/00
CPC分类号： B82Y30/00 , B05D1/185 , B82Y40/00 , D06M15/657 , D06M23/005 , Y10T428/2962 , Y10T428/2964 , Y10T428/31663 , Y10T442/2172 , Y10T442/2762 , Y10T442/2861 , Y10T442/2885 , Y10T442/2893
摘要： According to the invention, a chemically adsorbed film is formed on an apparel material which has a surface layer containing fluorocarbon groups and a stem which is chemically bonded by --Si-- bonds to the material. A high performance apparel material thus can be provided which retains intrinsic properties of material such as ventilation and aesthetic appearance and is excellently durable and highly water- and oil-repelling and anti-contaminating or excellently durable and highly hydrophilic. The chemically adsorbed film has a very thin surface layer containing fluorocarbon groups, and is thus excellently water- and oil-repelling and anti-contaminating. In addition, since its stem is chemically bonded via --Si-- bonds to the material, it does not separate and is excellently durable. Further, it is very thin and does not adversely effect intrinsic properties of material such as ventilation, color and aesthetic appearance.
摘要翻译：根据本发明，在具有含氟碳基团的表面层和通过-Si-键与材料化学键合的茎的衣服材料上形成化学吸附的膜。因此可以提供高性能的服装材料，其保持诸如通风和美观外观的材料的固有特性，并且具有优异的耐久性和高度防水和防油和防污染或优异的耐用和高亲水性。化学吸附膜具有非常薄的含有氟碳基团的表面层，因此具有极好的防水和防油和防污染性。此外，由于其茎通过-Si-键与材料化学键合，因此它不分离并且非常耐用。此外，它非常薄，并且不会不利地影响诸如通风，颜色和美学外观的材料的固有性质。

68. 发明授权

US5466487A Chemically adsorbed film and method of manufacturing the same 失效
标题翻译：化学吸附膜及其制造方法
公开(公告)号：US5466487A
公开(公告)日：1995-11-14
申请号：US316106
申请日：1994-09-30
申请人： Tadashi Ohtake , Norihisa Mino , Kazufumi Ogawa
发明人： Tadashi Ohtake , Norihisa Mino , Kazufumi Ogawa
IPC分类号： B05D1/18 , B05D3/02
CPC分类号： B82Y30/00 , B05D1/185 , B82Y40/00 , Y10T428/31504 , Y10T428/31533 , Y10T428/31536 , Y10T428/31989 , Y10T428/31993
摘要： A chemically adsorbed monomolecular or a laminated monomolecular film comprising a monomolecular film formed on said substrate surface by covalent S-bonds is disclosed. For example, the covalent S-bond is selected of a group consisting of --(S.dbd.O)-- and --(O.dbd.S.dbd.O)--. A method of producing a chemical adsorption film comprising; contacting a substrate containing hydroxl groups present on the surface with a non-aqueous solvent containing a material having a thionyl halide group or sulfuryl haloride group; removing unreacted surface active material remaining on the substrate by washing the substrate with a non-aqueous organic solution for making monomolecular a precursor film; reacting unreacted surface active material remaining on the adsorbed monomolecular precursor film with water; and drying the adsorbed monomolecular film is also disclosed. Further, a method of producing a laminated chemical adsorption film comprising laminating a monomolecular adsorption film by repeating the above steps is disclosed.
摘要翻译：公开了一种化学吸附单分子或包含通过共价S-键在所述基片表面上形成的单分子膜的层叠单分子膜。例如，共价S-键选自 - （S = O） - 和 - （O = S = O） - 。一种生产化学吸附膜的方法，包括：使含有存在于表面上的羟基的底物与含有具有亚硫酰卤基或硫酰卤基的物质的非水溶剂接触; 通过用用于制备单分子前体膜的非水有机溶液洗涤基板来除去残留在基板上的未反应的表面活性物质; 将残留在吸附的单分子前体膜上的未反应的表面活性物质与水反应; 并且还公开了吸附的单分子膜的干燥。此外，公开了通过重复上述步骤来层压单分子吸附膜的层压化学吸附膜的制造方法。

69. 发明授权

US5466486A Chemically adsorbed monomolecular lamination film 失效
标题翻译：化学吸附单分子层压膜
公开(公告)号：US5466486A
公开(公告)日：1995-11-14
申请号：US316105
申请日：1994-09-30
申请人： Kazufumi Ogawa , Norihisa Mino , Mamoru Soga
发明人： Kazufumi Ogawa , Norihisa Mino , Mamoru Soga
IPC分类号： B05D1/18 , C08J7/04 , C09D4/00 , C09D183/08 , B05D3/02
CPC分类号： C04B41/52 , B05D1/185 , B82Y30/00 , B82Y40/00 , B82Y5/00 , C04B41/009 , C04B41/89 , C08J7/047 , C09D183/08 , C09D4/00 , C04B2111/00965 , C08J2483/00 , Y10T428/261 , Y10T428/31612 , Y10T428/31663 , Y10T428/31667
摘要： The invention to provide a chemically adsorbed monomolecular lamination film comprising a chemically adsorbed monomolecular film formed via a siloxane-based monomolecular or polymer film on a substrate surface. It also seeks to provide a method of forming a chemically adsorbed monomolecular film efficiently and with high density on a substrate surface with few hydroxyl groups, which method comprises a step of contacting a substrate containing hydroxyl groups present on the surface with a non-aqueous solution containing a material with plural chlorosilanol groups in molecule, a step of removing the material remaining on the substrate without reaction by washing the substrate with a non-aqueous organic solution (if this process is omitted, the siloxane-based polymer film is prepared on the substrate), a step of forming a monomolecular film constituted by a compound containing a silanol group in molecule on the substrate by exposing to the air containing moisture or washing with water, after the removal step, and a step of laminating a monomolecular adsorption film by adsorbing a chlorosilane-based surface active agent constituted by a straight hydrocarbon chain having a chlorosilane groups at one end onto the substrate after the monomolecular or polymer film formation step.
摘要翻译：本发明提供一种化学吸附的单分子层叠膜，其包含在基材表面上通过基于硅氧烷的单分子或聚合物膜形成的化学吸附的单分子膜。它还寻求提供一种在几乎没有羟基的基材表面上有效且高密度地形成化学吸附的单分子膜的方法，该方法包括使含有表面上存在的羟基的基材与非水溶液接触的步骤含有分子中具有多个氯硅烷醇基团的材料，通过用非水有机溶液洗涤基材而除去残留在基材上的材料而不反应的步骤（如果省略该方法，则将硅氧烷基聚合物膜制备在底物），在除去步骤之后，通过暴露于含有水分的空气或用水洗涤的方式，在基板上分子形成由分子中含有硅烷醇基的化合物构成的单分子膜的步骤，以及将单分子吸附膜层叠吸附由o具有氯硅烷基的直链烃链构成的氯硅烷系表面活性剂在单分子或聚合物膜形成步骤之后结束到基底上。

70. 发明授权

US5443901A Magnetic recording medium having an adsorbed film of molecules comprising two species of straight carbon chain molecules 失效
标题翻译：具有包含两种直链碳链分子的分子的吸附膜的磁记录介质
公开(公告)号：US5443901A
公开(公告)日：1995-08-22
申请号：US155244
申请日：1993-11-22
申请人： Norihisa Mino , Mamoru Soga , Ogawa Kazufumi
发明人： Norihisa Mino , Mamoru Soga , Ogawa Kazufumi
IPC分类号： G11B5/72 , G11B5/725 , G11B5/735 , G11B5/738 , G11B5/00
CPC分类号： B82Y30/00 , B82Y10/00 , G11B5/72 , G11B5/725 , G11B5/735 , G11B5/738 , Y10S428/90 , Y10T428/265 , Y10T428/31663
摘要： A magnetic recording film, which has excellent slip durability, is run-proof and wear-proof as well as self-lubricating, is obtained by forming a chemically adsorbed film composed of straight carbon chain surface active materials having different carbon numbers, the chemically adsorbed film being chemically bonded via siloxane covalently bonds.In the method of manufacture, a magnetic recording medium, e.g., a hard disk, is contacted with a solution which is made by dissolving a straight carbon chain surface active material having a chlorosilyl group at one end and a fluorocarbon or hydrocarbon group at the other end in a non-aqueous solvent, thereby chemically bonding the chlorosilane-based straight chain surface active material to the surface of the magnetic recording medium via siloxane covalently bonds.
摘要翻译：通过形成由具有不同碳数的直链碳链表面活性材料构成的化学吸附膜，具有防滑，耐磨和自润滑的优异的耐滑性的磁记录膜，化学吸附通过硅氧烷化学键合的膜共价键合。在制造方法中，将磁记录介质（例如硬盘）与通过将一端具有氯甲硅烷基的直链碳链表面活性材料和另一端的碳氟化合物或烃基溶解而制成的溶液在非水溶剂中结束，从而通过硅氧烷将基于氯硅烷的直链表面活性材料化学键合到磁记录介质的表面进行共价键合。

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