会员体验
专利管家(专利管理)
工作空间(专利管理)
风险监控(情报监控)
数据分析(专利分析)
侵权分析(诉讼无效)
联系我们
交流群
官方交流:
QQ群: 891211   
微信请扫码    >>>
现在联系顾问~
热词
    • 59. 发明申请
    • PROCESS FOR PRODUCING DISPERSION OF PARTICLES OF RUTILE TITANIUM OXIDE
    • 生产分散的氧化钛颗粒的方法
    • US20130143729A1
    • 2013-06-06
    • US13816545
    • 2011-08-15
    • Takanori MoritaKenichi NakagawaAtsushi Nomura
    • Takanori MoritaKenichi NakagawaAtsushi Nomura
    • B01J31/38G02B1/04
    • B01J31/38C01G23/047C01G23/0536C01P2002/52C01P2002/54C01P2002/72C01P2004/51C01P2004/62C01P2006/12C08L101/00C09C1/3607C09D17/008G02B1/04
    • The invention provides a process for producing an aqueous dispersion of particles of rutile titanium oxide, which comprises: a first step in which after a chloride ion concentration of an aqueous solution of titanium tetrachloride is adjusted to 0.5 mole/L or more and less than 4.4 mole/L, the aqueous solution of titanium tetrachloride is heated at a temperature in a range of from 25° C. to 75° C. to hydrolyze the titanium tetrachloride, thereby obtaining a slurry containing the thus precipitated particles of rutile titanium oxide; a second step in which the slurry obtained in the first step is filtered and washed with water to remove water-soluble salts dissolved therein from the slurry; a third step in which the slurry obtained in the second step is subjected to a hydrothermal reaction in the presence of an organic acid; a fourth step in which the slurry obtained in the third step is filtered and washed with water to remove water-soluble salts dissolved therein from the slurry; a fifth step in which an acid is added to the slurry obtained in the fourth step to deflocculate the slurry, and the resulting slurry is subjected to wet dispersion treatment, thereby obtaining a dispersion; and a sixth step in which excess acid and water-soluble salts are removed from the dispersion obtained in the fifth step.
    • 本发明提供一种制备金红石型氧化钛颗粒的水性分散体的方法,其包括:第一步骤,其中将四氯化钛水溶液的氯离子浓度调节至0.5摩尔/升以上且小于4.4倍 摩尔/ L,将四氯化钛水溶液在25℃至75℃的温度范围内加热以水解四氯化钛,从而获得含有如此沉淀的金红石型氧化钛颗粒的浆料; 将第一步骤中获得的浆液过滤并用水洗涤以从浆料中除去溶解在其中的水溶性盐的第二步骤; 在第二步骤中获得的浆料在有机酸存在下进行水热反应的第三步骤; 将第三步骤中获得的浆液过滤并用水洗涤以从浆料中除去溶解在其中的水溶性盐的第四步骤; 在第四工序中得到的浆料中加入酸以使浆料脱絮凝的第五步骤,将得到的浆料进行湿分散处理,得到分散体; 以及从第五步骤中获得的分散体中除去过量的酸和水溶性盐的第六步骤。