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61. 发明公开

KR1020110076668A 탈브롬화제 및 알칼리 화합물에 의한 ＰＢＤＥｓ의 무해화 처리방법 无效
标题翻译：通过去除代谢物和碱性化合物的PBDES的脱氧方法
公开(公告)号：KR1020110076668A
公开(公告)日：2011-07-06
申请号：KR1020090133422
申请日：2009-12-29
申请人： 재단법인 포항산업과학연구원
发明人： 김병억 , 사영삼
IPC分类号： A62D3/30
CPC分类号： A62D3/34 , A62D3/36 , A62D3/37 , A62D2101/22
摘要： PURPOSE: A detoxification method of polybrominated diphenyl ethers is provided to safely and easily detoxificate polybrominated diphenyl ethers in the room temperature. CONSTITUTION: A detoxification method of polybrominated diphenyl ethers comprises adding a debrominating agent and an alkali compound to a polybrominated diphenyl ethers-containing solution, and stirring the mixture. A polybrominated diphenyl ethers-containing solution is a polybrominated diphenyl ethers-containing waste solution or polybrominated diphenyl ethers extract.
摘要翻译：目的：提供多溴二苯醚的解毒方法，在室温下安全，方便地解毒多溴二苯醚。构成：多溴二苯醚的解毒方法包括向多溴二苯醚溶液中加入脱溴剂和碱性化合物，并搅拌该混合物。含有多溴二苯醚的溶液是含有多溴二苯醚的废溶液或多溴二苯醚提取物。

62. 发明授权

KR100928971B1 토양에서 ＰＦＯＳ 또는 ＰＦＯＡ를 제거하는 방법 失效
标题翻译：如何从土壤中去除全氟辛烷磺酸或全氟辛酸铵
公开(公告)号：KR100928971B1
公开(公告)日：2009-11-26
申请号：KR1020070135403
申请日：2007-12-21
申请人： 재단법인 포항산업과학연구원
发明人： 김병억 , 김민균 , 사영삼
IPC分类号： B09C1/08
CPC分类号： B09C1/08
摘要： 토양에서 PFOS 또는 PFOA를 제거하는 방법이 제공된다. 상기 토양에서 PFOS 또는 PFOA를 제거하는 방법은 PFOS(Perfluorooctane sulfonate) 또는 PFOA(Perfluorooctanoic acid)로 오염된 토양을 준비하는 단계, 및 산화철 및 수소화 붕소나트륨(NaBH
4 )을 분해제로 사용하여 오염된 토양을 정화하는 단계를 포함한다.
오염된 토양, PFOS, PFOA, 산화철, 수소화 붕소나트륨
摘要翻译：提供了从土壤中去除PFOS或PFOA的方法。的如何删除PFOA或PFOS在土壤中的步骤制备污染土壤（全氟辛烷磺酸）或（全氟辛酸）PFOA PFOS和氧化铁和硼氢化钠（添加NaBH

63. 发明公开

KR1020080030291A 전자파 조사 및 산화제 및/또는 환원제를 사용한ＰＡＨｓ로 오염된 토양 및 물의 정화방법 无效
标题翻译：通过微波和氧化剂和/或还原产生PAHS的脱氧方法
公开(公告)号：KR1020080030291A
公开(公告)日：2008-04-04
申请号：KR1020060096188
申请日：2006-09-29
申请人： 재단법인 포항산업과학연구원
发明人： 김병억 , 김민균 , 사영삼
IPC分类号： B09C1/08
CPC分类号： B09C1/08 , A62D3/37 , A62D3/38 , C02F1/30
摘要： A method is provided to purify the contaminated soil or water within a short time without less affecting the environment by adding an oxidizer and/or a reductant to contaminated soil or water containing PAHs(Poly Aromatic Hydrocarbons) and irradiating electromagnetic waves onto the mixture. A method for purifying a material contaminated with PAHs(Poly Aromatic Hydrocarbons) comprises the steps of: adding an oxidizer, a reductant, or a mixture thereof to a material containing PAHs(Poly Aromatic Hydrocarbons); and irradiating electromagnetic waves onto the mixture to decompose the PAHs(Poly Aromatic Hydrocarbons). The oxidizer is hydrogen peroxide or superphosphate. The reductant is at least one of an ion-based reductant of FeCl2 or Fe metal, NaH2PO4, or Na2S. The electromagnetic waves are irradiated onto the material after sealing a material to which the oxidizer or the reductant is added, and which contains the PAHs(Poly Aromatic Hydrocarbons). The electromagnetic waves have a frequency of 2000 to 3000 MHz. The material containing PAHs(Poly Aromatic Hydrocarbons) is soil or water.
摘要翻译：提供了一种在短时间内净化污染的土壤或水的方法，而不会通过向污染的土壤或含有多环芳烃（多芳烃）的水中加入氧化剂和/或还原剂并且向混合物照射电磁波来影响环境。用于纯化被多环芳烃（Poly Aromatic Carbonons）污染的材料的方法包括以下步骤：将氧化剂，还原剂或其混合物加入到含有PAH（聚芳香族烃）的材料中; 并将电磁波照射到混合物上以分解PAH（聚芳香族烃）。氧化剂是过氧化氢或过磷酸盐。还原剂是FeCl 2或Fe金属，NaH 2 PO 4或Na 2 S的离子基还原剂中的至少一种。在密封添加了氧化剂或还原剂的材料之后，将电磁波照射到材料上，并含有PAH（聚芳香族烃）。电磁波的频率为2000〜3000MHz。含有多环芳烃（Poly Aromatic Carbonants）的物质是土壤或水。

64. 发明公开

KR1020070066727A 금속촉매 및 알카리에 의한 ＰＣＢｓ의 무해화 처리방법 无效
标题翻译：金属催化剂和碱性化合物PCBS的脱氧方法
公开(公告)号：KR1020070066727A
公开(公告)日：2007-06-27
申请号：KR1020050128190
申请日：2005-12-22
申请人： 재단법인 포항산업과학연구원
发明人： 김병억 , 김민균 , 사영삼
IPC分类号： B09B3/00 , B01D11/02 , A62D3/30
CPC分类号： B09B3/0016 , A62D3/30 , B01D11/02
摘要： A method for detoxifying contaminants containing PCBs(polychlorinated biphenyls) at a room temperature easily, safely and inexpensively by using a metal catalyst and an alkali is provided. A detoxification method of PCBs(polychlorinated biphenyls) comprises agitating contaminants containing PCBs in an extract obtained using an organic solvent as an extraction solvent in the presence of a nickel catalyst and alkali. The nickel catalyst is presented in an amount range from 2.5 to 10 g per 100 ml of the extract. The alkali is presented in an amount range from 0.5 to 1 g per 100 ml of the extract.
摘要翻译：提供了通过使用金属催化剂和碱容易，安全且廉价地在室温下对含有多氯联苯（多氯联苯）的污染物进行解毒的方法。 PCBs（多氯联苯）的解毒方法包括在镍催化剂和碱存在下，使用有机溶剂作为萃取溶剂，将含有PCBs的污染物搅拌。镍催化剂的存在量为每100ml提取物2.5至10g。碱的含量为每100ml提取物0.5至1g。

65. 发明授权

KR100644518B1 수중에 함유된 염소계 유기화합물 추출 방법 失效
标题翻译： 수중에함유된염소계유기화합물추출방법
公开(公告)号：KR100644518B1
公开(公告)日：2006-11-10
申请号：KR1020050103913
申请日：2005-11-01
申请人： 재단법인 포항산업과학연구원
发明人： 김병억 , 김민균 , 사영삼
IPC分类号： B01D15/02 , B01D11/02 , B01D17/022
摘要： A method for extracting chlorine organic compound contained in the water is provided to carry out the extraction in a short time with improved extraction efficiency by using a water-soluble adsorption agent. A method for extracting chlorine organic compound contained in the water includes the steps of oxidizing cokes powder by adding oxygenated water to the cokes powder and filtering to recover the cokes powder. An NaOH solution is added to the cokes powder for alkaline treatment. The result is filtered and recovered to form a water-soluble adsorption agent. 0.0001-0,001we% of the water-soluble adsorption agent is added to a subject water and the mixture is stirred. A cationic organic cohesive agent is added to the subject water and stirred, a weight of the cationic organic cohesive agent is 25-30 times of the weight of the water-soluble adsorption agent. A sample adsorbing chlorine organic compound is cohered. The subject water is filtered to recover the sample.
摘要翻译：提供一种提取水中含有的氯有机化合物的方法，通过使用水溶性吸附剂，在短时间内提取萃取效率提高。提取水中含有的氯有机化合物的方法包括通过向焦炭粉添加氧化水并过滤回收焦炭粉来氧化焦炭粉的步骤。向焦炭粉中加入NaOH溶液进行碱处理。将结果过滤并回收以形成水溶性吸附剂。将0.0001-0.001重量％的水溶性吸附剂加入到水中并搅拌混合物。将阳离子有机粘结剂加入到水中并搅拌，阳离子有机粘结剂的重量为水溶性吸附剂重量的25-30倍。吸附氯有机化合物的样品被凝聚。将对象水过滤以回收样品。

66. 发明授权

KR100453914B1 산화 및 탈염소화에 의한 다이옥신의 분해방법 失效
标题翻译： 산화및탈염소화에의한다이옥신의분해방법
公开(公告)号：KR100453914B1
公开(公告)日：2004-10-20
申请号：KR1020010053377
申请日：2001-08-31
申请人： 재단법인 포항산업과학연구원
发明人： 김병억 , 김민균 , 김경태 , 사영삼
IPC分类号： B01D53/38
摘要： PURPOSE: A degradation method of dioxins by peroxidation and dechlorination is provided, which can detoxify dioxine at low temperature, thus eliminating any heating step or treatment facility to treat harmful gas generated during dioxins degradation. CONSTITUTION: The degradation method of dioxins by peroxidation and dechlorination is characterized in that first dioxins are oxidized by Fenton's reagent at 15 to 300 deg.C, and then treated by alkali such as KOH and NaOH in the presence of polyethylene glycol serving as phase transfer catalyst.
摘要翻译：目的：提供过氧化和脱氯降解二恶英的方法，它可以在低温下对二恶英进行解毒，从而消除任何加热步骤或处理设施，以处理在二恶英降解过程中产生的有害气体。结构：过氧化和脱氯的二恶英的降解方法的特征在于，第一种二恶英在15-300℃用Fenton试剂氧化，然后在聚乙二醇存在下用碱处理，例如KOH和NaOH处理，作为相转移催化剂。

67. 发明公开

KR1020030018810A 산화 및 탈염소화에 의한 다이옥신의 분해방법 失效
标题翻译：通过过氧化和脱氯的二氧化钛的降解方法
公开(公告)号：KR1020030018810A
公开(公告)日：2003-03-06
申请号：KR1020010053377
申请日：2001-08-31
申请人： 재단법인 포항산업과학연구원
发明人： 김병억 , 김민균 , 김경태 , 사영삼
IPC分类号： B01D53/38
CPC分类号： B01D53/74 , B01D53/62 , B01D53/70
摘要： PURPOSE: A degradation method of dioxins by peroxidation and dechlorination is provided, which can detoxify dioxine at low temperature, thus eliminating any heating step or treatment facility to treat harmful gas generated during dioxins degradation. CONSTITUTION: The degradation method of dioxins by peroxidation and dechlorination is characterized in that first dioxins are oxidized by Fenton's reagent at 15 to 300 deg.C, and then treated by alkali such as KOH and NaOH in the presence of polyethylene glycol serving as phase transfer catalyst.
摘要翻译：目的：提供二恶英通过过氧化和脱氯的降解方法，可在低温下对二恶英进行解毒，从而消除任何加热步骤或处理设施，以处理二恶类降解过程中产生的有害气体。构成：通过过氧化脱氯的二恶英的降解方法的特征在于，第一二氧diox ins by by on on on at at at at at at at at at at at at at transfer transfer transfer transfer transfer transfer transfer transfer transfer transfer transfer transfer transfer transfer transfer transfer 催化剂。

68. 发明公开

KR1020010056201A 염소화반응을 이용한 다이옥신의 신속한 검출방법 失效
标题翻译：通过使用氯化法对二氧化硅进行速度检测的方法
公开(公告)号：KR1020010056201A
公开(公告)日：2001-07-04
申请号：KR1019990058353
申请日：1999-12-16
申请人： 재단법인 포항산업과학연구원
发明人： 김병억 , 김민균 , 사영삼 , 탁진권
IPC分类号： G01N30/02
摘要： PURPOSE: A method for promptly detecting dioxin is provided for accomplishing higher detection limit and correct quantification of dioxin with inexpensive gas chromatography/electron detection device by using antimony chloride to chlorinate dioxin isomers into dioxin octa-chloride. CONSTITUTION: The detection method comprises adding antimony chloride to an extract containing dioxin and heating it to 236-288 deg.C. to produce dioxin octa-chloride; adding HCl to the obtained dioxin octa-chloride to extract hexane material; removing high polar interference material; and detecting dioxin from the extract by means of gas chromatography/electron capturing detector. The method is useful for detecting the dioxin without alternately separating isomers because of the chlorination process and with no requiring commercial pre-treatment step separating isomers.
摘要翻译：目的：提供一种迅速检测二恶英的方法，通过使用氯化锑将二恶英异构体氯化成二恶英八氯化物，实现了较便宜的气相色谱/电子检测装置的检测限和正确定量二恶英。构成：检测方法包括向含有二恶英的提取物中加入氯化锑并加热至236-288℃。产生二恶英八氯化物; 向得到的二恶英八氯化碳中加入HCl以提取己烷物质; 去除高极性干扰材料; 并通过气相色谱/电子捕获检测器从提取物中检测二恶英。该方法可用于检测二恶英而不会因为氯化过程而交替分离异构体，并且不需要分离异构体的商业预处理步骤。

69. 发明公开

KR1020150048955A 일산화탄소 흡수액의 제조방법 및 상기 흡수액을 이용하여 전로가스로부터 일산화탄소를 분리 및 회수하는 방법 有权
标题翻译：用于制备一氧化碳吸收剂的方法，以及使用该方法从LDG气体中分离和回收一氧化碳的方法
公开(公告)号：KR1020150048955A
公开(公告)日：2015-05-11
申请号：KR1020130128569
申请日：2013-10-28
申请人： 재단법인 포항산업과학연구원
发明人： 이시훈 , 최진순 , 김국희 , 임동하 , 김경태 , 사영삼 , 김태훈
IPC分类号： B01D53/14 , B01D53/62 , B01D53/96 , B01D53/74
CPC分类号： Y02A50/2341 , B01D53/14 , B01D53/62 , B01D2257/502
摘要： 본발명은톨루엔의용매에염화구리(Ⅰ) 및염화알루미늄을특정무게비로혼합하여일산화탄소흡수액을제조하는방법을제공하고, 상기흡수액을이용하여전로가스로부터일산화탄소를흡수하고, 흡수된일산화탄소는가열에의해분리및 회수하는방법을제공함으로써, 일산화탄소가다량으로포함된전로가스로부터일산화탄소만을고순도로회수할수 있도록한다.
摘要翻译：在本发明中，提供了通过以一定重量比将氯化铜（I）和氯化铝与甲苯的溶剂混合来制造一氧化碳的方法，以及通过加热分离和收集所吸收的一氧化碳的方法，其中一氧化碳通过使用吸收溶液从LDG气体吸收，从而仅以高产率从具有多种一氧化碳的LDG气体中收集一氧化碳。

70. 发明授权

KR101351941B1 ＰＡＨｓ로 오염된 토양의 정화방법 失效
标题翻译： PAHs污染土壤的脱氧方法
公开(公告)号：KR101351941B1
公开(公告)日：2014-01-22
申请号：KR1020060130251
申请日：2006-12-19
申请人： 재단법인 포항산업과학연구원
发明人： 김병억 , 김민균 , 사영삼
IPC分类号： B09C1/08
摘要： 본 발명은 다환 방향족 탄화수소(PAHs; Poly Aromatic Hydrocarbons)로 오염된 토양 및 해양 퇴적토를 해롭지 않은 토양이 되도록 무해화 처리하는 방법에 관한 것으로, 더욱 상세하게는 산화제를 첨가하고 초음파를 일정시간 조사하는 것에 의해 PAHs를 분해하고 오염된 토양 또는 퇴적토를 정화하는 것을 특징으로 한다.
본 발명에 의하면, PAHs로 오염된 토양 및 퇴적토를 용이하고 안전하게 저 비용으로 무해화 처리가 가능하다. 더구나 반응 후 발생되는 2차 폐기물이 거의 발생되지 않기 때문에 추가적인 환경 오염 등 부작용 없이 오염된 토양을 처리할 수 있는 효과가 있다.

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