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51. 发明专利

CA2202577C PROCESS FOR PRODUCING PIPERIDINECARBINOLS 未知
公开(公告)号：CA2202577C
公开(公告)日：2006-05-30
申请号：CA2202577
申请日：1997-04-14
申请人： ASAHI GLASS CO LTD
发明人： WANG SHU-ZHONG , OKAZOE TAKASHI , MATSUMURA YASUSHI , OOKURA KAZUHIRO , MORI NOBUAKI , NISHINO JIRO
IPC分类号： C07D211/78 , C07B61/00 , C07C255/41 , C07D211/20 , C07D211/22 , C07D211/26
摘要： A process for producing a trans isomer of a piperidinecarbinol represented by the general formula (2), which comprises reducing a trans isomer of a compound represented by the general formula (1): (see formulas 1 and 2) wherein R1 is a hydrogen atom, a lower alkyl group or an aralkyl group, R2 is a hydrogen atom, a lower alkyl group, an aryl group or an aralkyl group, and X is a hydrogen atom, a halogen atom, an alkyl group, an aryl group, an aralkyl group, an alkoxy group, a dialkylamino group, an alkylthio group, an arylthio group or C m F2m+1- wherein m is an integer of from 1 to 20.

52. 发明专利

AT278657T 未知
公开(公告)号：AT278657T
公开(公告)日：2004-10-15
申请号：AT00956818
申请日：2000-08-30
申请人： ASAHI GLASS CO LTD
发明人： OKAZOE TAKASHI , WATANABE KUNIO , ITO MASAHIRO , SHIRAKAWA DAISUKE , TATEMATSU SHIN
IPC分类号： C07C43/16 , C07C43/17 , C07C43/178 , C07C51/09 , C07C51/58 , C07C51/60 , C07C53/50 , C07C59/135 , C07C59/315 , C07C62/08 , C07C67/08 , C07C67/14 , C07C67/287 , C07C67/307 , C07C69/003 , C07C69/63 , C07C69/708 , C08G73/24
摘要： The process for producing a vic-dichloro acid fluoride compound in a short process and in good yield from the starting material which is inexpensive and readily available is provided. (R -EH1-)CR R CH2-OCOR (I) is fluorinated in a liquid phase to form (CF2ClCFCl-EF -) CR R CF2-OCOR (II), and then, an ester bond of the compound (II) is decomposed to form (CF2ClCFCl-E -)CR R COF(III) or the compound (III) and FCOR (IV).

53. 发明专利

HK1052495A1 Method for producing fluorine-containing compound 未知
公开(公告)号：HK1052495A1
公开(公告)日：2003-09-19
申请号：HK03104749
申请日：2003-07-03
申请人： ASAHI GLASS CO LTD
发明人： OKAZOE TAKASHI , WATANABE KUNIO , STATEMATSU SHIN , ITO MASAHIRO , SHIRAKAWA DAISUKE , IWAYA MASAO , OKAMOTO HIDEKAZU
IPC分类号： C07C20060101 , C07C51/58 , C07C55/40 , C07C59/135 , C07C67/307 , C07C69/63 , C07C69/708
摘要： The present invention provides a method for obtaining a compound useful as a raw material for various fluororesins in high yield by a short process by using a starting material which is inexpensive and readily available. Namely, the present invention is characterized by reacting the following compound (1) with the following compound (2) to produce the following compound (3) having a fluorine content of at least 30 mass%, fluorinating the compound (3) in a liquid phase to produce the following compound (4), followed by a cleavage reaction of E of the compound (4) to obtain a compound (5) and/or a compound (6): E -R -E E -R R -E-R -E-R R -E -R -E -R E -R -E R -E wherein R is a fluorine-containing bivalent organic group which is the same as R , or a bivalent organic group which will be converted to R by a fluorination reaction, and R is a monovalent organic group which is the same as R , or a monovalent organic group which will be converted to R by a fluorination reaction, R is a fluorine-containing bivalent organic group which is the same as or different from R , and when different, it is a group having R fluorinated, R is a fluorine-containing monovalent organic group which is the same as or different from R , and when different, it is a group having R fluorinated, E and E are reactive groups which will react to each other to form a bivalent connecting group (E), E is a bivalent connecting group formed by the reaction of E and E , E is a group which is the same as E, or a group having E fluorinated, provided that at least one selected from R , R and E , is a group formed by a fluorination reaction, and each of E and E which are independent from each other, is a group formed by cleavage of E .

54. 发明专利

ES2190026T3 未知
公开(公告)号：ES2190026T3
公开(公告)日：2003-07-16
申请号：ES98118582
申请日：1998-10-01
申请人： ASAHI GLASS CO LTD
发明人： SUGIYAMA NORIHIDE , MUROFUSHI HIDENOBU , OKAZOE TAKASHI , TAMURA MASAYUKI , TATEMATSU SHIN , IRISAWA JUN
IPC分类号： G02B1/04

55. 发明专利

CA2423910A1 PROCESS FOR PRODUCING FLUORINATED ESTER COMPOUND 未知
公开(公告)号：CA2423910A1
公开(公告)日：2003-03-26
申请号：CA2423910
申请日：2001-09-27
申请人： ASAHI GLASS CO LTD
发明人： YANASE KOICHI , TATEMATSU SHIN , SUZUKI YASUHIRO , OKAZOE TAKASHI , WATANABE KUNIO , SHIRAKAWA DAISUKE
IPC分类号： C07C41/06 , C07C43/178 , C07C51/60 , C07C67/14 , C07C67/287 , C07C67/297 , C07C59/135 , C07C53/46 , C07C51/58 , C07C69/63 , C07C69/708
摘要： A process for producing an industrially useful fluorinated ester compound an d a fluorine compound such as an acid fluoride compound. The process for producing a fluorinated ester compound comprises fluorinating in a liquid phase a compound which is an ester of a hydroxyl compound with a compound having an acyl fluoride group and which has a structure capable of being fluorinated, and is characterized in that the ester compound being fluorinat ed is in the form of a liquid mixture with the compound having an acyl fluoride group.

56. 发明专利

AT230496T 未知
公开(公告)号：AT230496T
公开(公告)日：2003-01-15
申请号：AT98118582
申请日：1998-10-01
申请人： ASAHI GLASS CO LTD
发明人： SUGIYAMA NORIHIDE , MUROFUSHI HIDENOBU , OKAZOE TAKASHI , TAMURA MASAYUKI , TATEMATSU SHIN , IRISAWA JUN
IPC分类号： G02B1/04

57. 发明专利

DE69705896T2 未知
公开(公告)号：DE69705896T2
公开(公告)日：2002-04-11
申请号：DE69705896
申请日：1997-05-30
申请人： ASAHI GLASS CO LTD
发明人： WANG SHU-ZHONG , OKAZOE TAKASHI , MATSUMURA YASUSHI
IPC分类号： C07D405/12

58. 发明专利

AU9226801A Process for producing fluorinated ester compound 未知
公开(公告)号：AU9226801A
公开(公告)日：2002-04-08
申请号：AU9226801
申请日：2001-09-27
申请人： ASAHI GLASS CO LTD
发明人： OKAZOE TAKASHI , WATANABE KUNIO , TATEMATSU SHIN , YANASE KOICHI , SUZUKI YASUHIRO , SHIRAKAWA DAISUKE
IPC分类号： C07C41/06 , C07C43/178 , C07C51/60 , C07C67/14 , C07C67/287 , C07C67/297 , C07C69/63 , C07C69/708 , C07C51/58 , C07C53/46 , C07C59/135
摘要： The present invention provides a method for producing industrially useful fluorine-containing compounds such as a fluorinated ester compound and an acid fluoride compound. Namely, the present invention resides in a method for producing a fluorinated ester compound, which comprises fluorinating an ester compound which is an ester of a compound having hydroxyl group(s) with a compound having acyl fluoride group(s) and which has a structure which can be fluorinated, in a liquid phase to produce a fluorinated ester compound, wherein the fluorination is carried out in the form of a liquid mixture of the ester compound and the compound having acyl fluoride group(s).

59. 发明专利

AU9027201A Process for producing acyl fluoride and carboxylic acid salt 未知
公开(公告)号：AU9027201A
公开(公告)日：2002-04-08
申请号：AU9027201
申请日：2001-09-26
申请人： ASAHI GLASS CO LTD
发明人： WATANABE KUNIO , OKAZOE TAKASHI , ITO MASAHIRO , TATEMATSU SHIN , KAMIYA HIROKI , MUROTANI EISUKE
IPC分类号： C07C51/58 , C07C51/04 , C07C51/41 , C07C51/60 , C07C59/135 , C07C67/14 , C07C67/287 , C07C69/708 , C09K23/00 , C09K23/44 , C07C59/58 , C07C59/315 , B01F17/44
摘要： A process for efficiently producing an acyl fluoride and a carboxylic acid salt while inhibiting side reactions. R ÄOCH(CH3)CH2ÜnOH (1) and XCOR (R and R each is a group which upon fluorination becomes a perfluoroalkyl group, X is a halogen atom, and n is an integer of from 1 to 10) (2) are reacted to form an ester compound (3); the compound (3) is fluorinated in a liquid phase; and the ester bond of the fluorinated compound (4) is cleaved to obtain a perfluoroacyl fluoride (5). Further, this perfluoroacyl fluoride (5) is hydrolyzed and then reacted with ammonia or an alkali metal hydroxide to obtain a carboxylic acid salt (7).

60. 发明专利

AU9026001A Process for producing fluoroamine compound 未知
公开(公告)号：AU9026001A
公开(公告)日：2002-04-08
申请号：AU9026001
申请日：2001-09-21
申请人： ASAHI GLASS CO LTD
发明人： ITO MASAHIRO , WATANABE KUNIO , SHIRAKAWA DAISUKE , OKAZOE TAKASHI , TATEMATSU SHIN
IPC分类号： C07C213/08 , C07C219/08 , C07C229/20

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