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61. 发明授权

US5562887A Purification of alkyl nitrite-containing exhaust gases 失效
标题翻译：含烷基亚硝酸盐废气的净化
公开(公告)号：US5562887A
公开(公告)日：1996-10-08
申请号：US336365
申请日：1994-11-08
申请人： Heinz Landscheidt , Kaspar Hallenberger , Paul Wagner , Alexander Klausener
发明人： Heinz Landscheidt , Kaspar Hallenberger , Paul Wagner , Alexander Klausener
IPC分类号： B01D53/34 , B01D53/54 , B01D53/56 , B01D53/72 , C01B21/00
CPC分类号： B01D53/56 , B01D53/54 , B01D53/72
摘要： Alkyl nitrite-containing exhaust gases are purified in continuous form by treating them with equimolar to excess amidosulphuric acid in the form of an aqueous solution in the manner of a counter-current scrubbing at a temperature of 0.degree.-100.degree. C.
摘要翻译：含有亚烷基亚烷基的废气通过在0℃-100℃的温度下以逆流洗涤的方式以等摩尔至过量的酰胺硫酸的水溶液的形式，以连续的形式进行纯化。

62. 发明授权

US5543548A Process for the preparation of dimethyl carbonate 失效
标题翻译：碳酸二甲酯的制备方法
公开(公告)号：US5543548A
公开(公告)日：1996-08-06
申请号：US273548
申请日：1994-07-11
申请人： Heinz Landscheidt , Erich Wolters , Paul Wagner , Alexander Klausener
发明人： Heinz Landscheidt , Erich Wolters , Paul Wagner , Alexander Klausener
IPC分类号： C07B61/00 , C07C31/04 , C07C68/00 , C07C68/08 , C07C69/96 , C07C201/04 , C07C203/00
CPC分类号： C07C68/00
摘要： Dimethyl carbonate (DMC) is prepared by continuous gas reaction of carbon monoxide and methyl nitrite a heterogeneous catalyst comprising a platinum at 50.degree. to 170.degree. C. under 1 to 5 bar.
摘要翻译：通过一氧化碳和亚硝酸甲酯的连续气相反应制备碳酸二甲酯（DMC），该催化剂在1至5巴下在50至170℃下包含铂。

63. 发明授权

US5449806A Process for the preparation of dialkyl carbonates 失效
标题翻译：制备碳酸二烷基酯的方法
公开(公告)号：US5449806A
公开(公告)日：1995-09-12
申请号：US272497
申请日：1994-07-08
申请人： Alexander Klausener , Heinz Landscheidt , Reinhard Langer , Paul Wagner
发明人： Alexander Klausener , Heinz Landscheidt , Reinhard Langer , Paul Wagner
IPC分类号： B01J27/13 , B01J21/04 , B01J23/58 , C07B61/00 , C07C68/00 , C07C69/96
CPC分类号： C07C68/00 , B01J21/04 , B01J23/58
摘要： Dialkyl carbonates can be prepared by reacting carbon monoxide with alkyl nitrites in a continuous gas phase reaction in the presence of a catalyst using a fixed bed reactor with a short catalyst bed in the direction of flow. The dialkyl carbonates are formed with almost quantitative selectivity; thermal decomposition of the alkyl nitrite, with the resulting formation of decomposition products, is not observed.
摘要翻译：碳酸二烷基酯可以通过在催化剂存在下在连续气相反应中使一氧化碳与烷基亚硝酸盐反应来制备，所述催化剂使用在流动方向上具有短催化剂床的固定床反应器。以几乎定量的选择性形成碳酸二烷基酯; 没有观察到亚硝酸烷基酯的热分解，从而形成分解产物。

64. 发明授权

US5359118A Process for the continuous preparation of dialkyl carbonates 失效
标题翻译：连续制备碳酸二烷基酯的方法
公开(公告)号：US5359118A
公开(公告)日：1994-10-25
申请号：US059489
申请日：1993-05-10
申请人： Paul Wagner , Franz-Josef Mais , Hans-Josef Buysch , Reinhard Langer , Alexander Klausener
发明人： Paul Wagner , Franz-Josef Mais , Hans-Josef Buysch , Reinhard Langer , Alexander Klausener
IPC分类号： B01J23/08 , C07C68/06 , C07C69/96
CPC分类号： C07C68/065 , Y10S203/06
摘要： Di-(C.sub.1 -C.sub.4 -alkyl) carbonates can be prepared by catalysed counter-current reesterification of ethylene glycol carbonate or propylene glycol carbonate with a C.sub.1 -C.sub.4 -alcohol in a column, ethylene glycol carbonate or propylene glycol carbonate being introduced into the upper part of the column and a dialkyl carbonate-containing C.sub.1 -C.sub.4 -alcohol being introduced into the central or lower part of the column and pure alcohol being additionally introduced below the introduction of the dialkyl carbonate-containing alcohol.
摘要翻译：二 - （C 1 -C 4 - 烷基）碳酸酯可以通过催化的乙二醇碳酸酯或丙二醇碳酸酯与柱中的C 1 -C 4醇的逆流再酯交换，乙二醇碳酸酯或丙二醇碳酸酯引入上层将柱的一部分和含有二烷基碳酸酯的C 1 -C 4醇引入塔的中部或下部，并且在引入含二烷基碳酸酯的醇之外另外引入纯醇。

65. 发明授权

US5350862A Process for the preparation of ethylene glycol carbonate 失效
标题翻译：制备乙二醇碳酸酯的方法
公开(公告)号：US5350862A
公开(公告)日：1994-09-27
申请号：US984789
申请日：1992-12-03
申请人： Paul Wagner , Hans-Josef Buysch , Alexander Klausener , Franz-Josef Mais , Christine Mendoza-Frohn
发明人： Paul Wagner , Hans-Josef Buysch , Alexander Klausener , Franz-Josef Mais , Christine Mendoza-Frohn
IPC分类号： C07B61/00 , C07D317/38 , C07D317/36
CPC分类号： C07D317/38
摘要： A process is described for the catalytic preparation of ethylene glycol carbonate by reaction of ethylene oxide and CO.sub.2 in ethylene glycol carbonate as the reaction medium at elevated temperature and at elevated pressure with work-up by distillation to separate the resulting ethylene glycol carbonate from the catalyst. The process is carried out continuously under adiabatic temperature conditions. Per unit of time, ethylene glycol carbonate as reaction medium runs into the reactor in a amount 10 to 120 times that of ethylene glycol carbonate formed per unit of time. A CO.sub.2 excess over the other reaction partner ethylene oxide is maintained at all sites of the reactor. 80 to 98% by weight of the reaction mixture flowing out is returned to the inlet of the reactor, while the remainder is worked up by distillation to give ethylene glycol carbonate. The sensible heat produced in the reaction product as a result of the adiabatic temperature conditions, is used for the work-up.
摘要翻译：描述了通过环氧乙烷和CO 2在乙二醇碳酸酯中作为反应介质在升高的温度和升高的压力下反应制备乙二醇碳酸酯的方法，通过蒸馏进行后处理以将所得的乙二醇碳酸酯与催化剂分离。该过程在绝热温度条件下连续进行。每单位时间，作为反应介质的乙二醇碳酸酯以每单位时间形成的乙二醇碳酸酯的量的10至120倍的量进入反应器。在反应器的所有位置保持超过其他反应对象环氧乙烷的二氧化碳剩余量。将流出的反应混合物的80〜98重量％返回到反应器的入口，其余部分通过蒸馏处理得到乙二醇碳酸酯。作为绝热温度条件的结果，在反应产物中产生的显热用于后处理。

66. 发明授权

US5344954A Process for the preparation of diaryl carbonates 失效
标题翻译：制备碳酸二芳基酯的方法
公开(公告)号：US5344954A
公开(公告)日：1994-09-06
申请号：US103936
申请日：1993-08-06
申请人： Norbert Schon , Hans-Josef Buysch , Paul Wagner , Reinhard Langer
发明人： Norbert Schon , Hans-Josef Buysch , Paul Wagner , Reinhard Langer
IPC分类号： C07B61/00 , C07C68/06 , C07C69/96
CPC分类号： C07C68/06
摘要： Diaryl carbonates are prepared from dialkyl carbonates and phenolic compounds by transesterification in the presence of a transesterification catalyst at 60.degree.-320.degree. C. in an apparatus composed of two columns in a continuous procedure. In the first column, the starting materials form essentially the associated alkyl aryl carbonate, from which, in the second column, the diaryl carbonate is produced by further transesterification and disproportionation.
摘要翻译：碳酸二芳基酯由碳酸二烷基酯和酚类化合物通过在酯交换催化剂存在下，在60-320℃下在连续方法中由两列组成的装置中制备。在第一列中，起始材料基本上形成缔合的碳酸烷基芳基酯，在第二列中，通过进一步的酯交换和歧化产生碳酸二芳基酯。

67. 发明授权

US5298659A Method for the preparation of azomethines 失效
标题翻译：制备偶氮甲碱的方法
公开(公告)号：US5298659A
公开(公告)日：1994-03-29
申请号：US4349
申请日：1993-01-14
申请人： Reinhard Langer , Hans-Josef Buysch , Paul Wagner
发明人： Reinhard Langer , Hans-Josef Buysch , Paul Wagner
IPC分类号： C07B61/00 , C07C249/02 , C07C251/20
CPC分类号： C07C249/02
摘要： Azomethines can be prepared by the condensation of cycloalkanones and anilines in the presence of acid homogeneous catalysts while the water of reaction is removed azeotropically, the condensation being carried out in a continuous reaction in a column-like reactor to which a temperature profile is applied, the starting materials being fed in in the low-temperature region, and, of the reaction products, the water of reaction to be removed azeotropically being discharged also in the low-temperature region and the azomethine produced being discharged in the high-temperature region.
摘要翻译：偶氮甲碱可以通过在酸均相催化剂存在下环烷酮和苯胺的缩合制备，同时反应水共沸除去，缩合是在连续反应中进行的，其中应用了温度分布的柱状反应器，原料在低温区域进料，反应产物中的共沸脱除反应的水也在低温区域中排出，产生的偶氮甲碱在高温区域排出。

68. 发明授权

US09469697B2 Process for the production of water and solvent-free nitrile rubbers 有权
标题翻译：生产无水和无溶剂丁腈橡胶的方法
公开(公告)号：US09469697B2
公开(公告)日：2016-10-18
申请号：US13635810
申请日：2011-03-21
申请人： Hanns-Ingolf Paul , Paul Wagner , Rolf Feller , Jörg Kirchhoff , John Lovegrove , Florian Forner , Michael Klimpel , Peter Weuta , Sven Brandau
发明人： Hanns-Ingolf Paul , Paul Wagner , Rolf Feller , Jörg Kirchhoff , John Lovegrove , Florian Forner , Michael Klimpel , Peter Weuta , Sven Brandau
IPC分类号： C08L9/02 , C08C2/00 , C08C1/12 , C08C2/02
CPC分类号： C08C2/02 , C08C1/12 , C08C2/00 , C08L9/02
摘要： The present invention relates to specific water and solvent-free nitrile rubbers having specific functional groups and/or end groups, a process for the production thereof and the use thereof. This process involves removing volatile compounds from a fluid (F) containing (1) at least one nitrile rubber and (2) at least one volatile compound, wherein the process comprises at least the steps of a.) treating the fluid (F) in at least one conversation unit, b.) retreating the concentrated fluid from step a.) in at least one retreating unit and c.) feeding the retreated concentrated fluid from step b.) into at least one retreating unit.
摘要翻译：本发明涉及具有特定官能团和/或端基的具体的无水和无溶剂丁腈橡胶，其制备方法及其用途。该方法包括从含有（1）至少一种丁腈橡胶和（2）至少一种挥发性化合物的流体（F）中除去挥发性化合物，其中该方法至少包括以下步骤：a。）将至少一个通话单元，b）将至少一个后退单元中的步骤a。）中的浓缩流体退回，以及c）将从后续处理的浓缩流体从步骤b。进给至至少一个后退单元。

69. 发明授权

US09068031B2 Reactor and method for continuous polymerization 有权
标题翻译：反应器和连续聚合方法
公开(公告)号：US09068031B2
公开(公告)日：2015-06-30
申请号：US13995246
申请日：2011-12-29
申请人： Hanns-Ingolf Paul , Rolf Feller , Paul Wagner , John Lovegrove , Joachim Ritter , Ricarda Leiberich , Jörg Kirchhoff , Udo Wiesner
发明人： Hanns-Ingolf Paul , Rolf Feller , Paul Wagner , John Lovegrove , Joachim Ritter , Ricarda Leiberich , Jörg Kirchhoff , Udo Wiesner
IPC分类号： C08F2/01 , B01J19/18 , C08F136/08 , B01J19/20 , C08F210/12
CPC分类号： C08F136/08 , B01J19/18 , B01J19/1812 , B01J19/1887 , B01J19/20 , B01J2219/00094 , B01J2219/0011 , B01J2219/00159 , B01J2219/00166 , B01J2219/00189 , B01J2219/00245 , B01J2219/00254 , B01J2219/182 , C08F210/12 , C08F236/08 , C08F2/01
摘要： The present invention relates to a reactor (10) and a process for continuous polymerization, where the reactor (10) has an essentially tubular reactor housing (16). The reactor housing (16) has a drive (38) which runs along the geometric central axis (12) in the flow direction (22) and is configured as a central shaft. A rotatably arranged scraper or wiper (36) is provided within the reactor housing (16); the scraper or wiper (36) has at least one scraper or wiper blade (42) to run along an interior side (44) of the reactor housing (16). The rotational movement of the scraper or wiper (36) results in radial mixing of a stream within the reactor housing (16) which dominates gravity effects and, by virtue of shaping of the scrapers or wipers, optionally makes plug flow or a loop flow or backflow within the reactor (10) or else via an additional external pumped circulation system (23) possible. This allows the reaction conditions in the axial direction of the reactor housing (16) to be predicted and individually suitable reaction conditions to be set and controlled along the reactor housing, so that, in particular, a desired molecular weight distribution can be set.
摘要翻译：本发明涉及反应器（10）和连续聚合方法，其中反应器（10）具有基本上管状的反应器壳体（16）。反应器壳体（16）具有在流动方向（22）上沿几何中心轴线（12）延伸并被构造为中心轴的驱动器（38）。在反应器壳体（16）内设置有可旋转地布置的刮刀（36）。刮刀或擦拭器（36）具有至少一个沿着反应器壳体（16）的内侧（44）延伸的刮刀或刮片（42）。刮刀或擦拭器（36）的旋转运动导致在反应器壳体（16）内的流的径向混合，其支配重力作用，并且借助于刮板或刮水器的成形，可选地使塞子流或环流或反应器（10）内的回流，或经由另外的外部泵送循环系统（23）。这允许预测反应器壳体（16）的轴向方向的反应条件，并且可以沿着反应器壳体设置和控制各自适当的反应条件，使得特别地可以设定所需的分子量分布。

70. 发明授权

US08761423B2 Canal hearing devices and batteries for use with same 有权
标题翻译：运河听力装置和电池与其一起使用
公开(公告)号：US08761423B2
公开(公告)日：2014-06-24
申请号：US13303576
申请日：2011-11-23
申请人： Paul Wagner , Stuart Wenzel , Michael Au , Igal Ladabaum
发明人： Paul Wagner , Stuart Wenzel , Michael Au , Igal Ladabaum
IPC分类号： H04R25/00
CPC分类号： H04R25/608 , H04R25/02 , H04R25/30 , H04R25/554 , H04R25/602 , H04R25/604 , H04R25/65 , H04R25/654 , H04R25/658 , H04R2225/023 , H04R2225/49 , H04R2225/61 , H04R2460/17
摘要： Hearing devices configured to fit within the bony portion of the ear canal and batteries that may be used with same. One such hearing device includes a hearing device core, defining a size and a shape, and including a battery and an acoustic assembly, with a microphone and a receiver with a sound port that is adjacent to a portion of the battery, and a flexible seal apparatus on the hearing device core. The size, shape and configuration of the hearing device core, and the flexibility of the seal, are such that the hearing device is positionable within the ear canal bony region with the entire microphone medial of the bony-cartilaginous junction.
摘要翻译：听力装置被配置成装配在耳道的骨部分和可以与其一起使用的电池。一种这样的听力装置包括限定尺寸和形状的听力装置芯，并且包括电池和声学组件，麦克风和具有与电池的一部分相邻的声音端口的接收器，以及柔性密封件设备在听力设备核心上。听力装置芯的尺寸，形状和构型以及密封的灵活性使得听力装置可以位于耳道内的骨 - 软骨连接处的整个麦克风内部的耳道骨区域内。

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