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51. 发明授权

US06852871B2 Method for producing optically active salicylaldimine copper complex 失效
标题翻译：光学活性水杨醛亚胺铜络合物的制备方法
公开(公告)号：US06852871B2
公开(公告)日：2005-02-08
申请号：US10457514
申请日：2003-06-10
申请人： Makoto Itagaki , Koji Hagiya
发明人： Makoto Itagaki , Koji Hagiya
IPC分类号： C07B53/00 , C07C67/347 , C07C249/02 , C07C251/24 , C07F1/08
CPC分类号： C07C249/02 , C07B2200/07 , C07C67/347 , C07C2601/02 , C07C69/747 , C07C251/24
摘要： There is provided a method for producing an optically active salicylaldimine copper complex, which method is characterized in that an optically active amino alcohol compound represented by the following formula (1) is reacted with copper hydroxide (II) in an organic solvent: wherein R1 and R2 which are the same or different, each represent lower alkyl groups and the like which may be substituted, X1 and X2 which are the same or different, each represent a hydrogen atom, lower alkyl groups and the like, and the symbol * designates an asymmetric carbon atom.
摘要翻译：提供一种光学活性水杨醛亚胺铜络合物的制造方法，其特征在于，将下述式（1）表示的光学活性氨基醇化合物与氢氧化铜（II）在有机溶剂中反应：其中， 1＆gt;和R 2相同或不同，各自表示可以被取代的低级烷基等，X 1和X 2相同或不同，各自表示氢原子，低级烷基等，符号*表示不对称碳原子。

52. 发明授权

US06670500B2 Chiral copper complex and production processes thereof and using the same 有权
标题翻译：手性铜络合物及其制备方法及其使用
公开(公告)号：US06670500B2
公开(公告)日：2003-12-30
申请号：US09766575
申请日：2001-01-23
申请人： Masashi Kamitamari , Gohfu Suzukamo , Michio Yamamoto , Koji Hagiya , Makoto Itagaki
发明人： Masashi Kamitamari , Gohfu Suzukamo , Michio Yamamoto , Koji Hagiya , Makoto Itagaki
IPC分类号： C07C25124
CPC分类号： C07C251/24 , C07B2200/07 , C07C67/347 , C07C2601/02 , C07C69/747 , C07C69/74
摘要： There is disclosed an optically active salicylideneaminoalcohol compound of formula (1): wherein R1 represents an alkyl group or the like, R2 represents an aryl group and the like, and when X1 represents a nitro, X2 is a hydrogen atom, when X1 represents a chlorine atom, X2 is a chlorine atom, and when X1 is a hydrogen atom, X2 is a fluorine atom; and the carbon atom denoted by “*” is an asymmetric carbon atom having either an S or R configuration, and a chiral copper complex produced from the optically active salicylidenaminoalcohol compound and a copper compound.
摘要翻译：公开了式（1）的光学活性亚水杨基氨基醇化合物：其中R1表示烷基等，R2表示芳基等，当X1表示硝基时，X2表示氢原子，当X1表示氯原子时 X2是氯原子，当X1是氢原子时，X2是氟原子; 由“*”表示的碳原子是具有S或R构型的不对称碳原子和由光学活性水杨酰氨基醇化合物和铜化合物制备的手性铜络合物。

53. 发明授权

US5739401A N-(.alpha.-alkylbenzylidene)-.alpha.-phenylalkylamine, its use and process for producing the same and process for producing intermediate therefor 失效
标题翻译： N-（α-烷基亚苄基）-α-苯基烷基胺，其用途及其制备方法及其制备方法
公开(公告)号：US5739401A
公开(公告)日：1998-04-14
申请号：US624105
申请日：1996-03-29
申请人： Koji Hagiya , Etsuko Harada , Hideyuki Goto
发明人： Koji Hagiya , Etsuko Harada , Hideyuki Goto
IPC分类号： C07C251/24 , C07C251/06
CPC分类号： C07C251/24
摘要： There is disclosed an N-(.alpha.-alkylbenzylidene)-.alpha.-phenylalkylamine represented by the general formula (1): ##STR1## wherein R.sup.1 represents a lower alkyl group, R.sup.2 represents a hydrogen atom, a halogen atom, a lower alkyl group or a lower alkoxy group and X represents a halogen atom or a lower alkoxy group, its use and a process for producing the same and processes for producing intermediates therefor.
摘要翻译：公开了由通式（1）表示的N-（α-烷基亚苄基）-α-苯基烷基胺：其中R1表示低级烷基，R2表示氢原子，卤原子，低级烷基或低级烷氧基，X表示卤素原子或低级烷氧基，其用途及其制备方法以及其制备中间体的方法。

54. 发明授权

US4954651A Process for preparing trans-2,2-dimethyl-3-(2,2-dihalovinyl)-cyclopropane carboxylic acid halide 失效
标题翻译：制备反式-2,2-二甲基-3-（2,2-二卤代乙烯基） - 环丙烷羧酸卤化物的方法
公开(公告)号：US4954651A
公开(公告)日：1990-09-04
申请号：US345726
申请日：1989-05-01
申请人： Gohfu Suzukamo , Yoji Sakito , Masami Fukao , Koji Hagiya
发明人： Gohfu Suzukamo , Yoji Sakito , Masami Fukao , Koji Hagiya
IPC分类号： C07C51/487
CPC分类号： C07C51/487
摘要： Trans-2,2-dimethyl-3-(2,2-dihalovinyl)-cyclopropane carboxylic acid halides which are an intermediate for insecticides are prepared by allowing arylphosphines to react with cis- or cis-/trans-mixed 2,2-dimethyl-3-(2,2-dihalovinyl)-cyclopropane carboxylic acid halides of the formula ##STR1## wherein both X and Y are halogen atoms, respectively, at a temperature of -10.degree. to 100.degree. C., in the presence of absence of halogen compounds.

55. 发明申请

US20140235867A1 METHOD FOR PRODUCING ALPHA-HYDROXY KETONE COMPOUND 审中-公开
标题翻译：生产α-羟基酮酮化合物的方法
公开(公告)号：US20140235867A1
公开(公告)日：2014-08-21
申请号：US14236268
申请日：2012-08-27
申请人： Koji Hagiya , Akio Tanaka , Toshihiro Hodai
发明人： Koji Hagiya , Akio Tanaka , Toshihiro Hodai
IPC分类号： C07C45/64 , C07D277/22 , C07D277/60 , C07D277/72 , C07D277/62 , C07C319/14 , C07D277/36
CPC分类号： C07C45/64 , C07C45/75 , C07C319/14 , C07D277/22 , C07D277/36 , C07D277/60 , C07D277/62 , C07D277/72 , Y02P20/582 , C07C47/19
摘要： The present invention relates to a specific thiazolium salt used for producing an α-hydroxy ketone compound, and a method for producing an α-hydroxy ketone compound by carrying out a coupling reaction of an aldehyde compound in the presence of a base compound and the specific thiazolium salt.
摘要翻译：本发明涉及用于制备α-羟基酮化合物的特定的噻唑鎓盐，以及通过在碱性化合物的存在下进行醛化合物的偶联反应和特定的噻唑鎓盐。

56. 发明授权

US08178325B2 Process for producing sulfur-containing hydroxycarboxylic acid 失效
标题翻译：生产含硫羟基羧酸的方法
公开(公告)号：US08178325B2
公开(公告)日：2012-05-15
申请号：US12440621
申请日：2007-09-21
申请人： Hiroyuki Asako , Koji Hagiya
发明人： Hiroyuki Asako , Koji Hagiya
IPC分类号： C12P11/00
CPC分类号： C12P11/00
摘要： There is provided is a process for producing a sulfur-containing α-hydroxycarboxylic acid compound represented by the formula (2): wherein R1 represents hydrogen, C1-8 alkyl, or C6-20 aryl, which comprises subjecting a sulfur-containing ketol represented by the formula (1): wherein R1 is the same as defined above, to the action of microbial cells of a microorganism belonging to the genus Pseudomonas, Rhodococcus or Bacillus capable of converting the ketol into a corresponding α-hydroxycarboxylic acid compound, or a treated material thereof, thereby producing the sulfur-containing α-hydroxycarboxylic acid without using a hydroxynitrile compound as a starting material.
摘要翻译：提供了一种制备由式（2）表示的含硫α-羟基羧酸化合物的方法：其中R1表示氢，C1-8烷基或C6-20芳基，其包括使含硫的酮醇代表通过式（1）表示的化合物：其中R 1与上述定义相同，能够将酮转化成相应的α-羟基羧酸化合物的属于假单胞菌属，红球菌属或芽孢杆菌属的微生物的微生物细胞的作用，或不会使用羟基腈化合物作为起始原料，生成含硫的α-羟基羧酸。

57. 发明申请

US20110313197A1 METHOD FOR PRODUCING HALOGEN-SUBSTITUTED BENZENE DIMETHANOL 审中-公开
标题翻译：生产取代苯甲酸二甲醇的方法
公开(公告)号：US20110313197A1
公开(公告)日：2011-12-22
申请号：US13203508
申请日：2010-03-04
申请人： Koji Hagiya , Yasutaka Aoyagi
发明人： Koji Hagiya , Yasutaka Aoyagi
IPC分类号： C07C33/26 , C07C233/76
CPC分类号： C07C269/00 , C07C29/147 , C07C231/08 , C07C269/04 , C07C33/46 , C07C271/66 , C07C233/65
摘要： A method for producing a halogen-substituted benzene dimethanol, the method including:a first step of reacting a compound represented by formula (1) with a compound represented by formula (2) to obtain a dicarboxamide compound represented by formula (3), anda second step of reducing the dicarboxamide compound using a borohydride compound to obtain a halogen-substituted benzene dimethanol represented by formula (4).
摘要翻译：一种制备卤素取代的苯二甲醇的方法，该方法包括：使由式（1）表示的化合物与式（2）表示的化合物反应得到由式（3）表示的二羧酰胺化合物的第一步骤，以及使用硼氢化合物还原二羧酰胺化合物以获得由式（4）表示的卤素取代的苯二甲醇的第二步骤。

58. 发明申请

US20110207936A1 METHOD FOR PRODUCING OXADIAZOLINONE COMPOUND AND INTERMEDIATE THEREOF 失效
标题翻译：生产氧化氮杂环丁酮化合物的方法及其中间体
公开(公告)号：US20110207936A1
公开(公告)日：2011-08-25
申请号：US13124416
申请日：2009-10-19
申请人： Koji Hagiya , Yasutaka Aoyagi
发明人： Koji Hagiya , Yasutaka Aoyagi
IPC分类号： C07D271/113 , C07C271/58 , C07C269/04
CPC分类号： C07C281/02 , C07D271/10
摘要： A compound represented by the formula (1): wherein Ar represents an aromatic hydrocarbon group having 6 to 20 carbon atoms which may have a substituent, Ar′ represents an aromatic hydrocarbon group having 6 to 20 carbon atoms which may have a substituent, and R represents an alkyl group having 1 to 4 carbon atoms.
摘要翻译：由式（1）表示的化合物：其中Ar表示可以具有取代基的碳原子数6〜20的芳香族烃基，Ar'表示可以具有取代基的碳原子数6〜20的芳香族烃基，R 表示碳原子数1〜4的烷基。

59. 发明授权

US07754454B2 Process for producing sulfur-containing hydroxycarboxylic acid 失效
标题翻译：生产含硫羟基羧酸的方法
公开(公告)号：US07754454B2
公开(公告)日：2010-07-13
申请号：US11575446
申请日：2005-09-02
申请人： Hiroyuki Asako , Koji Hagiya
发明人： Hiroyuki Asako , Koji Hagiya
IPC分类号： C12P11/00
CPC分类号： C12P11/00
摘要： A process for producing a sulfur-containing α-hydroxycarboxylic acid compound, which comprises a step for reacting a sulfur-containing dihydroxy compound with a cell or a material from treated cell of a microorganism that has an ability to convert the sulfur-containing dihydroxy compound to a corresponding α-hydroxycarboxylic acid compound.
摘要翻译：一种含硫α-羟基羧酸化合物的制造方法，其包括使含硫二羟基化合物与具有转化含硫二羟基化合物的能力的微生物的处理细胞的细胞或物质反应的工序与相应的α-羟基羧酸化合物反应。

60. 发明申请

US20100174122A1 PROCESS FOR PRODUCTION OF HALOGEN-SUBSTITUTED BENZENEDIMETHANOL 失效
标题翻译：生产取代苯甲醛的方法
公开(公告)号：US20100174122A1
公开(公告)日：2010-07-08
申请号：US12303585
申请日：2007-06-21
申请人： Koji Hagiya
发明人： Koji Hagiya
IPC分类号： C07C29/147
CPC分类号： C07C29/147 , C07C33/46
摘要： A process for the production of a halogen-substituted benzenedimethanol represented by the formula (2): wherein X2, X2, X3 and X4 are the same or different and independently represent a hydrogen atom or a halogen atom, provided that at least one of X1, X2, X3 and X4 represents a halogen atom, comprising reacting a halogen-substituted terephthalic acid diester represented by the formula (1): wherein X1, X2, X3 and X4 are the same meanings as defined above and R1 and R2 are the same or different and independently represent an unsubstituted or substituted alkyl group, a metal borohydride compound and an acid in the presence of an ether solvent, wherein the amount of the acid is 0.2 to 3 moles per 1 mole of the metal borohydride compound based on protons, and the reaction is conducted under the condition where the liquid phase of the reaction mixture is a single layer.
摘要翻译：一种制备由式（2）表示的卤素取代的苯二甲醇的方法：其中X 2，X 2，X 3和X 4可以相同或不同，并且独立地表示氢原子或卤原子，条件是X1中的至少一个 X 1，X 3和X 4表示卤素原子，包括使由式（1）表示的卤素取代的对苯二甲酸二酯：其中X 1，X 2，X 3和X 4与上述相同，R 1和R 2相同或不同且独立地表示未取代或取代的烷基，金属硼氢化合物和酸，在醚溶剂存在下，其中每1摩尔基于质子的金属硼氢化合物的酸的量为0.2至3摩尔，反应在反应混合物的液相为单层的条件下进行。

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