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51. 发明授权

US4931466A Crystalline form and its preparation 失效
标题翻译：结晶形式及其制备
公开(公告)号：US4931466A
公开(公告)日：1990-06-05
申请号：US311419
申请日：1989-02-15
申请人： Siegfried Kersten , Karl-Friedrich Jaeger , Karl-Heinz Koenig , Albrecht Mueller , Josef B. Pawliczek , Hans-Gert Recker , Wolfgang Rohr , August Wigger
发明人： Siegfried Kersten , Karl-Friedrich Jaeger , Karl-Heinz Koenig , Albrecht Mueller , Josef B. Pawliczek , Hans-Gert Recker , Wolfgang Rohr , August Wigger
IPC分类号： C07C271/08 , A01N47/22 , C07C67/00 , C07C239/00 , C07C271/40
CPC分类号： A01N47/22
摘要： A compound of the chemical formula (I) ##STR1## in a specific crystalline form, processes for its preparation, and its use for pest control.
摘要翻译：具有特定结晶形式的化学式（I）化合物（I）的化合物，其制备方法及其用于害虫防治的用途。

52. 发明授权

US4670567A Process for the preparation of 5,6-dihydro-2H-thiopyran-3-carboxaldehyde derivatives wherein the reactions are conducted in a high boiling mineral oil without a catalyst 失效
标题翻译：制备5,6-二氢-2H-噻喃-3-甲醛衍生物的方法，其中反应在不含催化剂的高沸点矿物油中进行
公开(公告)号：US4670567A
公开(公告)日：1987-06-02
申请号：US758812
申请日：1985-07-25
申请人： Manfred Sauerwald , Toni Dockner , Wolfgang Rohr , Gernot Reissenweber
发明人： Manfred Sauerwald , Toni Dockner , Wolfgang Rohr , Gernot Reissenweber
IPC分类号： C07D335/02
CPC分类号： C07D335/02
摘要： 5,6-Dihydro-2H-thiopyran-3-carboxaldehydes of the formula ##STR1## where R denotes hydrogen or methyl, are prepared by a method in which acrolein or crotonaldehyde is reacted with hydrogen sulfide in a mineral oil whose boiling point is higher than those of the starting materials and of the end product, and the 5,6-dihydro-2H-thiopyran-3-carboxaldehyde is obtained by distillation. These aldehydes are important intermediates for the preparation of some crop protection agents.
摘要翻译：其中R表示氢或甲基的式“IMAGE”的5,6-二氢-2H-噻喃-3-甲醛通过以下方法制备：其中丙烯醛或巴豆醛与沸点较高的矿物油中的硫化氢反应比原料和最终产物的原料和5,6-二氢-2H-噻喃-3-甲醛通过蒸馏得到。这些醛是制备一些作物保护剂的重要中间体。

53. 发明授权

US4619929A Phenylpiperazine derivatives of hetarylphenols and hetarylanilines, their preparation, and therapeutic agents containing these compounds 失效
标题翻译：苯二甲基苯酚和杂芳基苯胺的苯基哌嗪衍生物，它们的制备和含有这些化合物的治疗剂
公开(公告)号：US4619929A
公开(公告)日：1986-10-28
申请号：US590746
申请日：1984-03-19
申请人： Peter C. Thieme , Gerd Steiner , Wolfgang Rohr , Dieter Lenke , Josef Gries , Harald Weifenbach , Hans-Juergen Teschendorf , Hans P. Hofmann , Horst Kreiskott
发明人： Peter C. Thieme , Gerd Steiner , Wolfgang Rohr , Dieter Lenke , Josef Gries , Harald Weifenbach , Hans-Juergen Teschendorf , Hans P. Hofmann , Horst Kreiskott
IPC分类号： C07D249/08 , A61K31/495 , A61K31/496 , A61P9/02 , A61P11/00 , A61P25/20 , C07D231/12 , C07D233/60 , C07D233/61 , C07D271/10 , C07D295/06 , C07D295/067 , C07D295/096 , C07D521/00 , C07D413/12 , C07D403/12 , C07D417/12
CPC分类号： C07D271/10 , C07D231/12 , C07D233/56 , C07D249/08 , C07D295/067 , C07D295/096
摘要： Novel phenylpiperazinylpropane and -butane derivatives of hetarylphenols and hetarylanilines of the formula ##STR1## where R.sup.1 is hydrogen or alkyl of 1 to 4 carbon atoms, R.sup.2 is hydrogen, halogen, alkyl of 1 to 4 carbon atoms or alkoxy where alkyl is of 1 to 3 carbon atoms, the phenyl ring can be monosubstituted or disubstituted by R.sup.2, X is oxygen or an NH group, and the heterocyclic structure Het. is 1,3,4-oxadiazolyl, triazolyl, imidazolyl or pyrazolyl, and their physiologically tolerated addition salts with acids, processes for their preparation, and pharmaceutical formulations which contain these compounds and exhibit predominantly sedative, neuroleptic and hypotensive properties.
摘要翻译：式（I）的芳基苯酚和杂芳基苯胺的新型苯基哌嗪基丙烷和丁烷衍生物，其中R 1为氢或1至4个碳原子的烷基，R 2为氢，卤素，1至4个碳原子的烷基或烷氧基，其中烷基为1〜 3个碳原子，苯环可以被R2单取代或二取代，X是氧或NH基，杂环结构Het。是1,3,4-恶二唑基，三唑基，咪唑基或吡唑基，以及它们与酸的生理学上可耐受的加成盐，其制备方法和含有这些化合物并且主要表现出镇静，抗精神病药和降血压性质的药物制剂。

54. 发明授权

US4593104A 2-halo-N-(azole-1-yl-methyl)-substituted acetanilides 失效
标题翻译： 2-卤代-N-（唑-1-基 - 甲基） - 取代的乙酰苯胺
公开(公告)号：US4593104A
公开(公告)日：1986-06-03
申请号：US839777
申请日：1977-10-06
申请人： Karl Eicken , Wolfgang Rohr , Bernd Zeeh , Bruno Wurzer
发明人： Karl Eicken , Wolfgang Rohr , Bernd Zeeh , Bruno Wurzer
IPC分类号： A01N43/36 , A01N43/50 , A01N43/56 , A01N43/647 , A01N43/653 , A01N43/713 , A01P13/00 , C07D231/06 , C07D231/12 , C07D231/20 , C07D231/32 , C07D233/56 , C07D233/58 , C07D233/60 , C07D233/61 , C07D233/68 , C07D249/04 , C07D249/06 , C07D249/08 , C07D249/10 , C07D257/04 , C07D521/00
CPC分类号： C07D257/04 , A01N43/36 , A01N43/50 , A01N43/56 , A01N43/647 , A01N43/653 , A01N43/713 , C07D231/12 , C07D233/56 , C07D233/68 , C07D249/04 , C07D249/06 , C07D249/08 , C07D249/10
摘要： New and valuable 2-halo-N-(azole-1-yl-methyl)-substituted acetanilides and having a good herbicidal action, and methods of controlling the growth of unwanted plants with these compounds.
摘要翻译：新的和有价值的2-卤代-N-（唑-1-基 - 甲基） - 取代的乙酰替苯胺并且具有良好的除草作用，以及用这些化合物控制不想要的植物的生长的方法。

55. 发明授权

US4514572A Preparation of fluorophthalic anhydrides 失效
标题翻译：氟代邻苯二甲酸酐的制备
公开(公告)号：US4514572A
公开(公告)日：1985-04-30
申请号：US572949
申请日：1984-01-23
申请人： Gerhard Hamprecht , Juergen Varwig , Wolfgang Rohr
发明人： Gerhard Hamprecht , Juergen Varwig , Wolfgang Rohr
IPC分类号： C07C51/567 , C07D307/89
CPC分类号： C07C51/567 , C07D307/89
摘要： Fluorophthalic anhydrides containing 1 or 2 fluorine atoms are prepared by a process in which a chlorophthalic anhydride containing 1 or 2 chlorine atoms is treated with an acid chloride of sulfurous acid or of carbonic acid in the presence of an aliphatic sulfone, and the reaction mixture is then reacted with potassium fluoride.
摘要翻译：含有1或2个氟原子的氟代邻苯二甲酸酐通过在脂族砜存在下用亚硫酸或碳酸的酰氯处理含有1或2个氯原子的氯代邻苯二甲酸酐的方法制备，反应混合物为然后与氟化钾反应。

56. 发明授权

US06533944B1 Method and device for recovering fine sand from a floating dredger 失效
标题翻译：从浮式挖泥船回收细沙的方法和装置
公开(公告)号：US06533944B1
公开(公告)日：2003-03-18
申请号：US09480592
申请日：2000-01-07
申请人： Wolfgang Rohr
发明人： Wolfgang Rohr
IPC分类号： B01D3304
CPC分类号： B03B9/00 , E02F7/023 , E02F7/065
摘要： The method relates to the recovery of fine sand on floating production equipment in the form of a floating grab-bucket type excavator or floating bucket chain dredger. In this case, the dredged material is dewatered and transported to shore via floating conveyor belts. The dredged material is transferred to dewatering screening machine having a dewatering deck with a dewatering coating. Below the dewatering deck the screening machine has a blind bottom covering the entire surface area, whereby in the direction of conveyance the end zone is provided with a discharge. The discharge is directed at a hydro belt separator, which has a revolving endless conveyor belt with a washing trough as the separation bed, and an ascending part leading away from the washing trough. The running direction of the conveyor belt is in the direction of the ascent, whereby the dredged material is transferred at the discharge of the screening machine to the washing trough of the hydro belt separator.
摘要翻译：该方法涉及以浮式抓斗式挖掘机或浮式铲斗链式挖泥船的形式回收浮式生产设备上的细砂。在这种情况下，疏浚物质通过浮动输送带脱水并输送到岸边。疏浚材料被转移到具有脱水层的脱水筛分机上。在脱水甲板的下方，筛选机具有覆盖整个表面区域的盲底，从而在输送方向上设有排出口。排放指向一个水力带分离器，该分离器具有带有作为分离床的洗涤槽的旋转环形输送带以及远离洗涤槽的上升部分。输送带的运行方向是上升的方向，由此将疏浚物料在筛分机的排放口转移到水力分离器的清洗槽。

57. 发明授权

US5164408A 1,2-dihaloazolylethane derivatives and crop protection agents containing them 失效
标题翻译： 1,2-DIHALOAZOLYLETHANE DORIVATIVES和作物保护剂含有它们
公开(公告)号：US5164408A
公开(公告)日：1992-11-17
申请号：US552037
申请日：1990-07-13
申请人： Rainer Seele , Norbert Goetz , Walter Himmele , Reiner Kober , Wolfgang Rohr , Eberhard Ammermann , Gisela Lorenz , Wilhelm Rademacher , Johann Jung
发明人： Rainer Seele , Norbert Goetz , Walter Himmele , Reiner Kober , Wolfgang Rohr , Eberhard Ammermann , Gisela Lorenz , Wilhelm Rademacher , Johann Jung
IPC分类号： A01N43/50 , A01N43/653 , C07D233/56 , C07D233/60 , C07D233/61 , C07D249/08 , C07D401/06 , C07D407/06 , C07D409/06 , C07D413/06 , C07D521/00
CPC分类号： C07D231/12 , A01N43/50 , A01N43/653 , C07D233/56 , C07D249/08
摘要： 1,2-Dihaloazolylethane derivatives of the general formula I ##STR1## where R.sup.1 and R.sup.2 are each substituted or unsubstituted phenyl, biphenyl, naphthyl or hetaryl, Z is chlorine or bromine, and X is CH or N, and their plant-tolerated acid addition salts and metal complexes, and fungicides and growth regulators containing these compounds.
摘要翻译：其中R 1和R 2各自为取代或未取代的苯基，联苯基，萘基或杂芳基，Z为氯或溴，X为CH或N，并且它们的植物耐受性为酸加成盐和金属配合物，以及含有这些化合物的杀真菌剂和生长调节剂。

58. 发明授权

US5122531A Vinylazoles and the use thereof for crop protection 失效
标题翻译：维生素及其作物保护的用途
公开(公告)号：US5122531A
公开(公告)日：1992-06-16
申请号：US586154
申请日：1990-09-21
申请人： Rainer Seele , Wolfgang Rohr , Bernhard Zipperer , Stefan Karbach , Lothar Rueb , Eberhard Ammermann , Gisela Lorenz , Wilhelm Rademacher , Johann Jung
发明人： Rainer Seele , Wolfgang Rohr , Bernhard Zipperer , Stefan Karbach , Lothar Rueb , Eberhard Ammermann , Gisela Lorenz , Wilhelm Rademacher , Johann Jung
IPC分类号： A01N43/50 , A01N43/653 , C07D233/56 , C07D233/60 , C07D249/08 , C07D401/06 , C07D401/14 , C07D405/06 , C07D405/14 , C07D521/00
CPC分类号： C07D231/12 , A01N43/50 , A01N43/653 , C07D233/56 , C07D249/08
摘要： Vinylazoles of the general formula I ##STR1## where R.sup.1 and R.sup.2 are alkyl, cycloalkyl, tetrahydropyranyl, pyridyl, naphthyl, biphenyl or phenyl, these radicals being substituted or unsubstituted, X is CH or N, and plant-tolerated acid addition salts and metal complexes thereof, and crop protection agents containing these compounds.
摘要翻译：通式I的乙烯基唑其中R 1和R 2是烷基，环烷基，四氢吡喃基，吡啶基，萘基，联苯基或苯基，这些基团是取代或未取代的，X是CH或N，以及植物耐受的酸加成盐和金属络合物和含有这些化合物的作物保护剂。

59. 发明授权

US4973736A Diethers of m- or p-hydroxyphenol 失效
标题翻译：对 - 对羟基苯酚的降解
公开(公告)号：US4973736A
公开(公告)日：1990-11-27
申请号：US395192
申请日：1989-08-15
申请人： Rainer Becker , Werner Hoffmann , Heinz-Guenter Oeser , Wolfgang Rohr , Juergen Varwig
发明人： Rainer Becker , Werner Hoffmann , Heinz-Guenter Oeser , Wolfgang Rohr , Juergen Varwig
IPC分类号： C07C69/66 , B01J23/00 , B01J27/00 , C07B61/00 , C07C41/00 , C07C41/01 , C07C41/16 , C07C41/26 , C07C43/205 , C07C43/225 , C07C43/23 , C07C43/29 , C07C43/295 , C07C51/00 , C07C59/125 , C07C59/64 , C07C67/00 , C07C201/00 , C07C205/38 , C07C253/00 , C07C255/54 , C07D213/64 , C07D241/44 , C07D277/68
CPC分类号： C07D277/68 , C07C205/38 , C07C41/16 , C07C41/26 , C07C43/225 , C07C43/23 , C07C43/29 , C07C59/64 , C07D213/64 , C07D241/44
摘要： Diethers of m- or p-hydroxyphenol, as well as the monoethers, are prepared by reacting m- or p-tert.-butoxyphenol of the formula II ##STR1## with a halogen compound in the presence of a hydroxide, carbonate and/or bicarbonate of an alkali metal or alkaline earth metal and an organic solvent which is inert under the reaction conditions, at from 20.degree. C. to 150.degree. C., and, if desired, reacting the resulting diether with a dilute aqueous inorganic acid at from 30.degree. to 100.degree. C. to give the monoether.The end products which can be prepared by the process according to the invention are useful starting materials for the preparation of dyes, drugs and crop protection agents.
摘要翻译：通过使式II II的m-或p-叔丁氧基苯酚与卤素化合物在氢氧化物，碳酸盐和/或其盐的存在下反应来制备间 - 或对羟基苯酚以及单醚，或碱性金属或碱土金属的碳酸氢盐和在反应条件下为惰性的有机溶剂，在20℃至150℃，如果需要，将所得二醚与稀无机酸水溶液反应从30℃至100℃，得到单醚。可通过本发明方法制备的最终产物是用于制备染料，药物和作物保护剂的有用起始材料。

60. 发明授权

US4562254A Preparation of 5-fluoro-2-phenyl-4H-3,1-benzoxazin-4-ones 失效
标题翻译：制备5-氟-2-苯基-4H-3,1-苯并恶嗪-4-酮
公开(公告)号：US4562254A
公开(公告)日：1985-12-31
申请号：US655726
申请日：1984-09-28
申请人： Jurgen Varwig , Gerhard Hamprecht , Wolfgang Rohr
发明人： Jurgen Varwig , Gerhard Hamprecht , Wolfgang Rohr
IPC分类号： C07D265/22 , C07D265/10
CPC分类号： C07D265/22
摘要： 5-Fluorobenzoxazinones (I) ##STR1## where R is hydrogen, halogen, C.sub.1 -C.sub.3 -alkyl, or trifluoromethyl, trifluoromethoxy, chlorodifluoromethoxy, difluoromethoxy, tetrafluoroethoxy, trifluoromethylmercapto or chlorodifluoromethylmercapto in the m- or p-position, are prepared by reacting the corresponding benzoxazinone (II) ##STR2## in particular one which is 5-chloro-substituted or 5-bromo-substituted, with a fluoride, in particular potassium fluoride, in the presence or absence of a solvent, by a process in which the reaction is carried out in the absence of water or using previously dried starting materials, and in the presence or absence of a decomposition inhibitor, drying preferably being carried out by treatment with an acid halide, e.g. thionyl chloride, and the inhibitor used being a metal iodide, e.g. sodium iodide, or iodine.
摘要翻译：制备5-氟苯并恶嗪酮（I）其中R是氢，卤素，C 1 -C 3 - 烷基或三氟甲基，三氟甲氧基，氯代二氟甲氧基，二氟甲氧基，四氟乙氧基，三氟甲基巯基或氯代二氟甲基巯基在m-或p-位上通过使相应的苯并恶嗪酮（II）（II）特别是5-氯取代或5-溴取代的苯并恶嗪酮（II）与氟化物，特别是氟化钾在溶剂存在或不存在下，通过反应在没有水或使用预先干燥的原料的情况下进行的方法，并且在存在或不存在分解抑制剂的情况下，干燥优选通过用酰卤处理，例如亚硫酰氯，并且使用的抑制剂是金属碘化物，例如。碘化钠或碘。

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