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51. 发明申请

US20050222373A1 Method for producing polyhydroxyalkanoate crystal 失效
标题翻译：聚羟基链烷酸酯晶体的制备方法
公开(公告)号：US20050222373A1
公开(公告)日：2005-10-06
申请号：US10992132
申请日：2004-11-19
申请人： Koichi Kinoshita , Fumio Osakada , Yasuyoshi Ueda , Karunakaran Narasimhan , Angella Cearley , Kenneth Yee , Isao Noda
发明人： Koichi Kinoshita , Fumio Osakada , Yasuyoshi Ueda , Karunakaran Narasimhan , Angella Cearley , Kenneth Yee , Isao Noda
IPC分类号： C08G67/00
CPC分类号： C08G63/90 , C08G63/06
摘要： The present invention provides a method for easily obtaining a biodegradable polyhydroxyalkanoate by a solvent extraction method. A method for producing a polyhydroxyalkanoate crystal which comprises mixing a solution of a polyhydroxyalkanoate in a good solvent with a poor solvent at 50 to 130° C. to precipitate a polyhydroxyalkanoate.
摘要翻译：本发明提供了一种通过溶剂萃取方法容易地获得可生物降解的聚羟基链烷酸酯的方法。一种制备聚羟基链烷酸酯晶体的方法，其包括在50-130℃下将聚羟基链烷酸酯在良溶剂中的溶液与不良溶剂混合以沉淀聚羟基链烷酸酯。

52. 发明授权

US06821612B1 Methods for preparing soft and elastic biodegradable polyhydroxyalkanoate copolymer compositions and polymer products comprising such compositions 失效
标题翻译：制备柔软和弹性可生物降解的聚羟基链烷酸酯共聚物组合物的方法和包含这种组合物的聚合物产品
公开(公告)号：US06821612B1
公开(公告)日：2004-11-23
申请号：US10111498
申请日：2002-04-25
申请人： David Harry Melik , Isao Noda
发明人： David Harry Melik , Isao Noda
IPC分类号： B32B702
CPC分类号： C08G63/06 , C08J5/18 , C08J2367/04 , Y10T428/249921 , Y10T428/29 , Y10T428/2913
摘要： Soft and elastic polymer products are obtained by stretching a composition comprising a biodegradable polyhydroxyalkanoate copolymer comprising at least two randomly repeating monomer units. The first randomly repeating monomer unit has structure (I), wherein R1 is H, or C1 or C2 alkyl, and n is 1 or 2. The second randomly repeating monomer unit is different from the first randomly repeating monomer unit and has structure (II), wherein m is 2 to about 9. At least about 70 mole % of the copolymer comprises randomly repeating monomer units having the structure of the first randomly repeating monomer unit (I). The products exhibit advantageous combinations of softness and elasticity while maintaining strength.
摘要翻译：通过拉伸包含至少两个随机重复的单体单元的可生物降解的聚羟基链烷酸酯共聚物的组合物获得软和弹性聚合物产物。第一个随机重复的单体单元具有结构（I），其中R 1是H或C 1或C 2烷基，n是1或2.第二个无规重复的单体单元不同于第一个无规重复的单体单元，并具有结构（II），其中m为2至约9.共聚物的至少约70摩尔％包含具有第一无规重复单体单元（I）结构的无规重复的单体单元。该产品在保持强度的同时表现出柔软和弹性的有利组合。

53. 发明授权

US6143947A Fibers, nonwoven fabrics and absorbent articles comprising a biodegradable polyhydroxyalkanoate comprising 3-hydroxybutyrate and 3-hydroxyhexanoate 失效
标题翻译：包含可生物降解的聚羟基链烷酸酯的纤维，非织造织物和吸收制品，其包含3-羟基丁酸酯和3-羟基己酸酯
公开(公告)号：US6143947A
公开(公告)日：2000-11-07
申请号：US385791
申请日：1999-08-30
申请人： Isao Noda
发明人： Isao Noda
IPC分类号： A61F13/15 , C08J5/18 , D04H1/42 , D04H1/00
CPC分类号： C08J5/18 , A61F13/15252 , D04H1/42 , C08J2367/04 , Y10T428/2913 , Y10T428/2915
摘要： The present invention relates to fibers, and nonwovens comprising said fibers, comprising a biodegradable copolymer, wherein the copolymer comprises at least two randomly repeating monomer units (RRMU) wherein the first RRMU monomer unit has the structure ##STR1## and the second RRMU has the structure ##STR2## wherein at least 50% of the RRMUs have the structure of the first RRMU. The present invention further relates to an absorbent article comprising a liquid pervious topsheet, a biodegradable liquid impervious backsheet comprising the above fibers and/or nonwovens, and an absorbent core positioned between the topsheet and the backsheet.
摘要翻译：本发明涉及纤维和包含所述纤维的无纺布，其包含可生物降解的共聚物，其中所述共聚物包含至少两个随机重复的单体单元（RRMU），其中所述第一RRMU单体单元具有所述结构，并且所述第二RRMU具有以下结构：至少有50％的RRMU具有第一个RRMU的结构。本发明还涉及一种吸收制品，其包括透液性顶片，包含上述纤维和/或非织造布的可生物降解的不透液体的底片以及位于顶片和底片之间的吸收芯。

54. 发明授权

US6077931A Biodegradable PHA copolymers 有权
标题翻译：可生物降解的PHA共聚物
公开(公告)号：US6077931A
公开(公告)日：2000-06-20
申请号：US217734
申请日：1998-12-21
申请人： Isao Noda
发明人： Isao Noda
IPC分类号： C08G63/08 , C08L101/16 , C08G63/06 , C08G63/12
CPC分类号： C08G63/08
摘要： The present invention relates to biodegradable PHA copolymers comprising at least two randomly repeating monomer units. The present invention further relates to a plastic article comprising a biodegradable copolymer, wherein the biodegradable copolymer comprises at least two randomly repeating monomer units (RRMU) wherein the first RRMU has the structure ##STR1## wherein R.sup.1 is H, or C.sub.1 or C.sub.2 alkyl, and n is 1 or 2; the second RRMU has the structure ##STR2## and wherein at least 50% of the RRMUs have the structure of the first RRMU. The present invention further relates to an absorbent article comprising a liquid pervious topsheet, a liquid impervious backsheet comprising a film comprising a PHA of the present invention and an absorbent core positioned between the topsheet and the backsheet.
摘要翻译：本发明涉及包含至少两个随机重复的单体单元的可生物降解的PHA共聚物。本发明还涉及包含可生物降解的共聚物的塑料制品，其中所述可生物降解共聚物包含至少两个随机重复的单体单元（RRMU），其中第一RRMU具有其中R 1为H或C 1或C 2烷基的结构，n为 1或2; 第二RRMU具有结构，并且其中至少50％的RRMU具有第一RRMU的结构。本发明还涉及一种吸收性物品，其包括透液性顶片，不透液体的底片，其包含由本发明的PHA构成的膜和位于顶片与底片之间的吸收芯。

55. 发明授权

US5942597A Solvent extraction of polyhydroxyalkanoates from biomass 失效
标题翻译：从生物质中提取聚羟基链烷酸酯
公开(公告)号：US5942597A
公开(公告)日：1999-08-24
申请号：US672692
申请日：1996-06-28
申请人： Isao Noda , Lee Arnold Schechtman
发明人： Isao Noda , Lee Arnold Schechtman
IPC分类号： C08G63/06 , C08G63/89 , C11B1/10 , C12P7/62 , C08K5/00
CPC分类号： C12P7/625 , C08G63/06 , C08G63/89
摘要： The present invention relates to a process for separating polyhydroxyalkanoate from a biomass, the process comprising extracting the polyhydroxyalkanoate with at least one PHA solvent selected from the group consisting of acetone, acetonitrile, benzene, butyl acetate, butyl propionate, .beta.-butyrolactone, .gamma.-butyrolactone, diethyl carbonate, diethylformamide, dimethyl carbonate, dimethyl succinate, dimethyl sulfoxide, dimethylformamide, ethyl acetate, ethylene glycol diacetate, methyl acetate, methyl ethyl ketone, 1,4-dioxane, tetrahydrofuran, toluene, xylene, and mixtures thereof.
摘要翻译：本发明涉及从生物质中分离聚羟基链烷酸酯的方法，该方法包括用至少一种PHA溶剂萃取聚羟基链烷酸酯，所述PHA溶剂选自丙酮，乙腈，苯，乙酸丁酯，丙酸丁酯，β-丁内酯，γ-丁内酯，丁内酯，二乙基甲酰胺，碳酸二甲酯，琥珀酸二甲酯，二甲基亚砜，二甲基甲酰胺，乙酸乙酯，乙二醇二乙酸酯，乙酸甲酯，甲基乙基酮，1,4-二恶烷，四氢呋喃，甲苯，二甲苯及其混合物。

56. 发明授权

US5918747A Process for recovering polyhydroxyalkanoates using centrifugal fractionation 失效
$Process for recovering polyhydroxyalkanoates using centrifugal fractionation$
标题翻译：使用离心分级回收聚羟基链烷酸酯的方法
公开(公告)号：US5918747A
公开(公告)日：1999-07-06
申请号：US910869
申请日：1997-07-13
申请人： Isao Noda
发明人： Isao Noda
IPC分类号： C08G63/06 , C08G63/78 , C08G63/89 , C08G63/90 , C12P7/62 , C12R1/05 , C12R1/19 , B03B5/30 , B03B5/32 , B03B5/34
CPC分类号： C08G63/89 , C12P7/625 , C08G63/06
摘要： The present invention relates to a process for recovering polyhydroxyalkanoate from a biological source material containing the polyhydroxyalkanoate, the process comprising: a) comminuting the biological source material; b) suspending the comminuted biological source material in a fluid; c) partitioning the polyhydroxyalkanoate from the other components of the biological source material by centrifugal fractionation to form a solid-solid separation; and d) recovering the polyhdroxyalkanoate.
摘要翻译：本发明涉及从含有聚羟基链烷酸酯的生物源材料中回收聚羟基链烷酸酯的方法，该方法包括：a）粉碎生物源材料; b）将粉碎的生物源材料悬浮在流体中; c）通过离心分级将聚羟基链烷酸酯与生物源材料的其它成分分离，以形成固 - 固分离; 和d）回收聚羟基链烷酸酯。

57. 发明授权

US5489470A Biodegradable copolymers and plastic articles comprising biodegradable copolymers 失效
标题翻译：包括可生物降解的共聚物的可生物降解的共聚物和塑料制品
公开(公告)号：US5489470A
公开(公告)日：1996-02-06
申请号：US422009
申请日：1995-04-13
申请人： Isao Noda
发明人： Isao Noda
IPC分类号： A61F20060101 , A61L15/26 , A61L15/62 , C08F20060101 , C08G20060101 , C08G63/06 , C08G63/08 , C08J5/18 , C08L67/04 , C09J20060101 , C09J167/04 , B32B27/00 , A61F13/15
CPC分类号： A61L15/26 , A61L15/62 , C08G63/06 , C08G63/08 , C08J5/18 , C08L67/04 , C09J167/04 , C08J2367/04 , Y10S428/913 , Y10S521/916 , Y10T442/671 , Y10T442/696
摘要： The present invention relates to biodegradable PHA copolymers comprising at least two randomly repeating monomer units. The present invention further relates to a plastic article comprising a biodegradable copolymer, wherein the biodegradable copolymer comprises at least two randomly repeating monomer units (RRMU) wherein the first RRMU has the structure ##STR1## wherein R.sup.1 is H, or C.sub.1 or C.sub.2 alkyl, and n is 1 or 2; the second RRMU has the structure ##STR2## wherein R.sup.2 is a C.sub.4 -C.sub.19 alkyl or alkenyl; and wherein at least 50% of the RRMUs have the structure of the first RRMU. The present invention further relates to an absorbent article comprising a liquid pervious topsheet, a liquid impervious backsheet comprising a film comprising a PHA of the present invention and an absorbent core positioned between the topsheet and the backsheet.
摘要翻译：本发明涉及包含至少两个随机重复的单体单元的可生物降解的PHA共聚物。本发明还涉及一种包含可生物降解的共聚物的塑料制品，其中该可生物降解的共聚物包含至少两个随机重复的单体单元（RRMU），其中第一RRMU具有其中R 1为H或C 1或C 2烷基的结构， n为1或2; 第二RRMU具有结构，其中R2是C4-C19烷基或烯基; 并且其中至少50％的RRMU具有第一RRMU的结构。本发明还涉及一种吸收性物品，其包括透液性顶片，不透液体的底片，其包含由本发明的PHA构成的膜和位于顶片与底片之间的吸收芯。

58. 发明授权

US5412027A Preparation of homogeneous polymers using supercritical fluid solutions 失效
标题翻译：使用超临界流体溶液制备均相聚合物
公开(公告)号：US5412027A
公开(公告)日：1995-05-02
申请号：US155041
申请日：1993-11-19
申请人： Annetta D. Shine , Steven D. Smith , Isao Noda
发明人： Annetta D. Shine , Steven D. Smith , Isao Noda
IPC分类号： C08J3/00 , C08J3/14 , C08L101/00 , C08G63/48 , C08L51/08
CPC分类号： C08J3/005 , C08J3/14 , Y02P20/544
摘要： Homogeneous polymer blends are prepared from otherwise thermodynamically immiscible polymers, especially including block copolymers. Thus, polymers such as polystyrene/poly(methyl methacrylate) block copolymer or polystyrene/poly(1,2-butadiene) block copolymer are dissolved under pressure in supercritical fluid solvents such as chlorodifluoromethane and n-butane, respectively, and expanded through a fine nozzle. As the SCF solvent evaporates, the polymer deposits as a substantially homogeneous material.
摘要翻译：均匀聚合物共混物由另外的热力学不混溶聚合物制备，特别是包括嵌段共聚物。因此，聚合物如聚苯乙烯/聚（甲基丙烯酸甲酯）嵌段共聚物或聚苯乙烯/聚（1,2-丁二烯）嵌段共聚物在压力下分别溶解在超临界流体溶剂如氯二氟甲烷和正丁烷中，并通过精细喷嘴。当SCF溶剂蒸发时，聚合物沉积为基本均匀的材料。

59. 发明授权

US5342875A Polycationic latex wet strength agent 失效
标题翻译：聚阳离子胶乳湿强力剂
公开(公告)号：US5342875A
公开(公告)日：1994-08-30
申请号：US45278
申请日：1993-04-07
申请人： Isao Noda
发明人： Isao Noda
IPC分类号： C08F299/02 , D21H17/56 , D21H21/20 , C08J3/02
CPC分类号： D21H21/20 , C08F299/024 , D21H17/56
摘要： Polycationic wet-strength materials such as KYMENE are chemically modified to provide unsaturated hydrocarbon substituents. The modified KYMENE is cross-linked onto and into latex particles to provide improved wet-strength agents for use in paper treatments. Thus, KYMENE is reacted, for example, with acrylic acid and cross-linked with styrene/butadiene to provide a polycationic latex wet-strength agent.
摘要翻译：聚阳离子湿强度材料如KYMENE被化学改性以提供不饱和烃取代基。改性的KYMENE交联到胶乳颗粒上并提供用于纸张处理的改进的湿强剂。因此，KYMENE例如与丙烯酸反应并与苯乙烯/丁二烯交联以提供聚阳离子胶乳湿强度剂。

60. 发明授权

US5200036A Paper with polycationic latex strength agent 失效
标题翻译：纸用聚阳离子胶乳强度剂
公开(公告)号：US5200036A
公开(公告)日：1993-04-06
申请号：US802022
申请日：1991-12-03
申请人： Isao Noda
发明人： Isao Noda
IPC分类号： D21C9/00 , D21H17/55
CPC分类号： D21H17/55 , D21C9/005
摘要： Polycationic wet strength agents such as KYMENE are chemically modified and cross-linked into and onto the surface of latex particles. Paper treated with the resulting polycationic latex particles exhibits enhanced wet strength. Thus, KYMENE is reacted, for example, with acrylic acid and cross-linked with styrene/butadiene to provide a polycationic latex which is used to treat paper. Paper sheets, bags, containers and the like are provided. Also provided are paper towels, and the like, having super-absorbent materials incorporated therein.
摘要翻译：聚阳离子湿强剂如KYMENE被化学改性并交联到胶乳颗粒的表面上和表面上。用所得聚阳离子胶乳颗粒处理的纸表现出增强的湿强度。因此，KYMENE例如与丙烯酸反应并与苯乙烯/丁二烯交联以提供用于处理纸的聚阳离子胶乳。提供纸张，袋子，容器等。还提供了在其中结合有超吸收材料的纸巾等。

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