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61. 发明申请

US20090023882A1 PROCESS FOR PREPARATION OF POLYISOBUTYLENE WHOSE CONTENT OF TERMINAL DOUBLE BONDS IS MORE THAN 50% FROM AN INDUSTRIAL C4 HYDROCARBON STREAM COMPRISING 1-BUTENE, 2-BUTENE AND ISOBUTENE 审中-公开
标题翻译：用于制备聚异丁烯的方法包含1-BOTENE，2-BOTENE和ISOBUTENE的端子双重含量的含量超过了工业C4烃类流体的50％以上
公开(公告)号：US20090023882A1
公开(公告)日：2009-01-22
申请号：US12278590
申请日：2007-02-15
申请人： Phillip Hanefeld , Hans-Michael Walter , Matthias Kiefer , Helmut Mach , Thomas Wettling , Marcus Sigl , Markus Schubert , Jurgen Stephan , Rainer Papp , Frank Poplow
发明人： Phillip Hanefeld , Hans-Michael Walter , Matthias Kiefer , Helmut Mach , Thomas Wettling , Marcus Sigl , Markus Schubert , Jurgen Stephan , Rainer Papp , Frank Poplow
IPC分类号： C08F110/10
CPC分类号： C10G57/02 , C08F110/10 , C10G25/00 , C10G2300/1044 , C10G2300/1092 , C08F2/00
摘要： Preparation of polyisobutylene having a content of terminal double bonds of more than 50% by polymerizing isobutene using a polymerization catalyst customary therefor from a technical 1-butene-, 2-butene- and isobutene-containing C4 hydrocarbon stream which may comprise up to 3000 ppm by weight, of 1,3-butadiene, by reducing the content of oxygenates in the C4 hydrocarbon stream before the polymerization of the isobutene by contacting it with an inorganic adsorbent at a pressure of from 1 to 20 bar and a temperature of from 20 to 220° C.
摘要翻译：通过聚合催化剂制备具有大于50％的末端双键的聚异丁烯，所用的聚合催化剂通常来自可以包含高达3000ppm的1-丁烯，2-丁烯和异丁烷的C4烃流通过在异丁烯聚合之前通过将其与无机吸附剂在1至20巴的压力和20至20℃的温度下接触来降低C4烃流中的含氧化合物的含量，从而降低1,3-丁二烯的含量 220°C

62. 发明申请

US20080194903A1 Metathesis Method for Purifying Starting Products 审中-公开
标题翻译：净化起始产品的复分解方法
公开(公告)号：US20080194903A1
公开(公告)日：2008-08-14
申请号：US11817237
申请日：2006-02-24
申请人： Markus Schubert , Jurgen Stephan , Frank Poplow , Thomas Heidemann , Uwe Diehlmann , Michaela Maltry
发明人： Markus Schubert , Jurgen Stephan , Frank Poplow , Thomas Heidemann , Uwe Diehlmann , Michaela Maltry
IPC分类号： C07C7/12
CPC分类号： C07B37/08 , C07C6/04 , C07C7/12 , C07C2521/04 , C07C2523/16 , Y02P30/464 , C07C11/02
摘要： Processes comprising: (a) providing a feed stream comprising a C4 compound having at least a nonaromatic C—C double bond or C—C triple bond; (b) contacting the feed stream with an adsorbent which has been activated at a temperature of 450 to 1000° C. comprising at least 3% by weight of aluminum oxide to remove one or more impurities from the feed stream; and (c) contacting the feed stream from which one or more impurities have been removed with a metathesis catalyst under metathesis reaction conditions to form a compound or a mixture of compounds having a nonaromatic C—C double bond or C—C triple bond.
摘要翻译：方法包括：（a）提供包含至少具有非芳族C-C双键或C-C三键的C 4+化合物的进料流; （b）使进料流与在450至1000℃的温度下活化的吸附剂接触，所述吸附剂包含至少3重量％的氧化铝以从进料流中除去一种或多种杂质; 和（c）在复分解反应条件下使已经除去一种或多种杂质的进料流与复分解催化剂接触，以形成具有非芳族C-C双键或C-C三键的化合物或混合物。

63. 发明申请

US20080188696A1 Process For Preparing A C4-Olefin Mixture By Selective Hydrogenation And Metathesis Process For Using This Stream 有权
标题翻译：通过选择性氢化和复分解方法制备C4-烯烃混合物的方法
公开(公告)号：US20080188696A1
公开(公告)日：2008-08-07
申请号：US11665161
申请日：2005-10-13
申请人： Jurgen Stephan , Andreas Brodhagen , Markus Schubert , Frank Poplow , Michael Roper , Thomas Hill
发明人： Jurgen Stephan , Andreas Brodhagen , Markus Schubert , Frank Poplow , Michael Roper , Thomas Hill
IPC分类号： C07C11/00 , C07C5/02 , C07C6/02
CPC分类号： C07C11/08 , C07C6/04 , C07C2523/44 , C07C11/107 , C07C11/10
摘要： A C4-olefin mixture having a 1,3-butadiene content of from 100 to 500 ppm and a content of 1,2-dienes of less than 10 ppm is described. The present invention further provides a process for preparing this C4-olefin mixture and provides for its use in a metathesis reaction for preparing 2-pentene and/or 3-hexene.
摘要翻译：描述1,3-丁二烯含量为100-500ppm，1,2-二烯含量小于10ppm的C 4 - 烯烃混合物。本发明还提供了一种制备该C 4烯烃混合物的方法，并提供其在复分解反应中用于制备2-戊烯和/或3-己烯的用途。

64. 发明申请

US20080033223A1 Method for the Production of C5 Aldehydes and Propene from a C4 Stream Containing 1-Butene and 2-Butene 有权
标题翻译：从含有1-丁烯和2-丁烯的C4流中制备C5醛和丙烯的方法
公开(公告)号：US20080033223A1
公开(公告)日：2008-02-07
申请号：US11661543
申请日：2005-08-06
申请人： Marcus Sigl , Markus Schubert , Jurgen Stephan , Rainer Papp , Frank Poplow
发明人： Marcus Sigl , Markus Schubert , Jurgen Stephan , Rainer Papp , Frank Poplow
IPC分类号： C07C6/04
CPC分类号： C07C6/04 , C07C7/13 , C07C45/50 , C07C11/06 , C07C11/08 , C07C47/02
摘要： Processes for preparing a C5 aldehyde and propene are disclosed, the processes comprising: (a) providing a feedstream, the feedstream comprising butane, 1-butene, 2-butene and 1,3-butadiene, the 1,3-butadiene present in the feedstream in an amount up to 1000 ppm; (b) contacting the feedstream with hydrogen and carbon monoxide in the presence of a hydroformylation catalsyt to form a 2-butene-rich butane stream and a C5 aldehyde; (c) separating the 2-butene-rich butane stream and the C5 aldehyde; and (d) contacting the 2-butene-rich butane stream with ethene in the presence of a metathesis catalyst to form a propene-containing hydrocarbon stream.
摘要翻译：公开了制备C 5 H 5醛和丙烯的方法，所述方法包括：（a）提供进料流，所述进料流包含丁烷，1-丁烯，2-丁烯和1,3-丁二烯，存在于进料流中的1,3-丁二烯以高达1000ppm的量存在; （b）在加氢甲酰化催化剂存在下使进料流与氢气和一氧化碳接触以形成富含2-丁烯的丁烷流和C 5 H 5醛; （c）分离富含2-丁烯的丁烷流和C 5 H 5醛; 和（d）在复分解催化剂存在下使富含2-丁烯的丁烷流与乙烯接触以形成含丙烯烃流。

65. 发明授权

US08658849B2 Process for the separation of unbranched hydrocarbons from their branched isomers 失效
标题翻译：从支链异构体中分离未分支烃的方法
公开(公告)号：US08658849B2
公开(公告)日：2014-02-25
申请号：US12668436
申请日：2008-06-30
申请人： Markus Schubert , Ulrich Mueller , Christoph Kiener , Ingo Richter , William Dolan , Frank Poplow
发明人： Markus Schubert , Ulrich Mueller , Christoph Kiener , Ingo Richter , William Dolan , Frank Poplow
IPC分类号： C07C7/13
CPC分类号： C07C7/12 , B01J20/22 , B01J20/226 , B01J2220/56 , C07C7/135 , C10G25/003 , C07C9/00
摘要： The present invention relates to a process for the separation of at least one unbranched C4-C2O hydrocarbon from a fluid mixture containing the unbranched hydrocarbon and at least one branched isomer of the unbranched hydrocarbon, which comprises the step of—contacting the fluid mixture with an adsorbent comprising a porous metal organic framework material, which material comprises at least one at least bidentate organic compound coordinately bound to at least one metal ion, to get the unbranched hydrocarbon adsorbed, wherein the at least one at least bidentate organic compound is a monocyclic, bicyclic or polycyclic ring system which is derived from at least one heterocycle selected from the group consisting of pyrrole, alpha-pyridone and gamma-pyridone and has at least two ring nitrogens and is unsubstituted or bears one or more substituents selected independently from the group consisting of halogen, Ci-6-alkyl, phenyl, NH2, NH(d-6-alkyl), N(C1-6-alkyl)2, OH, Ophenyl and OCi-6-alkyl, where the substituents Ci_6-alkyl and phenyl are unsubstituted or bear one or more substituents selected independently from the group consisting of halogen, NH2, NH(d-6-alkyl), N(C1-6-alkyl)2, OH, Ophenyl and OCi-6-alkyl. The present invention also relates to the use of said porous metal-organic framework material in a process for the separation of unbranched hydrocarbons from their branched isomers.
摘要翻译：本发明涉及从含有非支链烃和非支链烃的至少一种支链异构体的流体混合物中分离至少一种未分支的C 4 -C 20烃的方法，其包括使流体混合物与吸附剂，其包含多孔金属有机骨架材料，该材料包含与至少一种金属离子配位结合的至少一种至少二齿有机化合物，以获得非支化烃被吸附，其中至少一种至少二齿有机化合物是单环，衍生自选自吡咯，α-吡啶酮和γ-吡啶酮的至少一种杂环的双环或多环系统，并且具有至少两个环氮并且是未取代的或带有一个或多个独立地选自以下的取代基：的卤素，C 1-6 - 烷基，苯基，NH 2，NH（C 1-6 - 烷基），N（C 1-6 - 烷基）2，OH，苯基和OC 1-6 - 烷基，其中取代基C 1-6 - 烷基和苯基是未取代的或具有一个或多个独立地选自卤素，NH 2，NH（C 1-6 - 烷基），N（C 1-6 - 烷基）2，OH，和OC 1-6烷基。本发明还涉及所述多孔金属 - 有机骨架材料在从其支化异构体中分离未分支烃的方法中的用途。

66. 发明授权

US08174708B2 Analysis of molecular interactions on and/or in thin layers 有权
标题翻译：分析薄层上和/或薄层的分子相互作用
公开(公告)号：US08174708B2
公开(公告)日：2012-05-08
申请号：US12672535
申请日：2008-08-09
申请人： Guenter Gauglitz , Guenther Proll , Florian Proell , Lutz Steinle , Markus Schubert
发明人： Guenter Gauglitz , Guenther Proll , Florian Proell , Lutz Steinle , Markus Schubert
IPC分类号： G01B11/02
CPC分类号： G01N33/54373 , G01N21/45 , G01N21/8422 , G01N33/551
摘要： The invention relates to a carrier for a thin layer and a method for the analysis of molecular interactions on and/or in such a thin layer. A thin layer disposed on a carrier is illuminated with electromagnetic radiation from at least one radiation source and a reflected radiation part on boundary surfaces of the thin layer is detected by means of an optoelectronic converter that converts the detected radiation into a frequency- and intensity-dependant photocurrent. A reading voltage is applied to the optoelectronic converter. By changing the reading voltage, the spectral sensitivity of the optoelectronic converter is varied such that a substantially constant photocurrent is obtained. Alternatively or in addition to varying the spectral sensitivity by changing the reading voltage, the reflected radiation part is detected with an optoelectronic converter that is designed as a sensor layer in the carrier. The carrier is particularly characterized in that it comprises a substrate on which at least one sensor layer with optoelectronic properties is disposed.
摘要翻译：本发明涉及一种用于薄层的载体和用于分析在这种薄层上和/或其中的分子相互作用的方法。设置在载体上的薄层被来自至少一个辐射源的电磁辐射照射，并且通过光电转换器检测薄层边界表面上的反射辐射部分，该光电转换器将检测到的辐射转换成频率和强度 - 依赖光电流。读取电压被施加到光电转换器。通过改变读取电压，改变光电转换器的光谱灵敏度，使得获得基本恒定的光电流。或者或通过改变读取电压来改变光谱灵敏度，反射的辐射部分被设计为载体中的传感器层的光电转换器来检测。载体的特征在于其包括其上设置有至少一个具有光电特性的传感器层的基底。

67. 发明申请

US20110160504A1 PROCESS FOR PREPARING A C4-OLEFIN MIXTURE BY SELECTIVE HYDROGENATION AND METATHESIS PROCESS FOR USING THIS STREAM 有权
标题翻译：通过选择性氢化和使用本流程的METATHESIS过程制备C4-烯烃混合物的方法
公开(公告)号：US20110160504A1
公开(公告)日：2011-06-30
申请号：US13042142
申请日：2011-03-07
申请人： Jürgen Stephan , Andreas Brodhagen , Markus Schubert , Frank Poplow , Michael Röper , Thomas Hill
发明人： Jürgen Stephan , Andreas Brodhagen , Markus Schubert , Frank Poplow , Michael Röper , Thomas Hill
IPC分类号： C07C5/05
CPC分类号： C07C11/08 , C07C6/04 , C07C2523/44 , C07C11/107 , C07C11/10
摘要： A C4-olefin mixture having a 1,3-butadiene content of from 100 to 500 ppm and a content of 1,2-dienes of less than 10 ppm is described. The present invention further provides a process for preparing this C4-olefin mixture and provides for its use in a metathesis reaction for preparing 2-pentene and/or 3-hexene.
摘要翻译：描述1,3-丁二烯含量为100-500ppm，1,2-二烯含量小于10ppm的C 4 - 烯烃混合物。本发明还提供了一种制备该C 4烯烃混合物的方法，并提供其在复分解反应中用于制备2-戊烯和/或3-己烯的用途。

68. 发明申请

US20110011805A1 POROUS METAL ORGANIC FRAMEWORKS AS DESICCANTS 审中-公开
标题翻译：多孔金属有机框架作为干燥剂
公开(公告)号：US20110011805A1
公开(公告)日：2011-01-20
申请号：US12863339
申请日：2009-01-23
申请人： Markus Schubert , Ulrich Mueller , Christoph Kiener
发明人： Markus Schubert , Ulrich Mueller , Christoph Kiener
IPC分类号： B01D15/08
CPC分类号： B01J20/226 , B01D2253/204 , B01D2257/80 , B01J20/0233 , B01J2220/50
摘要： The present invention relates to the use of a porous metal organic framework comprising at least one at least bidentate organic compound coordinate to at least one metal ion as desiccant for reducing the water content of an organic liquid or for removing water from an organic liquid.
摘要翻译：本发明涉及多孔金属有机骨架的用途，所述多孔金属有机骨架包含至少一种至少二齿有机化合物与至少一种金属离子的配位作为干燥剂，用于降低有机液体的含水量或从有机液体中除去水分。

69. 发明授权

US07847115B2 Process for preparing porous organic framework materials 有权
标题翻译：制备多孔有机骨架材料的方法
公开(公告)号：US07847115B2
公开(公告)日：2010-12-07
申请号：US12161024
申请日：2007-02-08
申请人： Markus Schubert , Ulrich Mueller , Hendrick Mattenheimer
发明人： Markus Schubert , Ulrich Mueller , Hendrick Mattenheimer
IPC分类号： C07F3/00 , C07F15/00 , C07F5/02
CPC分类号： C07F3/003 , C07F19/005
摘要： The present invention relates to a process for preparing porous organic frameworks by reaction of a reaction mixture in a liquid phase comprising the appropriate starting compounds in the presence of a nonaqueous organic solvent in the presence of and/or with liberation of water, wherein the latter is withdrawn from the liquid phase of the reaction mixture during the reaction. Here, frameworks having relatively high specific surface areas can be obtained in a reproducible way.
摘要翻译：本发明涉及一种制备多孔有机骨架的方法，该方法通过在非水有机溶剂存在下和/或与水的释放下在包含合适的起始化合物的液相中反应混合物进行反应，其中后者在反应期间从反应混合物的液相中排出。这里，可以以可再现的方式获得比表面积相对较高的框架。

70. 发明申请

US20100154635A1 ALUMINIUM AMINOCAROBXYLATES AS POROUS METAL ORGANIC FRAMEWORKS 失效
标题翻译：作为多孔金属有机骨架的氨基铝酸铵
公开(公告)号：US20100154635A1
公开(公告)日：2010-06-24
申请号：US12601022
申请日：2008-05-20
申请人： Markus Schubert , Ulrich Mueller , Christoph Kiener
发明人： Markus Schubert , Ulrich Mueller , Christoph Kiener
IPC分类号： B01D53/02 , C07F5/06
CPC分类号： B01D53/02 , B01D2253/204 , B01D2253/306 , B01D2257/108 , B01D2257/504 , B01D2257/702 , B01D2259/4525 , B01J20/226 , B01J20/28042 , B01J20/28066 , B01J20/30 , B01J31/1691 , B01J31/1805 , B01J31/2226 , B01J2531/31 , C07F5/069 , F17C11/00 , F17C11/005 , Y02C10/08 , Y02P20/152
摘要： The present invention relates to a porous metal organic framework comprising an at least bidentate organic compound coordinated to at least one metal ion, where the at least one metal ion is AlIII and the at least bidentate organic compound is an at least monoamino-substituted aromatic dicarboxylic acid selected from the group consisting of terephthalic acid, 2,6-naphthalenedicarboxylic acid, 1,4-naphthalenedicarboxylic acid, 1,5-naphthalenedicarboxylic acid and derivatives thereof in which at least one CH group in the ring has been replaced by nitrogen, wherein the framework in powder form has a specific surface area determined by the Langmuir method (N2, 77 K) of at least 2500 m2/g.In addition, the invention relates to shaped bodies comprising these materials, their preparation and their use for the storage and separation of gases.
摘要翻译：本发明涉及一种多孔金属有机骨架，其包含与至少一种金属离子配位的至少二齿有机化合物，其中至少一种金属离子是AlIII，并且该至少二齿有机化合物是至少一个氨基取代的芳族二羧酸选自对苯二甲酸，2,6-萘二甲酸，1,4-萘二甲酸，1,5-萘二甲酸及其衍生物的酸，其中环中的至少一个CH基团已被氮取代，其中粉末形式的框架具有由Langmuir方法（N2，77K）确定的至少2500m2 / g的比表面积。此外，本发明涉及包含这些材料的成型体，它们的制备及其用于储存和分离气体的用途。

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