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51. 发明专利

JP2001213854A METHOD FOR PRODUCING CYCLOHEXANONE OXIME 失效
公开(公告)号：JP2001213854A
公开(公告)日：2001-08-07
申请号：JP2000024891
申请日：2000-02-02
申请人： ASAHI KASEI CORP
发明人： OGAWA HIROO , KANEJIMA SADATAKA
IPC分类号： B01J27/053 , C07B61/00 , C07C249/10 , C07C251/44
摘要： PROBLEM TO BE SOLVED: To provide a method for producing cyclohexanone oxime by a few processes in high conversion/productivity with small energy consumption under a mild reaction condition by a simple operation/facility. SOLUTION: This method for producing cyclohexanone oxime is characterized in that benzene is used as a starting raw material and production processes comprise (1) a process for partially hydrogenating (A) benzene in the presence of a catalyst (A) to give cyclohexene, (2) a process for nitrating cyclohexene to give nitrocyclohexene and (3) a process for partially hydrogenating (B) nitrocyclohexene in the presence of a catalyst (B) to give cyclohexanone oxime.

52. 发明专利

JPH0755925B2 失效
公开(公告)号：JPH0755925B2
公开(公告)日：1995-06-14
申请号：JP4198286
申请日：1986-02-28
IPC分类号： C08F2/50 , C07C67/00 , C07C239/00 , C07C249/10 , C07C251/62 , G03F7/031

54. 发明专利

JP2005126383A Method for producing halogenoxime derivative 审中-公开
标题翻译：生产杀胡萝卜素衍生物的方法
公开(公告)号：JP2005126383A
公开(公告)日：2005-05-19
申请号：JP2003364720
申请日：2003-10-24
申请人： Ihara Chem Ind Co Ltd , イハラケミカル工業株式会社
发明人： MATSUKAWA KOZO
IPC分类号： C07C249/10 , C07B61/00 , C07C251/34
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a halogenoxime derivative without using diethyl ether as a solvent and without discharging a heavy metal as a waste by a reduction method using an inexpensive and easily available reducing agent, and facilitating the temperature control of the reaction. SOLUTION: The method for producing the halogenoxime derivative represented by general formula (2) (wherein, X is independently a halogen atom) involves reacting a nitromethane derivative represented by general formula (1) (wherein, X is the same as the above) with an inorganic acid in the presence of iron. COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：待解决的问题：提供一种不使用乙醚作为溶剂并且不使用廉价且容易获得的还原剂通过还原方法排出重金属作为废物的卤代肟衍生物的制备方法，并且有助于温度控制反应。解决方案：由通式（2）表示的卤代肟衍生物的制造方法（其中，X独立地为卤素原子）包括使通式（1）表示的硝基甲烷衍生物（其中，X与上述）与无机酸在铁的存在下反应。版权所有（C）2005，JPO＆NCIPI

55. 发明专利

JP2980935B2 失效
公开(公告)号：JP2980935B2
公开(公告)日：1999-11-22
申请号：JP8765190
申请日：1990-04-03
申请人： BAIERU AG
发明人： KURAUSUUHERUMUUTO MYURAA , YOAHIMU KURUTO , KURAUSU KEENITSUHI , KARURUURUDORUFU GATSUSEN , KURUTO FUINDAIZEN , MARUKUSU RINDEITSUHI , KURAUSU RYURUSEN , HANSUUYOAHIMU ZANDERU , ROBERUTO AARU SHUMITSUTO
IPC分类号： A01N47/38 , A01N43/653 , A01N47/36 , C07C61/15 , C07C69/74 , C07C211/37 , C07C233/58 , C07C249/10 , C07C265/10 , C07D249/10 , C07D249/12

56. 发明专利

JPH09509425A 失效
公开(公告)号：JPH09509425A
公开(公告)日：1997-09-22
申请号：JP52234295
申请日：1995-01-17
IPC分类号： C07C45/42 , C07C45/51 , C07C49/167 , C07C249/04 , C07C249/10 , C07C251/38

57. 发明专利

JPH0135822B2 失效
公开(公告)号：JPH0135822B2
公开(公告)日：1989-07-27
申请号：JP8926880
申请日：1980-07-02
申请人： EGYT GYOGYSZERVEGYESZETI GYAR
发明人： ZORUTAAN BUDAI , ARANKA RAI , CHIBORU MESEI , RUITSUA PETOOTSU , KATARIN GURATSUSERU , IBORYA KOSOOTSUKII , ENIKO SUIRUTO , PEETERU GURUGU
IPC分类号： A61K31/15 , A61K31/495 , A61P25/04 , C07C67/00 , C07C239/00 , C07C249/10 , C07C251/58 , C07D295/02 , C07D295/088

58. 发明授权

US10539872B2 Photosensitive composition and compound 有权
公开(公告)号：US10539872B2
公开(公告)日：2020-01-21
申请号：US15323043
申请日：2015-07-14
申请人： TOKYO OHKA KOGYO CO., LTD.
发明人： Yoshinori Tadokoro , Dai Shiota
IPC分类号： G03F7/031 , G03F7/004 , C07C251/66 , C07C45/46 , G02B5/22 , G02F1/1335 , C07C201/12 , C07C249/10 , C07D333/22 , G03F7/00 , C07C333/26
摘要： A photosensitive composition having excellent sensitivity, an insulating film formed using the composition, a color filter formed using the composition, a display device provided with the insulating film or color filter, and a compound suitable for incorporation as a photopolymerization initiator into the composition. This photosensitive composition includes a photopolymerizable compound and a photopolymerization initiator. The photopolymerization initiator contains a compound represented by formula (1) below in which R1 is a hydrogen atom, a nitro group, or a monovalent organic group; R2 and R3 are each an optionally substituted linear alkyl group, an optionally substituted cyclic organic group, or a hydrogen atom, and R2 and R3 may be bonded to one another to form a ring; R4 is a monovalent organic group; R5 is a hydrogen atom, an optionally substituted C1-11 alkyl group, or an optionally substituted aryl group; n is an integer from 0 to 4; and m is 0 or 1.

59. 发明授权

US4395413A Oxime ethers and pharmaceutical compositions containing the same 失效
标题翻译：肟醚和含有它的药物组合物
公开(公告)号：US4395413A
公开(公告)日：1983-07-26
申请号：US162674
申请日：1980-06-24
申请人： Zoltan Budai , Aranka Lay nee Konya , Tibor Mezei , Lujza Petocz , Katalin Grasser , Ibolya Kosoczky , Eniko Szirt nee Kiszelly , Peter Gorog
发明人： Zoltan Budai , Aranka Lay nee Konya , Tibor Mezei , Lujza Petocz , Katalin Grasser , Ibolya Kosoczky , Eniko Szirt nee Kiszelly , Peter Gorog
IPC分类号： A61K31/15 , A61K31/495 , A61P25/04 , C07C67/00 , C07C239/00 , C07C249/10 , C07C251/58 , C07D295/02 , C07D295/088 , C07D295/08
CPC分类号： C07D295/088 , Y10S514/926 , Y10S514/927
摘要： The invention relates to novel oxime ethers of the general formula /I/ and acid addition salts and quaternary ammonium derivatives thereof, ##STR1## wherein A represents a C.sub.2-6 straight or branched alkylene chain,R and R.sup.1 each represent a C.sub.1-6 alkyl group or they form together with the adjacent nitrogen atom a heterocyclic ring containing 4 to 7 carbon atoms and optionally a further hetero atom, i.e. an oxygen, sulfur or nitrogen atom, and said ring may be optionally substituted by a C.sub.1-3 alkyl, phenyl or benzyl group,R.sup.2 and R.sup.3 each denote a hydrogen atom or together form a valency bond,R.sup.4 denotes a C.sub.1-10 alkyl or C.sub.2-10 alkenyl group, andn denotes an integer from 3 to 7.The compounds of the general formula /I/ are prepared according to the invention by reacting a cycloalkane derivative of the general formula /II/ ##STR2## wherein R.sup.2, R.sup.3, R.sup.4 and n have the same meaning as above, whereasY denotes an oxygen or sulphur atom or a .dbd.N--OH group with an aminoalkyl derivative of the general formula /III/ ##STR3## wherein R, R.sup.1 and A have the same meaning as stated above andZ means a halogen atom or a H.sub.2 N--O-- group or a salt thereof in the presence of a basic condensing agent.The new compounds of the general formula /I/ possess valuable nicotine-lethality inhibiting, local anaesthetic, analgesic effects, which are, in case of certain compounds, complemented by anti-hypertensive, maximum electroshock and tetracorspasm inhibiting, ulcus inhibiting and motility inhibiting effects, and can be applied to advantage in the therapy.
摘要翻译：本发明涉及通式I I的新型肟醚及其酸加成盐和季铵衍生物，其中A表示C2-6直链或支链亚烷基链，R和R1各自表示C1 -6烷基，或者它们与相邻的氮原子一起与含有4至7个碳原子的杂环和任选的另外的杂原子（即氧，硫或氮原子）一起形成，并且所述环可以任选地被C 1-3 烷基，苯基或苄基，R2和R3各自表示氢原子或一起形成价键，R4表示C1-10烷基或C2-10烯基，n表示3至7的整数。根据本发明通过使通式/ II / IMAGE / II /的环烷烃衍生物与其中R2，R3，R4和n具有与上述相同的含义反应制备通式/ I / I，而Y表示氧或硫原子或a =具有氨基烷基衍生物的N-OH基团通式/ III / / III /其中R，R 1和A具有与上述相同的含义，Z表示在碱性缩合剂存在下的卤素原子或H 2 N-O-基或其盐。新型化合物/ I /具有有价值的尼古丁杀伤力抑制，局部麻醉，止痛作用，在某些化合物的情况下，补充有抗高血压，最大电休克和四疣抑制作用，抑制溃疡和运动抑制作用，并且可以在治疗中有利地应用。

60. 发明公开

EP4296255A1 METHOD FOR CO-PRODUCING ADIPIC ACID AND CYCLOHEXANONE OXIME FROM CYCLOHEXANE 审中-公开
公开(公告)号：EP4296255A1
公开(公告)日：2023-12-27
申请号：EP21926342.3
申请日：2021-11-15
申请人： Xiangtan University
发明人： LUO, He'an , YOU, Kuiyi , JIAN, Jian , LIU, Pingle , NI, Wenjin , AI, Qiuhong
IPC分类号： C07C51/27 , C07C249/10 , C07C55/14 , C07C251/44
摘要： A method for producing adipic acid and cyclohexanone oxime from cyclohexane is provided. Cyclohexane and NO x undergo oxidation-nitration reaction to produce a mixture of adipic acid, nitrocyclohexane, nitrogen oxides and by-product A, from which adipic acid and nitrocyclohexane are separated. The nitrocyclohexane is catalytically hydrogenated with hydrogen to produce cyclohexanone oxime and a small amount of cyclohexylamine, where cyclohexanone oxime is collected, and the cyclohexylamine is partially oxidized with molecular oxygen to obtain cyclohexanone oxime and by-product B. Without separation, or after removing part or all of water from the reaction mixture, under the action of a catalyst, the reaction mixture undergoes hydrogenation and amination simultaneously or sequentially, or the hydrogenation alone, and separation to give cyclohexanone oxime.

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