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61. 发明授权

US06656884B2 3-(4-cyanophenyl) uracils 失效
标题翻译： 3-（4-氰基苯基）尿嘧啶
公开(公告)号：US06656884B2
公开(公告)日：2003-12-02
申请号：US10323931
申请日：2002-12-20
申请人： Ralf Klintz , Peter Schäfer , Gerhard Hamprecht , Elisabeth Heistracher , Christoph-Sweder von dem Bussche-Hünnefeld , Norbert Götz , Albrecht Harreus , Karl-Otto Westphalen , Helmut Walter , Ulf Misslitz
发明人： Ralf Klintz , Peter Schäfer , Gerhard Hamprecht , Elisabeth Heistracher , Christoph-Sweder von dem Bussche-Hünnefeld , Norbert Götz , Albrecht Harreus , Karl-Otto Westphalen , Helmut Walter , Ulf Misslitz
IPC分类号： C07D23954
CPC分类号： C07D239/54 , A01N43/54 , C07C255/60 , C07C275/42
摘要： 3-(4-Cyanophenyl)uracils of the formula I wherein A is hydrogen, methyl or amino; Y is oxygen or sulfur; R1 is hydrogen or halogen; R2 is hydrogen, halogen, alkyl, haloalkyl, alkylthio, alkylsulfenyl or alkylsulfonyl; R3 is hydrogen, halogen or alkyl; R4 is hydrogen, haloalkyl; or unsubstituted or substituted alkyl, cycloalkyl, alkenyl, alkynyl, alkylcarbonyl, alkenylcarbonyl, alkynylcarbonyl or alkylsulfonyl, methods and intermediates for their manufacture, and their use as herbicides or for the desiccation or defoliation of plants.
摘要翻译：式I的3-（4-氰基苯基）尿嘧啶，其中A是氢，甲基或氨基; Y是氧或硫; R 1是氢或卤素; R 2是氢，卤素，烷基，卤代烷基，烷硫基，或烷基磺酰基; R 3是氢，卤素或烷基; R 4是氢，卤代烷基; 或未取代或取代的烷基，环烷基，烯基，炔基，烷基羰基，烯基羰基，炔基羰基或烷基磺酰基，用于制备的方法和中间体，以及它们作为除草剂的用途或用于植物的干燥或脱叶。

62. 发明授权

US06482774B1 Substituted (4-brompyrazole-3-yl) benzazoles 失效
公开(公告)号：US06482774B1
公开(公告)日：2002-11-19
申请号：US09673996
申请日：2000-10-25
申请人： Cyrill Zagar , Gerhard Hamprecht , Markus Menges , Olaf Menke , Robert Reinhard , Peter Schäfer , Karl-Otto Westphalen , Martina Otten , Helmut Walter
发明人： Cyrill Zagar , Gerhard Hamprecht , Markus Menges , Olaf Menke , Robert Reinhard , Peter Schäfer , Karl-Otto Westphalen , Martina Otten , Helmut Walter
IPC分类号： C07D41704
CPC分类号： C07D413/04 , A01N43/74 , C07D231/16 , C07D417/04 , C07D417/14 , C07F9/6541 , C07F9/65583
摘要： Substituted (4-bromopyrazol-3-yl)benzazoles I and their salts where R1=H, C1-C4-alkyl, C1-C4-haloalkyl; R2=CN, Cl-C4-alkyl, C1-C4-haloalkyl, C1-C4-alkoxy, C1-C4-haloalkoxy, C1-C4-alkylthio, C1-C4-haloalkylthio, C1-C4-alkylsulfinyl, C1-C4-haloalkylsulfinyl, C1-C4-alkylsulfonyl, C1-C4-haloalkylsulfonyl; R4=H, halogen; R5=H, CN, halogen, C1-C4-alkyl, C1-C4-haloalkyl, C1-C4-alkoxy or C1-C4-haloalkoxy; Z=—N═C(XR6)—O— or —N═C(XR6)—S—, attached to &agr; via the nitrogen, oxygen or sulfur; X=a chemical bond, oxygen, sulfur, —S(O)—, —SO2—, —NH— or —N(R7)—; R6, R7=Cl-C6-alkyl, Cl-C6-haloalkyl, cyano-Cl-C4-alkyl, hydroxy-C1-C4-alkyl, C3-C6-alkenyl, cyano-C3-C6-alkenyl, C3-C6-haloalkenyl, C3-C6-alkynyl, cyano-C3-C6-alkynyl, C3-C6-haloalkynyl, C1-C4-alkoxy-C1-C4-alkyl, C1-C4-haloalkoxy-C1-C4-alkyl, C3-C4-alkenyloxy-C1-C4-alkyl, C3-C4-alkynyloxy-C1-C4-alkyl, C3-C8-cycloalkyloxy-C1-C4-alkyl, amino-Cl-C4-alkyl, C1-C4-alkylamino-C1-C4-alkyl, di(C1-C4-alkyl)amino-C1-C4-alkyl, Cl-C4-alkylthio-C1-C4-alkyl, C1-C4-haloalkylthio-C1-C4-alkyl, C3-C4-alkenylthio-C1-C4-alkyl, C3-C4-alkynylthio-C1-C4-alkyl, C1-C4-alkylsulfinyl-Cl-C4-alkyl, C1-C4-haloalkylsulfinyl-C1-C4-alkyl, C3-C4-alkenylsulfinyl-C1-C4-alkyl, C3-C4-alkynylsulfinyl-C1-C4-alkyl, C1-C4-alkylsulfonyl-C1-C4-alkyl, C1-C4-haloalkylsulfonyl-C1-C4-alkyl, C3-C4-alkenylsulfonyl-C1-C4-alkyl, C3-C4-alkynylsulfonyl-C1-C4-alkyl, hydroxycarbonyl-C1-C4-alkyl, C1-C4-alkoxycarbonyl-C1-C4-alkyl, which may carry a CN or C1-C4-alkoxycarbonyl group, C1-C4-alkylthiocarbonyl-C1-C4-alkyl, aminocarbonyl-C1-C4-alkyl, C1-C4-alkylaminocarbonyl-C1-C4-alkyl, di(C1-C4-alkyl)aminocarbonyl-C1-C4-alkyl, di(C1-C4-alkyl)-phosphonyl-C1-C4-alkyl, C1-C4-alkoxyimino-C1-C4-alkyl, C3-C4-alkenyloxyimino-C1-C4-alkyl, unsubstituted or substituted C3-C8-cycloalkyl, C3-C8-cycloalkyl-C1-C4-alkyl, phenyl, phenyl-C1-C4-alkyl, 3- to 7-membered heterocyclyl or heterocyclyl-C1-C4-alkyl, where each cycloalkyl and each heterocyclyl ring may contain a CO or CS ring member; if X=a chemical bond, —O—, —S—, —NH— or —N(R7)—, R6 may also be C1-C4-alkylcarbonyl, C1-C4-haloalkylcarbonyl, C1-C4-alkoxycarbonyl, C1-C4-alkylsulfonyl or C1-C4-haloalkylsulfonyl; if X=a chemical bond, R6 may furthermore be CN, SH, NH2, halogen, —CH2—CH(halogen)-R8, —CH═CH—R8 or —CH═C(halogen)-R8, where R8=COOH, C1-C4-alkoxycarbonyl, C1-C4-alkylthiocarbonyl, CONH2, C1-C4-alkylaminocarbonyl, di(C1-C4-alkyl)aminocarbonyl or di(C1-C4-alkyl)phosphonyl; or R6+R7=an unsubstituted or substituted 1,3-propylene, tetramethylene, pentamethylene or ethyleneoxyethylene chain. Use: As herbicides; for the desiccation/defoliation of plants.

63. 发明授权

US06420314B1 Substituted 2-phenyl pyridines, their manufacture and use as herbicides 失效
标题翻译：取代的2-苯基吡啶，其制造和用作除草剂
公开(公告)号：US06420314B1
公开(公告)日：2002-07-16
申请号：US09423971
申请日：1999-11-17
申请人： Gerhard Hamprecht , Peter Schäfer , Markus Menges , Olaf Menke , Robert Reinhard , Cyrill Zagar , Karl-Otto Westphalen , Martina Otten , Helmut Walter
发明人： Gerhard Hamprecht , Peter Schäfer , Markus Menges , Olaf Menke , Robert Reinhard , Cyrill Zagar , Karl-Otto Westphalen , Martina Otten , Helmut Walter
IPC分类号： A01N4340
CPC分类号： C07D213/70 , A01N43/40 , C07D213/26 , C07D213/61 , C07D213/71
摘要： Substituted 2-phenylpyridines of the formula I in which the substituents and the index m are defined in the specification.
摘要翻译：取代基和指数m在说明书中定义的式Iin的取代的2-苯基吡啶。

64. 发明授权

US06362380B1 Preparation of nitrobiphenyls 有权
标题翻译：硝基联苯的制备
公开(公告)号：US06362380B1
公开(公告)日：2002-03-26
申请号：US09645980
申请日：2000-06-01
申请人： Karl Eicken , Joachim Gebhardt , Harald Rang , Michael Rack , Peter Schäfer
发明人： Karl Eicken , Joachim Gebhardt , Harald Rang , Michael Rack , Peter Schäfer
IPC分类号： C07C20500
CPC分类号： C07C253/30 , C07B37/04 , C07C201/12 , C07C205/06 , C07C205/11 , C07C205/35
摘要： A process for preparing nitrobiphenyls of the formula I where m is 1 or 2, R is halogen R′ or OR′, where R′ is a C-organic radical which may carry groups inert under the reaction conditions, n is 0, 1, 2 or 3, and, in the case of n being 2 or 3, the radicals R are the same or different, by reacting a chloronitrobenzene of the formula II in the presence of a palladium catalyst and a base in a solvent with a phenylboronic acid (IIIa) or an alkyl ester thereof of the formula IIIb where R1 is C1-C6-alkyl, or an anhydride thereof. The compounds I are useful as precursors for biphenylamines, which in turn are intermediates for fungicidal crop protection agents.
摘要翻译：制备式I的硝基联苯的方法，其中m为1或2，R为卤素R'或OR'，其中R'为C-有机基团，其可以携带在反应条件下为惰性的基团，n为0,1,2 或3，并且在n为2或3的情况下，基团R相同或不同，通过使钯催化剂和碱在溶剂中的存在下的式II的氯硝基苯与苯基硼酸（IIIa ）或其中R 1为C 1 -C 6 - 烷基的式IIIb的烷基酯或其酸酐。化合物I可用作联苯胺的前体，其又是杀真菌作物保护剂的中间体。

65. 发明授权

US06268311B1 1-Amino-3-benzyluracils 失效
标题翻译： 1-氨基-3-苄基脲嘧啶
公开(公告)号：US06268311B1
公开(公告)日：2001-07-31
申请号：US08981049
申请日：1998-03-17
申请人： Olaf Menke , Ralf Klintz , Gerhard Hamprecht , Elisabeth Heistracher , Peter Schäfer , Cyrill Zagar , Norbert Götz , Karl-Otto Westphalen , Ulf Misslitz , Helmut Walter
发明人： Olaf Menke , Ralf Klintz , Gerhard Hamprecht , Elisabeth Heistracher , Peter Schäfer , Cyrill Zagar , Norbert Götz , Karl-Otto Westphalen , Ulf Misslitz , Helmut Walter
IPC分类号： C07D239545
CPC分类号： C07D239/54 , A01N43/54 , C07C275/24 , C07C281/02 , C07C281/06
摘要： 1-Amino-3-benzyluracils I (X=oxygen, sulfur; R1=C1-C4-haloalkyl; R2=H, halogen; R3, R7=H, CN, SCN, halogen, C1-C4-haloalkyl, C1-C4-haloalkoxy, C1-C4-haloalkylthio; R4=H, CN, SCN, halogen, C1-C4-alkyl, C1-C4-haloalkyl, C1-C4-alkoxy, C1-C4-haloalkoxy, C1-C4-haloalkylthio, C1-C6-alkylaminocarbonyl; R5=H, CN, NO2, halogen, OH, C1-C4-alkoxy, NH2, C1-C6-alkyl-amino; R6=H, CN, NO2, halogen, OH, C1-C4-alkoxy, NH2, C1-C6-alkyl-amino, CHO) and their salts are used as herbicides and for the desiccation/defoliation of plants.
摘要翻译： 1-氨基-3-苄基脲嘧啶I（X =氧，硫; R1 = C1-C4-卤代烷基; R2 = H，卤素; R3，R7 = H，CN，SCN，卤素，C1-C4卤代烷基，卤代烷氧基，C 1 -C 4卤代烷硫基，C 1 -C 4卤代烷硫基，C 1 -C 4卤代烷硫基，C 1 -C 4卤代烷硫基，C 1 -C 4卤代烷氧基， -C 1-6烷基氨基羰基; R 5 = H，CN，NO 2，卤素，OH，C 1 -C 4 - 烷氧基，NH 2，C 1 -C 6烷基 - 氨基; R 6 = H，CN，NO 2，卤素，OH，，NH2，C1-C6-烷基 - 氨基，CHO）及其盐用作除草剂和用于植物的干燥/脱叶。

66. 发明授权

US06232470B1 Substituted pyrazol-3-ylbenzazoles, their use as herbicides or desiccants/defoliants, and their preparation 失效
标题翻译：取代的吡唑-3-基苯并唑，其用作除草剂或干燥剂/脱叶剂，及其制备
公开(公告)号：US06232470B1
公开(公告)日：2001-05-15
申请号：US09331065
申请日：1999-06-16
申请人： Cyrill Zagar , Gerhard Hamprecht , Markus Menges , Olaf Menke , Peter Schäfer , Karl-Otto Westphalen , Ulf Misslitz , Helmut Walter
发明人： Cyrill Zagar , Gerhard Hamprecht , Markus Menges , Olaf Menke , Peter Schäfer , Karl-Otto Westphalen , Ulf Misslitz , Helmut Walter
IPC分类号： C07D41704
CPC分类号： C07D413/04 , A01N43/74 , C07D417/04
摘要： Substituted Pyrazol-3-ylbenzazoles I salts thereof, and their use as herbicides or for the desiccation/defoliation of plants.
摘要翻译：取代的吡唑-3-基苯并唑它们作为除草剂或作为植物干燥/脱叶的用途。

67. 发明授权

US06225313B1 Substituted 2-phenyl-3(2H)-pyridazinones 失效
标题翻译：取代的2-苯基-3（2H） - 哒嗪酮
公开(公告)号：US06225313B1
公开(公告)日：2001-05-01
申请号：US09508781
申请日：2000-03-16
申请人： Peter Schäfer , Gerhard Hamprecht , Markus Menges , Olaf Menke , Michael Rack , Robert Reinhard , Cyrill Zagar , Peter Münster , Karl-Otto Westphalen , Martina Otten , Helmut Walter
发明人： Peter Schäfer , Gerhard Hamprecht , Markus Menges , Olaf Menke , Michael Rack , Robert Reinhard , Cyrill Zagar , Peter Münster , Karl-Otto Westphalen , Martina Otten , Helmut Walter
IPC分类号： C07D23718
CPC分类号： C07D405/10 , A01N43/58 , C07D237/22
摘要： Substituted 2-phenyl-3(2H)-pyridazinones I and salts thereof, where n=0, 1, 2; R1=C1-C4-alkyl, C1-C4-haloalkyl; R2=H, halogen; R3=halogen, CN; R4=H, NO2, CN, CHO, NH—OH, C1-C4-alkyl, C1-C4-halogenalkyl, —OR5, —CH═N—OR6, —CH═C(R7)—CO—OR8, —CO—OR9, C1-C6-alkyl-SO2—NH, di(C1-C6-alkylsulfonyl)amino or R5=C1-C6-alkyl, C3-C6-alkenyl, C3-C6-alkynyl, (C1-C6-alkoxy)carbonyl-C1-C4-alkyl, (C3-C6-alkenyloxy)carbonyl-C1-C4-alkyl, (C3-C6-alkynyloxy)carbonyl-C1-C4-alkyl, C1-C4-alkoxy(C1-C4-alkoxy)carbonyl-C1-C4-alkyl; R6=H, C1-C4-alkyl, hydroxycarbonyl-C1-C4-alkyl, (C1-C4-alkoxy)carbonyl-C1-C4-alkyl; R7=H, halogen, C1-C4-alkyl; R8=H, C1-C6-alkyl; R9=H, C1-C6-alkyl, C3-C6-alkenyl, C3-C6-alkynyl, C1-C4-alkoxy-C1-C4-alkoxy, hydroxycarbonyl-C1-C4-alkyl, (C1-C6-alkoxy)carbonyl-C1-C4-alkyl, (C3-C6-alkenyloxy)carbonyl-C1-C4-alkyl, (C3-C6-alkynyloxy)carbonyl-C1-C4-alkyl, C1-C4-alkoxy-(C1-C4-alkoxy)carbonyl-C1-C4-alkyl; R10=H, C1-C6-alkyl, COOH, (C1-C6-alkoxy)carbonyl; and their use as herbicides and for the desiccation/defoliation of plants are described.
摘要翻译：取代的2-苯基-3（2H） - 哒嗪酮I和其盐，其中n = 0,1,2; R1 = C1-C4-烷基，C1-C4卤代烷基; R2 = H，卤素; R3 =卤素，CN; R4 = H，NO2，CN，CHO，NH-OH，C1-C4-烷基，C1-C4-卤代烷基，-OR5，-CH = N-OR6，-CH = C（R7） CO-OR 8，-CO-OR 9，C 1 -C 6烷基-SO 2 -NH，二（C 1 -C 6烷基磺酰基）氨基或R 5 = C 1 -C 6烷基，C 3 -C 6 - 烯基，C 3 -C 6炔基，（C 1 C 3-6 - 烷氧基）羰基-C 1 -C 4烷基，（C 3 -C 6 - 烯氧基）羰基-C 1 -C 4 - 烷基，（C 3 -C 6 - 炔氧基）羰基-C 1 -C 4烷基，C 1 -C 4 - C 1 -C 4 - 烷氧基）羰基-C 1 -C 4 - 烷基; R 6 = H，C 1 -C 4 - 烷基，羟基羰基-C 1 -C 4 - 烷基，（C 1 -C 4 - 卤素，C 1 -C 4 - 烷基; R8 = H，C1-C6-烷基; R9 = H，C1-C6-烷基，C3-C6-烯基，C3-C6-炔基，C1-C4-烷氧基-C1-C4-烷氧基，羟基羰基C1-C4- 烷基，（C 1 -C 6 - 烷氧基）羰基-C 1 -C 4 - 烷基，（C 3 -C 6 - 烯氧基）羰基-C 1 -C 4烷基，（C 3 -C 6 - 炔氧基）羰基-C 1 -C 4烷基，C 1 -C 4 - 烷氧基 - （C 1 -C 4 - 烷氧基）羰基-C 1 -C 4烷基; R 10 = H，C 1 -C 6烷基，COOH，（C 1 -C 6 - 烷氧基）羰基;及其作为除草剂和干燥/ 的植物被描述。

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