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61. 发明授权

US5288867A Process for the preparation of 2-hydroxy-4,6-diaryl-1,3,5-triazines 失效
标题翻译：制备2-羟基-4,6-二芳基-1,3,5-三嗪的方法
公开(公告)号：US5288867A
公开(公告)日：1994-02-22
申请号：US11931
申请日：1993-02-01
申请人： Dieter Reinehr , Jean-Pierre Bacher
发明人： Dieter Reinehr , Jean-Pierre Bacher
IPC分类号： C07D251/22 , C07D251/52
CPC分类号： C07D251/22
摘要： There is disclosed a process for the preparation of 2-hydroxy-4,6-diaryl-1,3,5-triazines, which comprises reacting the compound of formula ##STR1## wherein R is hydrogen, C.sub.1 -C.sub.4 alkyl or halogen, with urea, using a base selected from the class of the alkali metal hydrides, alkaline earth metal hydrides, or alkali metal amides, alkaline earth metal amides, or of the alkali metal C.sub.1 -C.sub.4 alcoholates in the presence of a polar solvent, to give the final products in a one step process in which the molar ratio of urea to base is 1:2 to 1:3 and the molar ratio of compound of formula (1) to urea is 2:1 to 5:1.2-Hydroxy-4,6-diaryl-1,3,5-triazines are prepared in very good yield by the inventive process. The compounds are used as intermediates for the synthesis of UV absorbers.
摘要翻译：公开了2-羟基-4,6-二芳基-1,3,5-三嗪的制备方法，该方法包括使式（*化学结构*）（1）的化合物（其中R是氢，C1- C4烷基或卤素与尿素反应，使用选自碱金属氢化物，碱土金属氢化物或碱金属氨化物，碱土金属氨化物或碱金属C1-C4醇化物的碱在极性溶剂存在下在一步法中给出最终产物，其中脲与碱的摩尔比为1:2至1:3，式（1）化合物与脲的摩尔比为2:1至5:1。通过本发明方法以非常好的收率制备2-羟基-4,6-二芳基-1,3,5-三嗪。该化合物用作合成UV吸收剂的中间体。

62. 发明授权

US5097076A Phenylalkyl glycidyl ether addition products 失效
标题翻译：苯乙醇甘油醚添加剂
公开(公告)号：US5097076A
公开(公告)日：1992-03-17
申请号：US543941
申请日：1990-06-26
申请人： Dieter Reinehr , Rosemarie Topfl
发明人： Dieter Reinehr , Rosemarie Topfl
IPC分类号： B01F17/42 , C08G65/04 , C08G65/26 , C08G65/32 , C08G65/331 , C08G65/338 , C09B67/46 , C11D1/06 , C11D1/12 , C11D1/29 , C11D1/34 , C11D1/72 , C11D3/37 , D06L1/14 , D06M13/02 , D06M13/224 , D06M13/322 , D06M13/402 , D06M13/405 , D06M13/51 , D06M13/513 , D06M15/53 , D06M101/00 , D06M101/02 , D06M101/06 , D06M101/08 , D06M101/16 , D06M101/30 , D06M101/32 , D06M101/34 , D06P1/613
CPC分类号： C08G65/04 , C08G65/2609 , C08G65/331 , C08G65/338 , C09B67/0085 , C11D1/06 , C11D1/123 , C11D1/29 , C11D1/345 , C11D1/72 , C11D3/3707 , D06L1/14 , D06P1/6133 , D06P1/6135
摘要： Addition products of phenylalkyl glycidyl ethers to polyalkylene glycol ethers of the formulaR-O Alkylene--O.sub.m H (1)their acid esters and salts thereof, wherein R is an aliphatic radical having at least 4 carbon atoms, "Alkylene" is an alkylene radical of 2 or 3 carbon atoms, and m is a number from 2 to 100.These products represent a novel class of non-ionic or anionic surfactants that are used as textile finishing agents, especially as emulsifiers, wetting agents, foaminhibitors or dyeing auxiliaries.
摘要翻译：苯基烷基缩水甘油醚与式RO亚烷基-OmH的聚亚烷基二醇醚的加成产物（1）它们的酸酯及其盐，其中R是具有至少4个碳原子的脂族基团，“亚烷基”是2或 3个碳原子，m为2至100.这些产品代表一类新型非离子或阴离子表面活性剂，用作纺织品整理剂，特别是作为乳化剂，润湿剂，阻燃剂或染色助剂。

63. 发明授权

US4918215A 4-halogenostilbene derivatives and processes for their preparation 失效
标题翻译： 4-卤代茋衍生物及其制备方法
公开(公告)号：US4918215A
公开(公告)日：1990-04-17
申请号：US657451
申请日：1984-10-03
申请人： Dieter Reinehr , Alwyn Spencer
发明人： Dieter Reinehr , Alwyn Spencer
IPC分类号： C07C69/65 , C07C17/00 , C07C17/26 , C07C25/24 , C07C63/66 , C07C63/74 , C07C67/00 , C07C69/618 , C07C253/00 , C07C255/34 , C07C255/35 , C07C255/51 , C07D295/16 , C07D295/185
CPC分类号： C07D295/185 , C07C17/2637 , C07C25/24 , C07C255/00 , C07C63/66 , C07C63/74
摘要： Novel compounds of the formula ##STR1## and processes for their preparation are described. X represents bromine or iodine and R.sub.1, R.sub.2 and R.sub.3 have the meaning indicated in the patent claim. The compounds (I) are valuable intermediates for the preparation of fluorescent brighteners of the divinylstilbene type.
摘要翻译：描述了新颖的式（Ⅰ）化合物及其制备方法。 X表示溴或碘，R1，R2和R3具有专利权利要求中所示的含义。化合物（I）是制备二乙烯基芪类荧光增白剂的有价值的中间体。

64. 发明授权

US4782187A Process for the preparation of 4,4'-stilbenedialdehydes 失效
标题翻译：制备4,4'-二苯乙醛的方法
公开(公告)号：US4782187A
公开(公告)日：1988-11-01
申请号：US940312
申请日：1986-12-10
申请人： Dieter Reinehr , Heinz Steiner
发明人： Dieter Reinehr , Heinz Steiner
IPC分类号： C07C47/546 , B01J23/00 , C07B61/00 , C07C45/00 , C07C45/41 , C07C65/30 , C07C67/00
CPC分类号： C07C45/41 , C07C65/30
摘要： The preparation of 4,4'-stilbenedialdehydes from the corresponding acid chlorides in the presence of a noble metal catalyst.
摘要翻译：在贵金属催化剂存在下，从相应的酰氯制备4,4'-二苯乙醛。

65. 发明授权

US4472318A 1,10-Substituted 10-amino-deca-3,7-diene-nitriles and process for their preparation 失效
标题翻译： 1,10-取代的10-氨基 - 十烯-3,7-二烯 - 腈及其制备方法
公开(公告)号：US4472318A
公开(公告)日：1984-09-18
申请号：US461045
申请日：1983-01-26
申请人： Dieter Reinehr , Josef Pfeifer
发明人： Dieter Reinehr , Josef Pfeifer
IPC分类号： C08G69/00 , C07C67/00 , C07C253/00 , C07C255/30 , C07C255/31 , C07C255/42 , C08G69/26 , C07C121/45 , C07C121/48 , C07C121/78
CPC分类号： C07C255/00 , C08G69/26
摘要： Novel 10-amino-deca-3,7-diene-nitriles of the formula ##STR1## are described, in which R.sub.1 is C.sub.1-12 -alkyl, R.sub.2 is H or C.sub.1-12 -alkyl, R.sub.3 is C.sub.1-12 -alkyl, cycloalkyl having 4-12 ring C atoms, C.sub.7-8 -aralkyl, substituted or unsubstituted aryl or, if R.sub.4 =H, --Ch.dbd.CH--alkyl or --C(alkyl).dbd.CH--alkyl each having 1-4 C atoms in the alkyl groups, and R.sub.4 =H, C.sub.1-12 -alkyl, cycloalkyl having 4-12 ring C atoms, C.sub.7-8 -aralkyl or substituted or unsubstituted aryl, or R.sub.1 and R.sub.2 and/or R.sub.3 and R.sub.4 together are C.sub.3-11 -alkylene. The compounds (I) can be reduced in a manner known per se to give the corresponding 1,11-diamino-undeca-3,7-dienes. The latter are valuable intermediates and are suitable especially for the preparation of transparent crosslinkable polyamides.
摘要翻译：描述了式（I）的新的10-氨基 - 癸-3,7-二烯 - 腈，其中R 1是C 1-12 - 烷基，R 2是H或C 1-12 - 烷基，R 3是C1- 具有4-12个环C原子的环烷基，C7-8-芳烷基，取代或未取代的芳基，或如果R4 = H，-Ch = CH-烷基或-C（烷基）= CH-烷基，各自具有1- 4个C原子，R4 = H，C1-12烷基，具有4-12个环C原子的环烷基，C7-8-芳烷基或取代或未取代的芳基，或R1和R2和/或R3和R4一起是C3-11-亚烷基。化合物（I）可以以本身已知的方式还原，得到相应的1,11-二氨基 - 十一碳-3,7-二烯。后者是有价值的中间体，并且特别适于制备透明的可交联聚酰胺。

66. 发明授权

US4440694A Process for the production of vinylstilbene compounds 失效
标题翻译：制备乙烯基芪化合物的方法
公开(公告)号：US4440694A
公开(公告)日：1984-04-03
申请号：US262001
申请日：1981-05-08
申请人： Daniel Bellus , Hans-Ulrich Blaser , Guglielmo Kabas , Dieter Reinehr , Alwyn Spencer , Kurt Weber
发明人： Daniel Bellus , Hans-Ulrich Blaser , Guglielmo Kabas , Dieter Reinehr , Alwyn Spencer , Kurt Weber
IPC分类号： C07C2/86 , C07C15/52 , C07C45/68 , C07C49/223 , C07C69/618 , C07C255/34 , C07D307/12 , C07D319/12 , C07C121/70 , C07C103/24
CPC分类号： C07C255/00 , C07C2/862 , C07C45/68 , C07C49/223 , C07D307/12 , C07D319/12 , C07C2531/22
摘要： The invention relates to vinylstilbene compounds of the formula ##STR1## wherein Q is the grouping --COX or ##STR2## These compounds are obtained by reacting 1 molar equivalent of a compound of the formula II ##STR3## wherein X is chlorine, bromine or iodine, in the presence of a base and with the addition of palladium metal or of palladium compounds, as catalyst, which, under the reaction conditions, form labile palladium(O) compounds which do not contain phosphorus, with 1 molar equivalent of a compound of the formula III or with 1 molar equivalent of each of the compounds of the formulae III and IV ##STR4##
摘要翻译：本发明涉及式（I）的乙烯基茋化合物，其中Q是分组-COX或这些化合物。这些化合物通过使1摩尔当量的式II化合物（II）反应，其中X 在碱的存在下，加入钯金属或钯化合物作为催化剂，其在反应条件下形成不含磷的不稳定钯（O）化合物，其中1是氯，溴或碘摩尔当量的式III化合物或1摩尔当量的式III和IV化合物的每一种

67. 发明授权

US4335055A Process for the preparation of alkenylbenzene derivatives or alkenylnaphthalene derivatives 失效
标题翻译：烯基苯衍生物或烯基萘衍生物的制备方法
公开(公告)号：US4335055A
公开(公告)日：1982-06-15
申请号：US262002
申请日：1981-05-08
申请人： Hans-Ulrich Blaser , Dieter Reinehr , Alwyn Spencer
发明人： Hans-Ulrich Blaser , Dieter Reinehr , Alwyn Spencer
IPC分类号： B01J23/00 , B01J23/44 , B01J27/00 , B01J27/13 , B01J31/00 , B01J31/22 , C07B31/00 , C07B37/04 , C07B61/00 , C07C1/00 , C07C2/86 , C07C15/40 , C07C15/44 , C07C15/52 , C07C15/58 , C07C17/26 , C07C17/263 , C07C25/24 , C07C41/30 , C07C43/215 , C07C45/68 , C07C47/548 , C07C67/00 , C07C205/06 , C07C255/34 , C07C255/41 , C07C255/50 , C07D239/26 , C07C121/70 , C07C49/217
CPC分类号： C07D239/26 , C07C17/263 , C07C2/862 , C07C201/12 , C07C255/00 , C07C43/215 , C07C45/68 , C07C2527/13 , C07C2531/04 , C07C2531/22
摘要： Compounds of the formula I ##STR1## in which Z, Z.sub.1, R, m and p are as defined in patent claim 1, can be obtained in a simple and economical manner by a novel process wherein a halide of the formula II ##STR2## is reacted with a substituted or unsubstituted vinylbenzene or vinylnaphthalene derivative in the presence of a base and of certain palladium catalysts, such as palladium acetate. The compounds (I) or functional derivatives preparable therefrom are useful, for example, for the preparation of known dyes or fluorescent brighteners, or can be used directly as fluorescent brighteners or as scintillators.
摘要翻译：其中Z，Z1，R，m和p如权利要求1中所定义的式I的化合物（I）可以简单和经济地通过新方法获得，其中式II的卤化物在碱和某些钯催化剂如乙酸钯存在下，将Z [（CHCH）mCOX] p（II）与取代或未取代的乙烯基苯或乙烯基萘衍生物反应。可由其制备的化合物（I）或官能衍生物可用于例如制备已知染料或荧光增白剂，或可直接用作荧光增白剂或闪烁剂。

68. 发明授权

US4332969A Substituted 11-aminoundecanols 失效
标题翻译：取代的11-氨基十一烷醇
公开(公告)号：US4332969A
公开(公告)日：1982-06-01
申请号：US124690
申请日：1980-02-26
申请人： Dieter Reinehr , Adolf Hubele
发明人： Dieter Reinehr , Adolf Hubele
IPC分类号： A01N33/08 , A01N49/00 , B01J23/00 , C07C67/00 , C07C213/00 , C07C215/08 , C07C215/20 , C07C215/42 , C07D225/02 , C07D225/06 , C07C85/20 , C07C87/40 , C07C87/453 , C07C91/04
CPC分类号： C07D225/02 , A01N33/08 , A01N49/00 , C07D225/06
摘要： Novel substituted 11-aminoundecanols of the formula ##STR1## and a process for their preparation are described; in the formula, R.sub.1 and R.sub.3 independently of one another are hydrogen or alkyl having 1-8 C atoms and R.sub.2 and R.sub.4 independently of one another are alkyl having 1-8 C atoms, or R.sub.1 and R.sub.2 and/or R.sub.3 and R.sub.4 together with the bonding C atom form a cycloaliphatic ring having 4-8 C atoms, and R.sub.5 and R.sub.6 independently of one another are hydrogen or alkyl having 1-4 C atoms. The compounds of the formula I are valuable active compounds for combating plant pests.
摘要翻译：描述了式（Ⅰ）＆lt; IMAGE＆gt;的新型取代的11-氨基十一烷及其制备方法; 在式中，R 1和R 3彼此独立地是氢或具有1-8个C原子的烷基，R 2和R 4彼此独立地是具有1-8个C原子的烷基，或者R 1和R 2和/或R 3和R 4与键合C原子形成具有4-8个C原子的脂环族环，R 5和R 6彼此独立地是氢或具有1-4个C原子的烷基。式I的化合物是用于防治植物害虫的有价值的活性化合物。

69. 发明授权

US4290964A Undescanoic acids and esters thereof 失效
标题翻译：壬酸及其酯
公开(公告)号：US4290964A
公开(公告)日：1981-09-22
申请号：US126081
申请日：1980-02-29
申请人： Dieter Reinehr , Paul Lienhard
发明人： Dieter Reinehr , Paul Lienhard
IPC分类号： C09B43/32 , C07C67/00 , C07C227/00 , C07C227/02 , C07C227/18 , C07C229/02 , C07C229/08 , C07C229/30 , C07C229/46 , C07D225/02 , C09B29/42 , C09B69/04 , C09F5/00
CPC分类号： C09B29/363 , C07D225/02 , C09B69/04
摘要： The invention relates to 11-aminoundecanoic acids and 11-aminoundeca-4,8-dienoic acids and the esters of these acids. They have the formula I ##STR1## wherein R.sup.1 and R.sup.3 are e.g. hydrogen and R.sup.2 and R.sup.4 are e.g. methyl and E is e.g. the radical --CH.sub.2 CH.sub.2 -- and R.sup.7 is hydrogen or an alkyl radical. The esters are suitable for the manufacture of salts of anionic dyes which are very readily soluble in organic solvents.
摘要翻译：本发明涉及11-氨基十一烷酸和11-氨基十一烷-4,8-二烯酸和这些酸的酯。它们具有式I（I）其中R 1和R 3是例如。氢和R2和R4是例如。甲基和E是例如。基团-CH 2 CH 2 - 和R 7是氢或烷基。这些酯适用于制造非常容易溶于有机溶剂的阴离子染料的盐。

70. 发明授权

US4277621A Substituted 11-amino-undeca-4,8-dienal and 11-amino-undecanal derivatives and processes for their preparation 失效
标题翻译：取代的11-氨基 - 十一烷-4,8-二烯酸和11-氨基 - 十一烷醛衍生物及其制备方法
公开(公告)号：US4277621A
公开(公告)日：1981-07-07
申请号：US83140
申请日：1979-10-09
申请人： Dieter Reinehr , Josef Pfeifer
发明人： Dieter Reinehr , Josef Pfeifer
IPC分类号： C08G59/00 , C07C67/00 , C07C209/00 , C07C209/40 , C07C209/42 , C07C209/52 , C07C209/62 , C07C211/09 , C07C211/17 , C07C211/25 , C07C211/27 , C07C211/29 , C07C239/00 , C07C241/00 , C07C251/04 , C07C251/16 , C07C251/34 , C07C251/52 , C07C251/78 , C07C251/80 , C07C251/82 , C07C281/06 , C07C281/08 , C07D225/00 , C07D225/02 , C07D225/04 , C07D307/52 , C07D333/06 , C07D333/20 , C08G59/50 , C08G69/26 , C07C109/14 , C07C109/16 , C07C131/00
CPC分类号： C07C251/72 , C07D225/00 , C07D225/02 , C07D225/04 , C07D307/52 , C07D333/20 , C08G59/50 , C08G69/26
摘要： Novel substituted 11-amino-undeca-4,8-dienal and 11-amino-undecanal aldehyde-derivatives of the formulae Ia ##STR1## in which R.sub.1 to R.sub.6, Y and m are as defined in patent claim 1, and processes for their preparation are described. The compounds of the formulae Ia and Ib can be catalytically hydrogenated to novel 1,11-diaminoundecanes, which, in turn, can be used, for example, for the preparation of polycondensation products, in particular transparent polyamides, or as curing agents for epoxide resins.
摘要翻译：（Ia）或Ib（VI）的新型取代的11-氨基 - 十一碳-4,8-二烯酸和11-氨基 - 十一醛醛衍生物，其中R 1至R 6，Y 和m如专利权利要求1中所定义，并描述了其制备方法。式Ia和Ib的化合物可以催化氢化成新的1,11-二氨基十一烷，其又可用于例如缩聚产物，特别是透明聚酰胺的制备，或作为环氧化物的固化剂树脂。

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