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61. 发明授权

US5306851A High viscosity index lubricant fluid 失效
标题翻译：高粘度指数润滑油
公开(公告)号：US5306851A
公开(公告)日：1994-04-26
申请号：US979962
申请日：1992-11-23
申请人： Margaret M. Wu , Dong-Ming Shen , Catherine S. H. Chen
发明人： Margaret M. Wu , Dong-Ming Shen , Catherine S. H. Chen
IPC分类号： C07C13/615 , C10M105/04 , C10M127/02 , C10M171/00 , C10M127/00
CPC分类号： C10M127/02 , C07C13/615 , C10M105/04 , C10M171/002 , C07C2103/74 , C10M2203/02 , C10M2203/022 , C10M2203/024 , C10M2203/04 , C10N2240/08
摘要： The invention provides a composition comprising at least about 10 different diamondoid compounds selected from the group consisting of methyl-substituted and ethyl-substituted adamantane, diamantane, and triamantane, wherein each of said selected diamondoid compounds comprises no more than about 10 weight percent of said composition. The composition is useful as high quality lubricating fluid and exhibits the unusual combination of high Viscosity Index and very low pour point.
摘要翻译：本发明提供包含至少约10种不同的金刚石类化合物的组合物，其选自甲基取代的和乙基取代的金刚烷，金刚烷和三金刚，其中所述选择的金刚石类化合物中的每一种包括不超过所述组成。该组合物可用作高品质润滑液，并且具有高粘度指数和极低倾点的不寻常组合。

62. 发明授权

US5276229A High VI synthetic lubricants from thermally cracked slack wax 失效
标题翻译：来自热裂的松散蜡的高VI合成润滑剂
公开(公告)号：US5276229A
公开(公告)日：1994-01-04
申请号：US903392
申请日：1992-06-24
申请人： J. Scott Buchanan , Margaret M. Wu
发明人： J. Scott Buchanan , Margaret M. Wu
IPC分类号： C10M107/10 , C07C2/74 , C07C2/02
CPC分类号： C10M107/10 , C10M2205/028 , C10M2205/14 , C10M2205/16 , C10M2205/17 , C10M2205/18
摘要： A process for the production of synthetic lubricants having high viscosity index by oligomerizing a mixture of alpha-olefins produced from the thermal cracking of slack wax or recycled slack wax. The oligomerization is carried out with a reduced metal oxide catalyst, preferably a carbon monoxide reduced chromium oxide on a silica support. The olefin product from the thermal cracking step is purified, preferably by hydrotreating prior to the oligomerization step.
摘要翻译：一种制备具有高粘度指数的合成润滑剂的方法，其通过由松散蜡或回收的松散蜡的热裂解产生的α-烯烃的混合物进行低聚。低聚反应用二氧化硅载体上还原的金属氧化物催化剂，优选一氧化碳还原的氧化铬进行。来自热裂解步骤的烯烃产物被纯化，优选在低聚步骤之前通过加氢处理。

63. 发明授权

US5157177A VI enhancing compositions and newtonian lube blends 失效
标题翻译： VI增强组合物和牛顿润滑剂混合物
公开(公告)号：US5157177A
公开(公告)日：1992-10-20
申请号：US686639
申请日：1991-04-17
申请人： Bruce P. Pelrine , Margaret M. Wu
发明人： Bruce P. Pelrine , Margaret M. Wu
IPC分类号： C08F10/14 , C08F110/14 , C08F210/14 , C10G50/02 , C10M143/08
CPC分类号： C08F10/14 , C10G50/02 , C10M143/08 , C08F110/14 , C08F210/14 , C10M2205/00 , C10M2205/028 , C10N2220/02 , Y02P20/582
摘要： A novel composition is disclosed that is particularly useful as a lubricant viscosity index improver. The composition comprises branched C.sub.30 -C.sub.10000 hydrocarbons that have a branch ratio of less than 0.19 and viscosity at 100.degree. C. between 725 cS and 15,000 cS. The novel compositions comprise the product of the oligomerization of C.sub.6 to C.sub.20 alpha-olefin feedstock, or mixtures thereof, under oligomerization conditions at a temperature between -20.degree. C. and +90.degree. C. in contact with a reduced valence state Group VIB metal catalyst on porous support. The compositions have viscosities at 100.degree. C. between 725 cS and 15,000 cS. Using the foregoing compositions in admixture with mineral oil and synthetic lubricants provides novel lubricant blends that show an elevated viscosity index. The mixtures also show an increased stability to shear stress at high temperature with all blends notable by exhibiting Newtonian flow.
摘要翻译：公开了作为润滑剂粘度指数改进剂特别有用的新型组合物。该组合物包含分支比小于0.19且在100℃下的粘度在725cS和15,000cS之间的支链C30-C10000烃。该新型组合物包括C6-C20α-烯烃原料低聚的产物，或其混合物，在低温条件下，在-20℃至+ 90℃之间的温度下与还原的化合价VIB金属多孔载体上的催化剂。组合物在100℃下的粘度在725cS和15,000cS之间。使用与矿物油和合成润滑剂混合的上述组合物提供显示升高的粘度指数的新型润滑剂共混物。混合物还显示出在高温下对剪切应力的稳定性增加，所有共混物通过显示牛顿流动显着。

64. 发明授权

US5105038A Synthetic polyolefin lubricant blends 失效
标题翻译：合成聚烯烃润滑剂混合物
公开(公告)号：US5105038A
公开(公告)日：1992-04-14
申请号：US623840
申请日：1990-12-07
申请人： Catherine S. H. Chen , Margaret M. Wu
发明人： Catherine S. H. Chen , Margaret M. Wu
IPC分类号： C10M169/04
CPC分类号： C10M169/041 , C10M2203/0206 , C10M2205/024 , C10M2205/0245 , C10M2205/026 , C10M2205/0265 , C10M2205/028 , C10N2220/02
摘要： Synthetic lubricant blends exhibiting superior lubricant properties such as high viscosity index, including mixtures of oligomeric products of shape selective catalysis with other lubricants, such as high viscosity index poly-alpha-(.alpha.-)olefins lubricant basestock, conventional poly(.alpha.-olefin) and/or other liquid lubricant basestock material.Preferred lubricant mixtures comprise hydrogenated components:a) a low viscosity C.sub.20 -C.sub.60 lubricant range liquid comprising substantially linear hydrocarbon moietoes prepared by shape selective catalysis of lower olefin with medium pore acid zeolite catalyst to provide substantially linear liquid olefinic intermediates or C.sub.20.sup.+ lubricants, said lubricant range liquid having a kinematic viscosity of about 2-10 cS at 100.degree. C.; andb) at least one poly(.alpha.-olefin) having viscosity greater than 20 cS and viscosity index improvement properties.
摘要翻译：合成润滑剂共混物表现出优异的润滑性能，例如高粘度指数，包括形状选择性催化与其它润滑剂的低聚产物的混合物，例如高粘度指数聚-α-（α-）烯烃润滑剂基础油，常规聚（α-烯烃）和/或其它液体润滑剂基础材料。优选的润滑剂混合物包括氢化组分：a）低粘度的C 20 -C 60润滑剂范围液体，其包含基本上由线性烃气溶胶组成，所述烃气溶胶通过低分子烯烃与中孔酸沸石催化剂的形状选择性催化制备，以提供基本上线性的液体烯烃中间体或C20 +润滑剂，所述润滑剂在100℃下运动粘度为约2-10cS的范围液体; 和b）至少一种粘度大于20cS的聚（α-烯烃）和粘度指数改进性能。

65. 发明授权

US4969522A Polymer-coated support and its use as sand pack in enhanced oil recovery 失效
标题翻译：聚合物涂层载体及其作为砂包在增强采油中的应用
公开(公告)号：US4969522A
公开(公告)日：1990-11-13
申请号：US288334
申请日：1988-12-21
申请人： Darrell D. Whitehurst , Margaret M. Wu
发明人： Darrell D. Whitehurst , Margaret M. Wu
IPC分类号： C09K8/565 , C09K8/575
CPC分类号： C09K8/5756 , C09K8/565 , Y10T428/2998
摘要： A non-friable support, e.g., sand, coated with a polymer is prepared by contacting the support containing a polymerization catalyst with a monomer which is at least one multi-functional olefin, e.g., a diene, under monomer polymerization conditions. The product of the polymerization process is a highly cross-linked coating which engulfs the support, thereby rendering it hydrolytically and thermally stable. The support can be used as a sand pack in enhanced oil recovery operations, wherein it is resistant to deterioration due to high temperature, pressure and alkaline conditions existing in the subterranean formations.
摘要翻译：通过在单体聚合条件下使包含聚合催化剂的载体与至少一种多官能烯烃（例如二烯）的单体接触来制备涂覆有聚合物的非易碎载体，例如砂。聚合过程的产物是一种高度交联的涂层，其吸收载体，从而使其具有水解和热稳定性。该支撑体可以用作强化采油操作中的砂堆，其中耐地层中存在高温，高压和碱性条件的劣化。

66. 发明授权

US4912272A Lubricant blends having high viscosity indices 失效
标题翻译：具有高粘度指数的润滑剂共混物
公开(公告)号：US4912272A
公开(公告)日：1990-03-27
申请号：US210454
申请日：1988-06-23
申请人： Margaret M. Wu
发明人： Margaret M. Wu
IPC分类号： C10M105/04 , C10M107/02 , C10M111/04 , C10M127/02 , C10N20/00 , C10N20/04 , C10N30/02 , C10N60/02 , C10N70/00
CPC分类号： C10M111/04 , C10M2203/02 , C10M2203/022 , C10M2203/024 , C10M2203/04 , C10M2203/1006 , C10M2203/1025 , C10M2203/1045 , C10M2203/1065 , C10M2203/1085 , C10M2205/0206 , C10M2205/024 , C10M2205/026 , C10M2205/028 , C10M2205/0285 , C10M2209/08 , C10M2209/084 , C10M2209/0845 , C10M2209/0863 , C10M2209/101 , C10M2209/1013 , C10M2209/102 , C10M2209/1023 , C10M2209/1033 , C10M2209/1045 , C10M2209/1055 , C10M2209/1065 , C10M2209/1075 , C10M2209/1085 , C10M2209/1095 , C10M2211/06 , C10M2213/00 , C10M2213/02 , C10M2213/023 , C10M2213/043 , C10M2213/0606 , C10M2213/062 , C10M2213/0623 , C10M2217/0403 , C10M2217/0415 , C10M2217/0425 , C10M2217/0435 , C10M2217/044 , C10M2217/0443 , C10M2217/045 , C10M2217/0453 , C10M2217/0465 , C10M2221/003 , C10M2221/025 , C10M2221/0405 , C10N2220/02
摘要： Novel lubricant mixtures are disclosed having unexpectedly high viscosity indices. The mixtures are blends of high viscosity index polyalphaolefins prepared with activated chromium on silica catalyst and polyalphaolefins prepared with BF3, aluminum chloride, or Ziegler-type catayst. Superior blends are also prepared from HVIXPAO with mineral oil and/or other synthetic liquid lubricants.
摘要翻译：公开了具有出乎意料的高粘度指数的新型润滑剂混合物。混合物是由二氧化硅催化剂上活化的铬制备的高粘度指数的聚α-烯烃与用BF 3，氯化铝或齐格勒型催化剂制备的聚α-烯烃的共混物。还可以使用矿物油和/或其他合成液体润滑剂从HVI＆upbar＆XPAO制备优质混合物。

67. 发明授权

US4876321A Preparation of alpha-olefin polymers of relatively narrow molecular weight distribution 失效
标题翻译：制备相对较窄分子量分布的α-烯烃聚合物
公开(公告)号：US4876321A
公开(公告)日：1989-10-24
申请号：US17285
申请日：1987-02-20
申请人： Frederick Y. Lo , Thomas E. Nowlin , Margaret M. Wu
发明人： Frederick Y. Lo , Thomas E. Nowlin , Margaret M. Wu
IPC分类号： C08F4/02 , C08F10/00
CPC分类号： C08F10/00 , Y10S526/901
摘要： A catalyst composition for polymerizing alpha-olefins is prepared by treating a carrier containing OH groups with a liquid solution containing an excess of an organomagnesium composition with respect to the OH groups and contacting the thus-formed magnesium-containing carrier with a hydrocarbyl alcohol and at least one transition metal compound. Prior to contacting the magnesium-containing carrier with the alcohol, most of the liquid must be removed therefrom, so that it comprises not more than about 6% of the liquid. The amount of the transition metal compound is such that the molar ratio thereof to magnesium in the reaction mixture is about 0.3 to about 0.9. Also disclosed is a process for polymerizing alpha-olefins in the presence of the catalyst of the invention.
摘要翻译：用于聚合α-烯烃的催化剂组合物通过用含有过量的有机镁组合物的液体溶液相对于OH基团处理含有OH基团的载体并将如此形成的含镁载体与烃基接触并在至少一种过渡金属化合物。在使含镁载体与醇接触之前，大部分液体必须从其中除去，使其不超过约6％的液体。过渡金属化合物的量使得其与反应混合物中的镁的摩尔比为约0.3至约0.9。还公开了在本发明催化剂存在下聚合α-烯烃的方法。

68. 发明授权

US4760121A Preparation of alpha-olefin polymers of relatively narrow molecular weight distrbution 失效
标题翻译：制备相对较窄分子量分布的α-烯烃聚合物
公开(公告)号：US4760121A
公开(公告)日：1988-07-26
申请号：US17289
申请日：1987-02-20
申请人： Frederick Y. Lo , Thomas E. Nowlin , Margaret M. Wu
发明人： Frederick Y. Lo , Thomas E. Nowlin , Margaret M. Wu
IPC分类号： C08F4/64 , C08F10/00
CPC分类号： C08F10/00 , Y10S526/901
摘要： A catalyst composition for polymerizing alpha-olefins is prepared by treating a carrier containing OH groups with a liquid solution containing an excess of an organomagnesium composition with respect to the OH groups and contacting the thus-formed magnesium-containing carrier with a solution of at least one transition metal compound. Prior to contacting the magnesium-containing carrier with the transition metal compound, most of the liquid must be removed therefrom, so that it comprises not more than about 6% of the liquid. The amount of the transition metal compound is such that the molar ratio of the transition metal to magnesium in the reaction mixture is about 0.3 to about 0.9. Also disclosed is a process for polymerizing alpha-olefins in the presence of the catalyst of the invention.
摘要翻译：用于聚合α-烯烃的催化剂组合物通过用含有过量的有机镁组合物的液体溶液相对于OH基团处理含有OH基团的载体来制备，并将如此形成的含镁载体与至少一种过渡金属化合物。在使含镁载体与过渡金属化合物接触之前，必须从其中除去大部分液体，使其含有不超过约6％的液体。过渡金属化合物的量使得反应混合物中过渡金属与镁的摩尔比为约0.3至约0.9。还公开了在本发明催化剂存在下聚合α-烯烃的方法。

69. 发明授权

US4677087A Catalyst composition for polymerizing alpha-olefin polymers of relatively narrow molecular weight distribution 失效
标题翻译：用于聚合具有相对较窄分子量分布的α-烯烃聚合物的催化剂组合物
公开(公告)号：US4677087A
公开(公告)日：1987-06-30
申请号：US816091
申请日：1986-01-03
申请人： Frederick Y. Lo , Thomas E. Nowlin , Margaret M. Wu
发明人： Frederick Y. Lo , Thomas E. Nowlin , Margaret M. Wu
IPC分类号： C08F4/60 , C08F4/62 , C08F4/64 , C08F10/00 , C08F4/68
CPC分类号： C08F10/00
摘要： A catalyst composition for polymerizing alpha-olefins is prepared by treating a carrier containing OH groups with a liquid solution containing an excess of an organomagnesium composition with respect to the OH groups and contacting the thus-formed magnesium-containing carrier with a solution of at least one transition metal compound. Prior to contacting the magnesium-containing carrier with the transition metal compound, most of the liquid must be removed therefrom, so that it comprises not more than about 6% of the liquid. The amount of the transition metal compound is such that the molar ratio of the transition metal to magnesium in the reaction mixture is about 0.3 to about 0.9. Also disclosed is a process for polymerizing alpha-olefins in the presence of the catalyst of the invention.
摘要翻译：用于聚合α-烯烃的催化剂组合物通过用含有过量的有机镁组合物的液体溶液相对于OH基团处理含有OH基团的载体来制备，并将如此形成的含镁载体与至少一种过渡金属化合物。在使含镁载体与过渡金属化合物接触之前，必须从其中除去大部分液体，使其含有不超过约6％的液体。过渡金属化合物的量使得反应混合物中过渡金属与镁的摩尔比为约0.3至约0.9。还公开了在本发明催化剂存在下聚合α-烯烃的方法。

70. 发明授权

US4449961A Process for light olefin production 失效
标题翻译：轻烯烃生产工艺
公开(公告)号：US4449961A
公开(公告)日：1984-05-22
申请号：US474842
申请日：1983-03-14
申请人： Nancy P. Forbus , Margaret M. Wu
发明人： Nancy P. Forbus , Margaret M. Wu
IPC分类号： B01J29/50 , B01J29/70 , B01J29/90 , C07C1/20
CPC分类号： B01J29/06 , B01J29/50 , B01J29/70 , B01J29/7015 , B01J29/90 , C07C1/20 , B01J2229/26 , B01J2229/42 , C07C2529/50 , C07C2529/70 , Y02P20/52 , Y02P20/584 , Y02P30/42
摘要： A process for converting methanol and/or methyl ether to light olefins over a zeolite catalyst comprising at least some crystalline aluminosilicate zeolitic material having pore windows formed by 8-membered rings of oxygen atoms, e.g., Zeolon 500 or ZSM-34, in the presence of hydrogen, or mixtures of hydrogen and carbon monoxide as a gaseous diluent, at elevated temperature and pressure. By using such zeolite catalysts, hydrogen-containing diluents and reaction conditions, methanol and/or methyl ether can be converted to an olefin-containing hydrocarbon product enriched in ethylene and propylene with enhanced catalyst lifetime.
摘要翻译：一种在沸石催化剂上将甲醇和/或甲基醚转化成轻质烯烃的方法，该沸石催化剂包含至少一些结晶的硅铝酸盐沸石材料，其具有通过8-元环氧原子形成的孔窗，例如Zeolon 500或ZSM-34 的氢气，或氢气和一氧化碳作为气体稀释剂的混合物，在升高的温度和压力下。通过使用这种沸石催化剂，含氢稀释剂和反应条件，甲醇和/或甲基醚可以转化成富含乙烯和丙烯的含烯烃的烃产物，并具有增强的催化剂寿命。

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