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61. 发明授权

US07973126B2 Emissive polymeric materials for optoelectronic devices 有权
标题翻译：用于光电器件的发射聚合材料
公开(公告)号：US07973126B2
公开(公告)日：2011-07-05
申请号：US11957579
申请日：2007-12-17
申请人： Joseph John Shiang , Kelly Scott Chichak , James Anthony Cella , Larry Neil Lewis , Kevin Henry Janora
发明人： Joseph John Shiang , Kelly Scott Chichak , James Anthony Cella , Larry Neil Lewis , Kevin Henry Janora
IPC分类号： C08G79/00 , H01L51/54 , C09K11/06
CPC分类号： C08G61/12 , C08G2261/142 , C08G2261/1526 , C08G2261/3142 , C08G2261/3162 , H01L51/0039 , H01L51/5012 , Y10S428/917
摘要： Polymers including at least one structural unit derived from a compound of formula I or including at least one pendant group of formula II may be used in optoelectronic devices wherein R1, R3, R4 and R6 are independently hydrogen, alkyl, alkoxy, oxaalkyl, alkylaryl, aryl, arylalkyl, heteroaryl, substituted alkyl; substituted alkoxy, substituted oxaalkyl, substituted alkylaryl, substituted aryl, substituted arylalkyl, or substituted heteroaryl; R1a is hydrogen or alkyl; R2 is alkylene, substituted alkylene, oxaalkylene, CO, or CO2; R2a is alkylene; R5 is independently at each occurrence hydrogen, alkyl, alkylaryl, aryl, arylalkyl, alkoxy, carboxy, substituted alkyl; substituted alkylaryl, substituted aryl, substituted arylalkyl, or substituted alkoxy, X is halo, triflate, —B(OR1a)2, or located at the 2, 5- or 2, 7-positions; and L is derived from phenylpyridine, tolylpyridine, benzothienylpyridine, phenylisoquinoline, dibenzoquinozaline, fluorenylpyridine, ketopyrrole, 2-(1-naphthyl)benzoxazole)), 2-phenylbenzoxazole, 2-phenylbenzothiazole, coumarin, thienylpyridine, phenylpyridine, benzothienylpyridine, 3-methoxy-2-phenylpyridine, thienylpyridine, phenylimine, vinylpyridine, pyridylnaphthalene, pyridylpyrrole, pyridylimidazole, phenylindole, derivatives thereof or combinations thereof.
摘要翻译：包括至少一种衍生自式I化合物或包含至少一个式II侧基的结构单元的聚合物可用于其中R 1，R 3，R 4和R 6独立地为氢，烷基，烷氧基，氧杂烷基，烷芳基，芳基，芳基烷基，杂芳基，取代的烷基; 取代的烷氧基，取代的氧杂烷基，取代的烷基芳基，取代的芳基，取代的芳基烷基或取代的杂芳基; R1a是氢或烷基; R2是亚烷基，取代的亚烷基，氧杂亚烷基，CO或CO 2; R2a是亚烷基; R5各自独立地为氢，烷基，烷基芳基，芳基，芳基烷基，烷氧基，羧基，取代的烷基; 取代的烷基芳基，取代的芳基，取代的芳基烷基或取代的烷氧基，X是卤素，三氟甲磺酸酯，-B（OR1a）2，或位于2,5-或2,7-位; 苯基吡啶，苯并噻吩并吡啶，二苯并喹嗪，芴基吡啶，酮吡咯，2-（1-萘基）苯并恶唑）），2-苯基苯并恶唑，2-苯基苯并噻唑，香豆素，噻吩基吡啶，苯基吡啶，苯并噻吩基吡啶，3-甲氧基 - 2-苯基吡啶，噻吩基吡啶，苯基亚胺，乙烯基吡啶，吡啶基萘，吡啶基吡咯，吡啶基咪唑，苯基吲哚，其衍生物或其组合。

62. 发明授权

US07910386B2 Method of making organic light emitting devices 有权
标题翻译：制造有机发光装置的方法
公开(公告)号：US07910386B2
公开(公告)日：2011-03-22
申请号：US11637582
申请日：2006-12-12
申请人： Joseph John Shiang , Kevin Henry Janora , Gautam Parthasarathy , James Anthony Cella , Kelly Scott Chichak
发明人： Joseph John Shiang , Kevin Henry Janora , Gautam Parthasarathy , James Anthony Cella , Kelly Scott Chichak
IPC分类号： H01L29/72
CPC分类号： H01L51/0043 , H01L51/0003 , H01L51/0035 , H01L51/0039 , H01L51/005 , H01L51/0085 , H01L51/56 , Y10T428/31511
摘要： The present invention provides a method for the preparation of organic light-emitting devices comprising a bilayer structure made by forming a first film layer comprising an electroactive material and an INP precursor material, and exposing the first film layer to a radiation source under an inert atmosphere to generate an interpenetrating network polymer composition comprising the electroactive material. At least one additional layer is disposed on the reacted first film layer to complete the bilayer structure. The bilayer structure is comprised within an organic light-emitting device comprising standard features such as electrodes and optionally one or more additional layers serving as a bipolar emission layer, a hole injection layer, an electron injection layer, an electron transport layer, a hole transport layer, exciton-hole transporting layer, exciton-electron transporting layer, a hole transporting emission layer, or an electron transporting emission layer.
摘要翻译：本发明提供一种制备有机发光器件的方法，其包括通过形成包含电活性材料和INP前体材料的第一膜层制备的双层结构，并在惰性气氛下将第一膜层暴露于辐射源以产生包含电活性材料的互穿网络聚合物组合物。在反应的第一膜层上设置至少一个附加层以完成双层结构。双层结构包括在包括标准特征的有机发光器件中，例如电极和可选地用作双极型发射层的一个或多个附加层，空穴注入层，电子注入层，电子传输层，空穴传输层，激子 - 空穴传输层，激子 - 电子传输层，空穴传输发射层或电子传输发射层。

63. 发明授权

US07830081B2 Optoelectronic devices with multilayered structures 有权
标题翻译：具有多层结构的光电器件
公开(公告)号：US07830081B2
公开(公告)日：2010-11-09
申请号：US11748195
申请日：2007-05-14
申请人： Larry Neil Lewis , Kelly Scott Chichak , James Anthony Cella , Joseph John Shiang
发明人： Larry Neil Lewis , Kelly Scott Chichak , James Anthony Cella , Joseph John Shiang
IPC分类号： C08G77/398 , H01J1/62
CPC分类号： C08G77/58 , G02B1/043 , C08L83/04
摘要： Optoelectronic devices include polysiloxanes derived from hydrosilation of an organometallic compound of formula L2MZ,wherein L and Z are independently bidentate ligands; at least one of L and Z comprises alkenyl, alkenylaryl, alkenyloxy, alkenyloxyaryl, alkynyl, alkynylaryl, alkynyloxy, alkynyloxyaryl, substituted alkenyl, substituted alkenylaryl, substituted alkenyloxy, substituted alkenyloxyaryl, substituted alkynyl, substituted alkynylaryl, substituted alkynyloxy, substituted alkynyloxyaryl, acrylate, methacrylate, or a combination thereof; and M is Zr, Nb, Mo, Tc, Ru, Rh, Pd, Ag, Cd, Hf, Ta, W, Re, Os, Ir, Pt, Au, Hg, Ga, Ge, In, Sn, Sb, Tl, Pd, Bi, Po, La, Ce, Pr, Nd, Pm, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, or Lu.
摘要翻译：光电器件包括衍生自式L2MZ的有机金属化合物的氢化硅石的聚硅氧烷，其中L和Z独立地是二齿配体; L和Z中的至少一个包括烯基，烯基芳基，烯氧基，烯基氧基芳基，炔基，炔基芳基，炔氧基，炔氧基芳基，取代的烯基，取代的烯基芳基，取代的烯氧基，取代的烯基氧基芳基，取代的炔基，取代的炔基芳基，取代的炔氧基，取代的炔氧基芳基，丙烯酸酯，甲基丙烯酸酯或其组合; 并且M是Zr，Nb，Mo，Tc，Ru，Rh，Pd，Ag，Cd，Hf，Ta，W，Re，Os，Ir，Pt，Au，Hg，Ga，Ge，In，Sn，Sb，，Pd，Bi，Po，La，Ce，Pr，Nd，Pm，Sm，Eu，Gd，Tb，Dy，Ho，Er，Tm，Yb或Lu。

64. 发明申请

US20100268479A1 SENSOR SYSTEM AND METHODS FOR ANALYTE DETECTION 有权
标题翻译：传感器系统和分析仪检测方法
公开(公告)号：US20100268479A1
公开(公告)日：2010-10-21
申请号：US12424016
申请日：2009-04-15
申请人： Radislav Alexandrovich Potyrailo , James Anthony Cella , Cheryl Margaret Surman , Kelly Scott Chichak , Steven Go
发明人： Radislav Alexandrovich Potyrailo , James Anthony Cella , Cheryl Margaret Surman , Kelly Scott Chichak , Steven Go
IPC分类号： G01R27/26 , G01N31/00
CPC分类号： G01N27/026
摘要： A system for selectively determining at least two analytes, comprising at least one resonant sensor circuit comprising a sensing material that predictably affects the resonant complex impedance response of a sensor electrode, wherein the sensing material having at least two material properties that change upon exposure to two or more analytes; and a processor that generates a multivariate sensor response pattern that is based at least in part on a change in the two material properties of the sensing material and a sensing device and methods adapted to detect an analyte using the same sensor system.
摘要翻译：一种用于选择性地确定至少两种分析物的系统，包括至少一个谐振传感器电路，其包括可预测地影响传感器电极的共振复阻抗响应的感测材料，其中所述感测材料具有至少两种材料性质，或更多分析物; 以及处理器，其产生至少部分地基于感测材料的两种材料性质的变化的感测装置和适于使用相同的传感器系统检测分析物的方法的多变量传感器响应图案。

65. 发明申请

US20100144976A1 FUNCTIONALIZED POLYFLUORENES FOR USE IN OPTOELECTRONIC DEVICES 有权
标题翻译：用于光电器件的功能化聚偏氟乙烯
公开(公告)号：US20100144976A1
公开(公告)日：2010-06-10
申请号：US12328805
申请日：2008-12-05
申请人： Kelly Scott Chichak , Larry Neil Lewis , James Anthony Cella , Joseph John Shiang
发明人： Kelly Scott Chichak , Larry Neil Lewis , James Anthony Cella , Joseph John Shiang
IPC分类号： C08F212/32 , C08F4/72
CPC分类号： C08G61/02 , C08G2261/1412 , C08G2261/1424 , C08G2261/143 , C08G2261/148 , C08G2261/1526 , C08G2261/5242 , C08G2261/95 , C09K11/06 , C09K2211/185 , H01L51/0039 , H01L51/0085 , H05B33/14
摘要： The present invention relates to process comprising reacting a polyfluorenes comprising at least one structural group of formula I with an iridium (III) compound of formula II wherein R1 and R2 are independently alkyl, substituted alkyl, aryl, substituted aryl or a combination thereof; R5is H or CHO; R3 and R4 are independently hydrogen, alkyl, substituted alkyl, aryl, substituted aryl or a combination thereof; R11 and R12 taken together form a substituted or unsubstituted monocyclic or bicyclic heteroaromatic ring; R13 is independently at each occurrence halo, nitro, hydroxy, amino, alkyl, aryl, arylalkyl, alkoxy, substituted alkoxy, substituted alkyl, substituted aryl, or substituted arylalkyl; Ar is aryl, heteroaryl, substituted aryl, substituted heteroaryl, or a combination thereof; X is selected from a direct bond, alky, substituted alkyl, and combinations thereof; Y is CHO or NH2; Z is CHO or NH2 where Z does not equal Y; and p is 0, 1 or 2. The invention also relates to the polyfluorenes, which are products of the reaction, and the use of the polyfluorenes in optoelectronic devices.
摘要翻译：本发明涉及包括使包含至少一个式I结构基团的聚芴与式II的铱（III）化合物反应的方法，其中R 1和R 2独立地为烷基，取代的烷基，芳基，取代的芳基或其组合; R5is H或CHO; R3和R4独立地是氢，烷基，取代的烷基，芳基，取代的芳基或其组合; R11和R12一起形成取代或未取代的单环或双环杂芳环; R13各自独立地为卤素，硝基，羟基，氨基，烷基，芳基，芳基烷基，烷氧基，取代的烷氧基，取代的烷基，取代的芳基或取代的芳基烷基; Ar是芳基，杂芳基，取代的芳基，取代的杂芳基或其组合; X选自直接键，烷基，取代的烷基及其组合; Y为CHO或NH2; Z是CHO或NH2，其中Z不等于Y; 并且p为0,1或2.本发明还涉及作为反应产物的聚芴以及聚芴在光电器件中的应用。

66. 发明授权

US07718277B2 Electronic devices comprising organic iridium compositions 有权
标题翻译：包含有机铱组合物的电子器件
公开(公告)号：US07718277B2
公开(公告)日：2010-05-18
申请号：US11504870
申请日：2006-08-16
申请人： Kelly Scott Chichak , James Anthony Cella , Kyle Erik Litz , Joseph John Shiang , Qing Ye
发明人： Kelly Scott Chichak , James Anthony Cella , Kyle Erik Litz , Joseph John Shiang , Qing Ye
IPC分类号： H01L51/54 , C09K11/06
CPC分类号： H01L51/0085 , H01L51/0035 , H01L51/004 , H01L51/0043 , H01L51/5016 , Y02E10/549 , Y10S428/917
摘要： The present invention provides electronic devices comprising novel polymeric organic iridium compositions which provide for enhanced device performance. The polymeric organic iridium compositions employed comprise a polymeric organic iridium compound comprising at least one cyclometallated ligand and at least one ketopyrrole ligand. The polymeric organic iridium compositions employed are referred to as Type (2) organic iridium compositions and are constituted such that at least one ligand of the polymeric organic iridium compound has a number average molecular weight of 2,000 grams per mole or greater (as measured by gel permeation chromatography). Type (2) organic iridium compositions are referred to herein as comprising “polymeric organic iridium complexes”. In one aspect, the present invention provides optoelectronic devices, such as OLED devices and photovoltaic devices. In another aspect, the invention provides OLED devices exhibiting enhanced color properties and light output efficiencies.
摘要翻译：本发明提供了包含新型聚合物有机铱组合物的电子器件，其提供增强的器件性能。所用的聚合有机铱组合物包括含有至少一个环金属配体和至少一个酮基吡咯配体的聚合有机铱化合物。所使用的聚合有机铱组合物称为类型（2）有机铱组合物，并且构成为使得聚合有机铱化合物的至少一种配体的数均分子量为每摩尔或更大2000克（通过凝胶测量）渗透色谱）。类型（2）有机铱组合物在本文中被称为包含“聚合有机铱络合物”。在一个方面，本发明提供了诸如OLED器件和光伏器件之类的光电器件。在另一方面，本发明提供具有增强的颜色特性和光输出效率的OLED器件。

67. 发明申请

US20080145665A1 BIS-CARBAZOLE MONOMERS AND POLYMERS 有权
标题翻译：双酚A单体和聚合物
公开(公告)号：US20080145665A1
公开(公告)日：2008-06-19
申请号：US11610032
申请日：2006-12-13
申请人： Qing Ye , Jie Liu , James Anthony Cella , Kyle Erik Litz , Joseph John Shiang
发明人： Qing Ye , Jie Liu , James Anthony Cella , Kyle Erik Litz , Joseph John Shiang
IPC分类号： B32B27/36 , B32B27/00 , C08F26/12
CPC分类号： C07D209/88 , C08G63/6854 , C08G64/12 , C08G73/1046 , C08G73/1085 , H01L51/0035 , H01L51/0037 , H01L51/0072 , H01L51/0085 , H01L51/5012 , Y10T428/31507 , Y10T428/31721 , Y10T428/31786
摘要： The invention relates to compounds of formula I wherein R1, R2, and R4 are independently at each occurrence a C1-C20 aliphatic radical, a C3-C20 aromatic radical, or a C3-C20 cycloaliphatic radical; R3 and R5 are independently at each occurrence hydrogen, a C1-C20 aliphatic radical, a C3-C20 aromatic radical, or a C3-C20 cycloaliphatic radical; and a, b and d are independently 0 or an integer ranging from 1 to 3. The invention further relates to polymers derived from compounds of formula I. The polymers may be polyesters, polyethers, polycarbonates, polyestercarbonates, polyetherketones, or polyethersulfones. Compounds and polymers of the invention find use in light emitting devices.
摘要翻译：本发明涉及式I化合物，其中R 1，R 2，R 4和R 4各自独立地为C 1 C 20 -C 20脂肪族基团，C 3 -C 20芳族基团或C 3 H 3 -C 20脂环族基团; R 3和R 5在每次出现时独立地为氢，C 1 -C 20脂族基团， C 3 -C 20芳族基团或C 3 -C 20脂环族基团; C 3 -C 20芳族基团或C 3 -C 20 -C 20脂环族基团; 并且a，b和d独立地为0或1至3的整数。本发明还涉及衍生自式I化合物的聚合物。聚合物可以是聚酯，聚醚，聚碳酸酯，聚酯碳酸酯，聚醚酮或聚醚砜。本发明的化合物和聚合物可用于发光器件。

68. 发明申请

US20080026477A1 Method for preparing polymeric organic iridium compositions 有权
标题翻译：聚合有机铱组合物的制备方法
公开(公告)号：US20080026477A1
公开(公告)日：2008-01-31
申请号：US11599972
申请日：2006-11-15
申请人： James Anthony Cella , Kelly Scott Chichak
发明人： James Anthony Cella , Kelly Scott Chichak
IPC分类号： G01N33/20
CPC分类号： C07F15/0033 , C07B2200/11 , H01L51/0035 , H01L51/0085 , H01L51/5012 , Y10S428/917
摘要： The present invention provides a method for the preparation of polymeric organic iridium complexes useful in electronic devices such as OLEDs. The method provides polymeric organic iridium compositions comprising at least one cyclometallated ligand and at least one ketopyrrole ligand. The polymeric organic iridium compositions provided are referred to as Type (2) organic iridium compositions and are constituted such that at least one ligand of the polymeric organic iridium compound has a number average molecular weight of 2,000 grams per mole or greater (as measured by gel permeation chromatography). Type (2) organic iridium compositions are referred to herein as comprising “polymeric organic iridium complexes”. In one embodiment, the method comprises providing a non-polymeric organic iridium complex comprising one or more reactive functional groups and carrying out a polymerization step to provide the polymeric organic iridium complex comprising at least one cyclometallated ligand and at least one ketopyrrole ligand.
摘要翻译：本发明提供了制备用于诸如OLED的电子器件中的聚合有机铱络合物的方法。该方法提供包含至少一种环金属配体和至少一种酮吡咯配体的聚合有机铱组合物。提供的聚合有机铱组合物称为类型（2）有机铱组合物，并且构成为使得至少一种高分子有机铱化合物的配位体的数均分子量为每摩尔或更大2000克（通过凝胶测量）渗透色谱）。类型（2）有机铱组合物在本文中被称为包含“聚合有机铱络合物”。在一个实施方案中，该方法包括提供包含一个或多个反应性官能团的非聚合有机铱络合物，并进行聚合步骤以提供包含至少一种环金属配体和至少一种酮吡咯配体的聚合有机铱络合物。

69. 发明申请

US20080026249A1 Electronic devices comprising organic iridium compositions 有权
标题翻译：包含有机铱组合物的电子器件
公开(公告)号：US20080026249A1
公开(公告)日：2008-01-31
申请号：US11506002
申请日：2006-08-17
申请人： Kelly Scott Chichak , James Anthony Cella , Kyle Erik Litz , Joseph John Shiang , Qing Ye , Kevin Henry Janora , Gautam Parthasarathy
发明人： Kelly Scott Chichak , James Anthony Cella , Kyle Erik Litz , Joseph John Shiang , Qing Ye , Kevin Henry Janora , Gautam Parthasarathy
IPC分类号： H01L51/54 , C09K11/06
CPC分类号： H01L51/0085 , C09K11/06 , C09K2211/1029 , C09K2211/1037 , C09K2211/1044 , C09K2211/1088 , C09K2211/1092 , C09K2211/1466 , C09K2211/1475 , C09K2211/185 , H01L51/0035 , H01L51/0039 , H01L51/0043 , H01L51/5016 , H01L51/5048 , H01L51/5088 , H05B33/14 , Y02E10/549 , Y10S428/917
摘要： The present invention provides electronic devices comprising novel organic iridium compositions which provide for enhanced device performance. The novel iridium compositions employed comprise at least one novel organic iridium compound which comprises at least one cyclometallated ligand and at least one ketopyrrole ligand. The organic iridium compositions employed are referred to as Type (1) organic iridium compositions and are constituted such that no ligand of the novel organic iridium compound has a number average molecular weight of 2,000 grams per mole or greater (as measured by gel permeation chromatography). Type (1) organic iridium compositions are referred to herein as comprising “organic iridium complexes”. In one aspect, the present invention provides optoelectronic devices, such as OLED devices and photovoltaic devices. In another aspect, the invention provides OLED devices exhibiting enhanced color properties and light output efficiencies.
摘要翻译：本发明提供了包含新型有机铱组合物的电子器件，其提供增强的器件性能。所用的新型铱组合物包含至少一种包含至少一种环金属配体和至少一种酮基吡咯配体的新型有机铱化合物。使用的有机铱组合物称为类型（1）有机铱组合物，并且构成为使得新型有机铱化合物的配体的数均分子量为每摩尔或更大2000克（通过凝胶渗透色谱法测量）。类型（1）有机铱组合物在本文中被称为包含“有机铱络合物”。在一个方面，本发明提供了诸如OLED器件和光伏器件之类的光电器件。在另一方面，本发明提供具有增强的颜色特性和光输出效率的OLED器件。

70. 发明授权

US07259223B2 Process for the production of polycarbonate 有权
标题翻译：聚碳酸酯生产工艺
公开(公告)号：US07259223B2
公开(公告)日：2007-08-21
申请号：US10802705
申请日：2004-03-17
申请人： Hans Peter Brack , James Anthony Cella , Dennis Karlik , Lina Prada
发明人： Hans Peter Brack , James Anthony Cella , Dennis Karlik , Lina Prada
IPC分类号： C08G64/00
CPC分类号： C08G64/14 , C08G64/307
摘要： A process for the production of polycarbonate having increased end-cap levels, the process comprising adding a terminal blocking agent of the formula: wherein R1 is a propoxy or butoxy and R2 is selected from the group consisting of C1-C30 alkyl, C1-C30 alkoxy, C6-C30 aryl, C7-C30 aralkyl, and C6-C30 aryloxy.
摘要翻译：一种生产具有增加的端帽水平的聚碳酸酯的方法，该方法包括加入下式的封端剂：其中R 1是丙氧基或丁氧基，R 2是 >选自C 1 -C 30烷基，C 1 -C 30烷氧基，C 1 -C 30烷基， C 6 -C 30芳基，C 7 -C 30芳烷基和C 6 - 仲-C 30芳氧基。

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