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51. 发明授权

US5553714A Method for detecting and separating thermoplastic containers with near infrared fluorosphores 失效
标题翻译：用近红外荧光团检测和分离热塑性容器的方法
公开(公告)号：US5553714A
公开(公告)日：1996-09-10
申请号：US339318
申请日：1994-11-14
申请人： Michael R. Cushman , James J. Krutak , William W. Parham , Clarence A. Coates , Max A. Weaver , Gabor Patonay
发明人： Michael R. Cushman , James J. Krutak , William W. Parham , Clarence A. Coates , Max A. Weaver , Gabor Patonay
IPC分类号： C07D487/22 , B07C5/342 , C07D209/60 , C07F5/06 , C07F7/02 , C07F7/08 , C08K5/00 , C08K5/34 , C08K5/3412 , C08K5/3415 , C08L67/00 , C08L101/00 , C09B47/06 , C09B47/067 , C09B47/073 , C09B47/08 , C09B47/18 , C09B57/00 , C09B67/20 , C09K11/06 , B07C5/10
CPC分类号： C09B47/063 , B07C5/342 , B07C5/365 , C07D209/60 , C07F5/069 , C07F7/025 , C07F7/0858 , C08K5/0008 , C08K5/0041 , C08K5/34 , C09B47/0675 , C09B47/0676 , C09B47/073 , C09B47/08 , C09B47/18 , C09B57/007 , C09B67/0061 , B29B2017/0279 , Y02W30/622
摘要： Provided is a method for tagging thermoplastic containers using near infrared fluorescing compounds or copolymerized residues readily capable of detection. Also provided is a method for identifying a thermoplastic container. Also provided are thermoplastic polymer compositions comprised of the near infrared fluorescing compounds or residues and articles comprised of such compositions.
摘要翻译：提供了使用近红外荧光化合物或易于检测的共聚残基来标记热塑性容器的方法。还提供了一种用于识别热塑性容器的方法。还提供了由近红外荧光化合物或由这些组合物组成的残余物和制品组成的热塑性聚合物组合物。

52. 发明授权

US5461136A Method for tagging thermoplastic materials with near infrared fluorophores 失效
标题翻译：用近红外荧光团标记热塑性材料的方法
公开(公告)号：US5461136A
公开(公告)日：1995-10-24
申请号：US265904
申请日：1994-06-27
申请人： James J. Krutak , Michael R. Cushman , Clarence A. Coates , William W. Parham , Max A. Weaver , Gabor Patonay
发明人： James J. Krutak , Michael R. Cushman , Clarence A. Coates , William W. Parham , Max A. Weaver , Gabor Patonay
IPC分类号： C07D487/22 , B07C5/342 , C07D209/60 , C07F5/06 , C07F7/02 , C07F7/08 , C08K5/00 , C08K5/34 , C08K5/3412 , C08K5/3415 , C08L67/00 , C08L101/00 , C09B47/06 , C09B47/067 , C09B47/073 , C09B47/08 , C09B47/18 , C09B57/00 , C09B67/20 , C09K11/06 , C08G73/00
CPC分类号： C09B47/063 , B07C5/342 , B07C5/365 , C07D209/60 , C07F5/069 , C07F7/025 , C07F7/0858 , C08K5/0008 , C08K5/0041 , C08K5/34 , C09B47/0675 , C09B47/0676 , C09B47/073 , C09B47/08 , C09B47/18 , C09B57/007 , C09B67/0061 , B29B2017/0279 , Y02W30/622
摘要： Provided is a method for tagging thermoplastic containers using near infrared fluorescing compounds or copolymerized residues readily capable of detection. Also provided is a method for identifying a thermoplastic container. Also provided are thermoplastic polymer compositions comprised of the near infrared fluorescing compounds or residues and articles comprised of such compositions. Also provided are new compounds useful as near infrared fluorophoric markers in the practice of this invention. The methods, compositions, and compounds of the present invention thus provide a total system useful for marking, for identification purposes, the various classes of thermoplastic wastes, so that they can be identified, sorted, and subsequently recycled.
摘要翻译：提供了使用近红外荧光化合物或易于检测的共聚残基来标记热塑性容器的方法。还提供了一种用于识别热塑性容器的方法。还提供了由近红外荧光化合物或由这些组合物组成的残余物和制品组成的热塑性聚合物组合物。还提供了在本发明的实践中用作近红外荧光标记的新化合物。因此，本发明的方法，组合物和化合物提供了用于标识目的的各种类型的热塑性废物的总体系统，以便可以鉴定，分类和随后再循环。

53. 发明授权

US5397819A Thermoplastic materials containing near infrared fluorophores 失效
标题翻译：含有近红外荧光团的热塑性材料
公开(公告)号：US5397819A
公开(公告)日：1995-03-14
申请号：US156746
申请日：1993-11-24
申请人： James J. Krutak , Michael R. Cushman , Clarence A. Coates , William W. Parham , Max A. Weaver , Gabor Patonay
发明人： James J. Krutak , Michael R. Cushman , Clarence A. Coates , William W. Parham , Max A. Weaver , Gabor Patonay
IPC分类号： C07D487/22 , B07C5/342 , C07D209/60 , C07F5/06 , C07F7/02 , C07F7/08 , C08K5/00 , C08K5/34 , C08K5/3412 , C08K5/3415 , C08L67/00 , C08L101/00 , C09B47/06 , C09B47/067 , C09B47/073 , C09B47/08 , C09B47/18 , C09B57/00 , C09B67/20 , C09K11/06
CPC分类号： C09B47/063 , B07C5/342 , B07C5/365 , C07D209/60 , C07F5/069 , C07F7/025 , C07F7/0858 , C08K5/0008 , C08K5/0041 , C08K5/34 , C09B47/0675 , C09B47/0676 , C09B47/073 , C09B47/08 , C09B47/18 , C09B57/007 , C09B67/0061 , B29B2017/0279 , Y02W30/622
摘要： Provided is a method for tagging thermoplastic containers using near infrared fluorescing compounds or copolymerized residues readily capable of detection. Also provided is a method for identifying a thermoplastic container. Also provided are thermoplastic polymer compositions comprised of the near infrared fluorescing compounds or residues and articles comprised of such compositions. Also provided are new compounds useful as near infrared fluorophoric markers in the practice of this invention. The methods, compositions, and compounds of the present invention thus provide a total system useful for marking, for identification purposes, the various classes of thermoplastic wastes, so that they can be identified, sorted, and subsequently recycled.
摘要翻译：提供了使用近红外荧光化合物或易于检测的共聚残基来标记热塑性容器的方法。还提供了一种用于识别热塑性容器的方法。还提供了由近红外荧光化合物或由这些组合物组成的残余物和制品组成的热塑性聚合物组合物。还提供了在本发明的实践中用作近红外荧光标记的新化合物。因此，本发明的方法，组合物和化合物提供了用于识别目的的各种类型的热塑性废物的总体系统，以便可以鉴定，分类和随后再循环。

54. 发明授权

US5106942A Copolymerized methine colorant-polyester color concentrates 失效
标题翻译：共聚甲基染料 - 聚酯颜料浓度
公开(公告)号：US5106942A
公开(公告)日：1992-04-21
申请号：US461961
申请日：1990-01-08
申请人： James J. Krutak , William W. Parham , Max A. Weaver , Clarence A. Coates, Jr. , Terry A. Oldfield
发明人： James J. Krutak , William W. Parham , Max A. Weaver , Clarence A. Coates, Jr. , Terry A. Oldfield
IPC分类号： C07D209/08 , C07D215/12 , C07D265/36 , C08G63/685 , C09B67/44 , C09B69/10
CPC分类号： C08G63/6858 , C09B69/105
摘要： Disclose are polyester color concentrates, especially amorphous and partially-crystalline, polyester color concentrates, comprising a polyester having copolymerized therein colored residues of at least one polyester-reactive, thermally-stable methine colorant compound. The color concentrates may be used to impart yellow shades and colors to various polymeric materials, shaped articles fabricated of and coatings formulated from such polymeric materials and, especially, personal, medical and home care products where non-extractability of the colorant material is essential. Also disclosed are colored semicrystalline powders derived from the color concentrates.
摘要翻译：折叠是聚酯颜色浓缩物，特别是无定形和部分结晶的聚酯彩色浓缩物，其包含在其中共聚有至少一种聚酯反应性热稳定的次甲基着色剂化合物的着色残余物的聚酯。颜色浓缩物可以用于赋予各种聚合物材料，由这些聚合材料制成的成型制品和由此类聚合材料配制的涂层，特别是着色剂材料的不可萃取性是必需的个人，医疗和家庭护理产品的黄色色调和颜色。还公开了衍生自颜色浓缩物的着色半结晶粉末。

55. 发明授权

US5032670A Copolymerized anthraquinone-polyester color concentrates 失效
标题翻译：共聚蒽醌 - 聚酯颜色浓缩液
公开(公告)号：US5032670A
公开(公告)日：1991-07-16
申请号：US400423
申请日：1989-08-30
申请人： William W. Parham , James J. Krutak , Max A. Weaver , Clarence A. Coates, Jr. , Terry A. Oldfield
发明人： William W. Parham , James J. Krutak , Max A. Weaver , Clarence A. Coates, Jr. , Terry A. Oldfield
IPC分类号： C08G63/685 , C08G73/00 , C08J3/02 , C08J3/20 , C08J3/22 , C09B1/16 , C09B1/28 , C09B69/10
CPC分类号： A61K8/355 , A61K8/85 , C08G63/6856 , C08J3/226 , C09B1/285 , C09B69/101 , A61K2800/43 , A61K2800/57 , C08J2467/00
摘要： Disclosed are color concentrate compositions which comprise a polyester having copolymerized therein at least 0.5 weight percent of an anthraquinone colorant compound having the formula ##STR1## wherein AQ is a 1,5- or 1,8-anthraquinonylene radical; R.sup.1 and R.sup.2 are the same or different and are unsubstituted or substituted alkyl, cycloalkyl or aryl; and X is a group reactive with at least one of the functional groups of the monomers from which the polyester is prepared. Amorphous polyesters and partially-crystalline polyesters are preferred embodiments of the color concentrates. Also disclosed are colored semicrystalline powders which may be obtained from the amorphous and partially-crystalline color concentrates by a dissolution-crystallization-precipitation procedure.

56. 发明授权

US5703229A Method for tagging thermoplastic materials with near infrared fluorophores 失效
标题翻译：用近红外荧光团标记热塑性材料的方法
公开(公告)号：US5703229A
公开(公告)日：1997-12-30
申请号：US609011
申请日：1996-02-29
申请人： James J. Krutak , Michael R. Cushman , Clarence A. Coates , William W. Parham , Max A. Weaver , Gabor Patonay
发明人： James J. Krutak , Michael R. Cushman , Clarence A. Coates , William W. Parham , Max A. Weaver , Gabor Patonay
IPC分类号： C07D487/22 , B07C5/342 , C07D209/60 , C07F5/06 , C07F7/02 , C07F7/08 , C08K5/00 , C08K5/34 , C08K5/3412 , C08K5/3415 , C08L67/00 , C08L101/00 , C09B47/06 , C09B47/067 , C09B47/073 , C09B47/08 , C09B47/18 , C09B57/00 , C09B67/20 , C09K11/06 , C07B47/24
CPC分类号： C09B47/063 , B07C5/342 , B07C5/365 , C07D209/60 , C07F5/069 , C07F7/025 , C07F7/0858 , C08K5/0008 , C08K5/0041 , C08K5/34 , C09B47/0675 , C09B47/0676 , C09B47/073 , C09B47/08 , C09B47/18 , C09B57/007 , C09B67/0061 , B29B2017/0279 , Y02W30/622
摘要： Provided are new compounds useful as near infrared fluorophoric markers. In the practice of this invention a method is also provided for tagging thermoplastic containers using near infrared fluorescing compounds or copolymerized residues readily capable of detection. The new compounds are phthalocyanine and naphthalocyanine derivatives which are covalently bonded to substituted silicon and aluminum compounds. The methods, compositions, and compounds described herein thus provide a total system useful for marking, for identification purposes, the various classes of thermoplastic wastes, so that they can be identified, sorted, and subsequently recycled.
摘要翻译：提供用作近红外荧光标记的新化合物。在本发明的实践中，还提供了使用近红外荧光化合物或易于检测的共聚残基来标记热塑性容器的方法。新化合物是与取代的硅和铝化合物共价键合的酞菁和萘酞菁衍生物。因此，本文所述的方法，组合物和化合物提供了用于标识目的的各种类型的热塑性废物的总体系统，以便可以鉴定，分类和随后再循环。

57. 发明授权

US5453482A Process for preparing arylsulfonyl halides 失效
标题翻译：制备芳基磺酰卤的方法
公开(公告)号：US5453482A
公开(公告)日：1995-09-26
申请号：US210785
申请日：1994-03-18
申请人： Max A. Weaver , William W. Parham , James J. Krutak , Kim S. Chamberlin
发明人： Max A. Weaver , William W. Parham , James J. Krutak , Kim S. Chamberlin
IPC分类号： C07C303/08 , C07C309/88 , C07C319/20 , C07C323/66 , C07D221/18 , C07F5/06 , C08G8/02 , C08G75/00
CPC分类号： C07F5/069 , C07C303/08 , C07C319/20 , C07D221/18 , C07C2103/24
摘要： Provided is a new process useful for preparing arylsulfonyl halides, which comprises the addition or drowning of halosulfonation reaction products, produced by the reaction of aromatic compounds (arenes), with excess halosulfonic acid, into C.sub.3 -C.sub.6 aliphatic ketones, preferably acetone, isopropyl alcohol, or mixtures thereof, instead of drowning into water as is known in the art of aromatic sulfonyl chloride preparation. Less heat of reaction is observed, thus making the drowning of the halosulfonation reaction mixture safer and more controllable. Further, less hydrogen chloride gas is evolved from the drowning mixture and generally more highly pure arylsulfonyl chlorides are produced.
摘要翻译：提供了一种用于制备芳基磺酰卤的新方法，其包括将芳族化合物（芳烃）与过量的卤代磺酸反应生成的卤代磺化反应产物加入或淹没在C 3 -C 6脂族酮中，优选丙酮，异丙醇，或其混合物，而不是如本领域已知的芳族磺酰氯制剂淹没在水中。观察到较少的反应热，从而使得卤化磺化反应混合物的淹没更加安全并且更可控。此外，从淹没混合物中放出较少的氯化氢气体，通常产生更高纯度的芳基磺酰氯。

58. 发明授权

US5423432A Water-dissipatable polyesters and amides containing near infrared fluorescent compounds copolymerized therein 失效
标题翻译：含有其中共聚的近红外荧光化合物的可水分散的聚酯和酰胺
公开(公告)号：US5423432A
公开(公告)日：1995-06-13
申请号：US238300
申请日：1994-05-05
申请人： James J. Krutak , Michael R. Cushman , William W. Parham , Clarence A. Coates , Max A. Weaver , Gabor Patonay
发明人： James J. Krutak , Michael R. Cushman , William W. Parham , Clarence A. Coates , Max A. Weaver , Gabor Patonay
IPC分类号： C08G63/68 , C08G69/04 , G06K7/12 , G06K19/06 , B07C5/00 , C08G73/06
CPC分类号： G06K7/12 , C08G63/68 , C08G69/04 , G06K19/06009 , Y10T428/31786 , Y10T428/3179
摘要： Provided are water-dissipatable, sulfo-containing polyesters and polyester-amides having copolymerized therein thermally stable near infrared flourophoric compounds. The polymers are useful in coating or ink compositions, which are in turn useful for marking articles for identification/authentication purposes. Also provided is a method for invisibly marking such articles and a method for detecting and sorting articles by utilizing the near infrared flourophoric ink or coating compositions.
摘要翻译：提供了在其中共聚有热稳定性近红外光滑化合物的可水分散的含磺基聚酯和聚酯酰胺。聚合物可用于涂料或油墨组合物，这些组合物又用于标记物品以用于鉴定/认证目的。还提供了一种用于不可见地标记这种物品的方法，以及通过利用近红外荧光墨水或涂料组合物来检测和分选物品的方法。

59. 发明授权

US4698651A Magenta dye-donor element used in thermal dye transfer 失效
标题翻译：用于热染料转移的品红染料供体元件
公开(公告)号：US4698651A
公开(公告)日：1987-10-06
申请号：US923444
申请日：1986-10-27
申请人： William H. Moore , Max A. Weaver , Kin K. Lum
发明人： William H. Moore , Max A. Weaver , Kin K. Lum
IPC分类号： C09B29/033 , B41M5/26 , B41M5/385 , B41M5/388 , B41M5/39
CPC分类号： B41M5/388 , Y10S428/913 , Y10S428/914 , Y10S430/146 , Y10T428/24901 , Y10T428/31504 , Y10T428/31786
摘要： A magenta dye-donor element for thermal dye transfer comprises a support having thereon a magenta dye dispersed in a polymeric binder, the magenta dye comprising a substituted 5-arylazoisothiazole.In a preferred embodiment, the magenta dye has the formula ##STR1## wherein R.sup.1 and R.sup.2 may each independently be hydrogen, alkyl, allyl, cycloalkyl or aryl; or R.sup.1 and R.sup.2 may be taken together to form a ring; or R.sup.1 or R.sup.2 may be part of a 5- or 6-membered heterocyclic ring;R.sup.3 may be hydrogen, alkyl, aryl, alkylthio or halogen;J may be alkyl, aryl or NHA, where A is an acyl or sulfonyl radical; andQ may be cyano, thiocyanato, alkylthio or alkoxycarbonyl.
摘要翻译：用于热染料转移的品红染料供体元件包括其上分散有聚合物粘合剂中的品红色染料的载体，品红色染料包含取代的5-芳基异噻唑。在优选的实施方案中，品红色染料具有下式：其中R 1和R 2可各自独立地为氢，烷基，烯丙基，环烷基或芳基; 或者R1和R2可以一起形成环; 或R 1或R 2可以是5-或6-元杂环的一部分; R3可以是氢，烷基，芳基，烷硫基或卤素; J可以是烷基，芳基或NHA，其中A是酰基或磺酰基; 并且Q可以是氰基，硫氰酸酯基，烷硫基或烷氧基羰基。

60. 发明授权

US4568738A Thiophen-2-ylazopyrazole compounds as colorants for textile fibers 失效
标题翻译：噻吩-2-基吡唑化合物作为纺织纤维的着色剂
公开(公告)号：US4568738A
公开(公告)日：1986-02-04
申请号：US590809
申请日：1984-03-19
申请人： Max A. Weaver , Clarence A. Coates, Jr.
发明人： Max A. Weaver , Clarence A. Coates, Jr.
IPC分类号： C09B29/00 , C09B29/46 , C09B29/033 , C09B29/36 , D06P3/26 , D06P3/36
CPC分类号： C09B29/3652 , C09B29/0059
摘要： Thiophen-2-ylazopyrazole dyes useful for dyeing polyesters, cellulose acetate esters, and polyamides in fast yellow shades have the general formula: ##STR1## wherein: X is alkyl, allyloxy, alkoxy, aryl, aryloxy, amino, alkylamino, arylamino, cyclohexyloxy,, thienyl, cycloalkylamino, N,N-dialkylamino, or N-alkyl-N-arylamino; Y is hydrogen, alkyl, or aryl; Z is alkyl, aryl, alkylsulfonyl, 2-benzothiazolyl, cyano or COX; R and R.sub.1 are alkyl or aryl; R.sub.2 is hydrogen, alkyl, aryl, acyl, benzothiazolyl, pyridyl, sulfolanyl, quinolyl, thiocarbamyl, carbamyl, alkoxycarbonyl, aroyl, aryl-carbamyl and alkanoyl; and wherein the hydrocarbon moieties of the above radicals may be substituted with up to three of --OH, alkoxy, hydroxyalkoxy, carbamyl, and similar groups conventionally used in the azo dye art.
摘要翻译：用于染色聚酯，乙酸纤维素酯和聚酰胺的噻吩-2-基吡唑类染料具有以下通式：其中：X为烷基，烯丙氧基，烷氧基，芳基，芳氧基，氨基，烷基氨基，芳基氨基，环己氧基，噻吩基，环烷基氨基，N，N-二烷基氨基或N-烷基-N-芳基氨基; Y是氢，烷基或芳基; Z是烷基，芳基，烷基磺酰基，2-苯并噻唑基，氰基或COX; R和R 1是烷基或芳基; R2是氢，烷基，芳基，酰基，苯并噻唑基，吡啶基，环丁砜基，喹啉基，硫代氨基甲酰基，氨基甲酰基，烷氧基羰基，芳酰基，芳基 - 氨基甲酰基和烷酰基。并且其中上述基团的烃部分可被至多三个-OH，烷氧基，羟基烷氧基，氨基甲酰基以及常规用于偶氮染料领域的类似基团取代。

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