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51. 发明授权

US07696296B2 Compositions and articles prepared from the thioether functional oligomeric polythiols 有权
标题翻译：由硫醚官能低聚多硫醇制备的组合物和制品
公开(公告)号：US07696296B2
公开(公告)日：2010-04-13
申请号：US11744240
申请日：2007-05-04
申请人： Nina V. Bojkova , Thomas G. Rukavina , Gregory J. McCollum
发明人： Nina V. Bojkova , Thomas G. Rukavina , Gregory J. McCollum
IPC分类号： C08G18/00
CPC分类号： C08G18/3876 , C08G18/3234 , C08G18/324 , C08G18/722 , C08G18/755 , C08G18/758 , C08G18/765 , C08G75/045 , C08L81/02 , C09D175/04 , G02B1/041 , Y10T428/31551 , C08L2666/14 , C08L75/04 , C08L81/00
摘要： Provided is a composition including a reaction product of: (A) a reactive compound that includes a material having functional groups that are reactive with active hydrogens; (B) a thioether-functional, oligomeric polythiol prepared by reacting together: (1) a compound having at least two thiol functional groups; (2) a compound having triple bond functionality; and optionally (3) a compound having at least two double bonds; and, optionally, (C) a compound different from (B) containing active hydrogens. Coating compositions, articles of manufacture and related processes also are provided.
摘要翻译：本发明提供了包含以下反应产物的组合物：（A）包含具有与活性氢反应的官能团的材料的反应性化合物; （B）通过一起反应制备的硫醚官能的低聚多硫醇：（1）具有至少两个硫醇官能团的化合物; （2）具有三键官能团的化合物; 和（3）具有至少两个双键的化合物; 和（C）不同于含有活性氢的（B）化合物的化合物。还提供了涂料组合物，制品和相关方法。

52. 发明授权

US07125931B2 Thermosetting compositions containing alternating copolymers of isobutylene type monomers 失效
公开(公告)号：US07125931B2
公开(公告)日：2006-10-24
申请号：US10887733
申请日：2004-07-09
申请人： Simion Coca , Edward R. Coleridge , Gregory J. McCollum , James B. O'Dwyer , James E. Poole , Victoria A. Trettel
发明人： Simion Coca , Edward R. Coleridge , Gregory J. McCollum , James B. O'Dwyer , James E. Poole , Victoria A. Trettel
IPC分类号： C08F8/00
CPC分类号： B05D7/57 , B05D1/007 , B05D3/0209 , B05D3/067 , B05D7/53 , C08F8/00 , C08F210/10 , C08F220/10 , C08F290/046 , C08G18/6229 , C08G18/792 , C08G18/798 , C08G18/8025 , C08G18/807 , C08G18/8074 , C08G2150/20 , C08L33/068 , C09D123/22 , C09D133/062 , C09D133/08 , Y10T428/31504 , Y10T428/31511 , C08F220/00 , C08F220/12 , C08F210/00 , C08L2666/28 , C08L2666/02 , C08F214/18 , C08F2500/03 , C08F2500/02 , C08F212/00 , C08F222/00 , C08F2500/26 , C08L2666/04
摘要： A thermosetting composition that includes an ungelled copolymer composition and a crosslinking agent. The ungelled copolymer composition includes a functional group-containing copolymer that includes segments of alternating residues derived from a donor monomer composition comprising an acceptor monomer composition. The donor monomer composition includes one or both of isobutylene and diisobutylene, and the acceptor monomer composition includes acrylic monomers and monomers containing functional groups. The ungelled copolymer composition is substantially free of transition metals and Lewis acids, and the copolymer is substantially free of maleate-type monomer residues and fumarate-type monomer residues. The crosslinking agent has at least two functional groups that are reactive with the functional groups of the copolymer. The thermosetting composition may be in liquid, powder, or dispersed form and may be applied by traditional or electrocoating methods.

53. 发明授权

US07070683B2 Electrodepositable coating compositions and processes related thereto 失效
标题翻译：电沉积涂料组合物及其相关方法
公开(公告)号：US07070683B2
公开(公告)日：2006-07-04
申请号：US10365982
申请日：2003-02-13
申请人： Robin M. Peffer , Brian G. Thebaud , Steven R. Zawacky , Gregory J. McCollum , Al J. Kaylo
发明人： Robin M. Peffer , Brian G. Thebaud , Steven R. Zawacky , Gregory J. McCollum , Al J. Kaylo
IPC分类号： C25D13/12
CPC分类号： C09D5/4492 , C08K3/014 , C09D7/48
摘要： The present invention is directed to a curable electrodepositable coating composition having a resinous phase dispersed in an aqueous medium. The resinous phase includes (a) one or more ungelled, active hydrogen-containing cationic salt group-containing resins which are electrodepositable on a cathode; (b) one or more at least partially blocked polyisocyanate curing agents; (c) at least one substantially non-volatile antioxidant; and (d) at least one volatile antioxidant. The present invention also provides a process for electrodeposition using the coating and substrates coated therewith.
摘要翻译：本发明涉及一种具有分散在水性介质中的树脂相的可固化的可电沉积涂料组合物。树脂相包括（a）一种或多种无电极活性含氢阳离子盐基的树脂，其可电沉积在阴极上; （b）一种或多种至少部分封闭的多异氰酸酯固化剂; （c）至少一种基本上不挥发的抗氧化剂; 和（d）至少一种挥发性抗氧化剂。本发明还提供一种使用涂层和涂覆的基材进行电沉积的方法。

54. 发明授权

US07000313B2 Process for fabricating circuit assemblies using electrodepositable dielectric coating compositions 失效
标题翻译：使用电沉积介电涂层组合物制造电路组件的方法
公开(公告)号：US07000313B2
公开(公告)日：2006-02-21
申请号：US10184192
申请日：2002-06-27
申请人： Gregory J. McCollum , Thomas C. Moriarity , Kevin C. Olson , Michael G. Sandala , Alan E. Wang , Steven R. Zawacky
发明人： Gregory J. McCollum , Thomas C. Moriarity , Kevin C. Olson , Michael G. Sandala , Alan E. Wang , Steven R. Zawacky
IPC分类号： H01K3/10
CPC分类号： H05K3/44 , H01L2924/0002 , H05K1/056 , H05K3/0032 , H05K3/0035 , H05K3/445 , H05K2201/09554 , H05K2203/0582 , H05K2203/135 , Y10T29/49155 , Y10T29/49156 , Y10T29/49165 , H01L2924/00
摘要： Provided is a process for forming metallized vias in a substrate including the steps of (I) applying to an electroconductive substrate an electrodepositable coating composition onto all exposed surfaces of the substrate to form a conformal dielectric coating; (II) ablating a surface of the dielectric coating to expose a section of the substrate; (III) applying a layer of metal to all surfaces to form metallized vias in the substrate. Also disclosed are processes for fabricating a circuit assembly which include the application of an electrodoepositable coating composition onto exposed surfaces of the substrate/core to form a conformal dielectric coating thereon. The electrodepositable coating composition includes a resinous phase dispersed in an aqueous phase, where the resinous phase has a covalently bonded halogen content of at least 1 percent by weight. The dielectric coating derived therefrom has a low dielectric constant and low dielectric loss factor.
摘要翻译：提供了一种用于在基底中形成金属化通孔的方法，包括以下步骤：（I）将可电沉积涂料组合物施加到导电基底上，以在基底的所有暴露表面上形成共形绝缘涂层; （II）烧蚀所述电介质涂层的表面以暴露所述衬底的一部分; （III）将金属层施加到所有表面以在基底中形成金属化通孔。还公开了用于制造电路组件的方法，其包括将电沉积涂料组合物施加到基材/芯的暴露表面上以在其上形成共形绝缘涂层。电沉积涂料组合物包括分散在水相中的树脂相，其中树脂相具有至少1重量％的共价键合的卤素含量。由此得到的电介质涂层具有低介电常数和低介电损耗因子。

55. 发明授权

US06992137B2 Alternating copolymers of isobutylene type monomers 失效
公开(公告)号：US06992137B2
公开(公告)日：2006-01-31
申请号：US10697413
申请日：2003-10-30
申请人： Simion Coca , Edward R. Coleridge , Gregory J. McCollum , James B. O'Dwyer , James E. Poole , Victoria A. Trettel
发明人： Simion Coca , Edward R. Coleridge , Gregory J. McCollum , James B. O'Dwyer , James E. Poole , Victoria A. Trettel
IPC分类号： C08F8/00
CPC分类号： C09D201/02 , C08F8/00 , C08F10/00 , C08F20/00
摘要： A copolymer composition that includes a copolymer comprised of at least 30 mol % of residues having the following alternating residues from a donor monomer and from an acceptor monomer. The copolymer contains at least 15 mol % of an isobutylene type donor monomer and at least 15 mol % of an acrylic monomer as an acceptor monomer. The copolymer is substantially free of maleate or fumarate monomer segments and the copolymer composition is substantially free of Lewis acids and transition metals. Also disclosed is a thermosetting composition that includes a reactant comprising functional groups, a crosslinking agent having at least two functional groups that are reactive with the functional groups first reactant, and a copolymer flow control agent that includes the copolymer composition as well as substrates coated with the thermosetting composition.

56. 发明授权

US06900279B2 Compositions containing copolymers of post-polymerization reacted (meth) acrylate monomers 失效
标题翻译：含有后聚合反应的（甲基）丙烯酸酯单体的共聚物的组合物
公开(公告)号：US06900279B2
公开(公告)日：2005-05-31
申请号：US10348367
申请日：2003-01-21
申请人： Simion Coca , Gregory J. McCollum , James B. O'Dwyer , Edward R. Coleridge , Steven V. Barancyk
发明人： Simion Coca , Gregory J. McCollum , James B. O'Dwyer , Edward R. Coleridge , Steven V. Barancyk
IPC分类号： B05D7/24 , B05D1/00 , B05D3/02 , B05D3/06 , B05D7/00 , B32B27/30 , C08F8/00 , C08F210/00 , C08F210/10 , C08F210/14 , C08F220/10 , C08F290/04 , C08G18/62 , C08G18/79 , C08G18/80 , C08K5/092 , C08L23/20 , C08L23/22 , C08L33/06 , C08L33/14 , C08L63/00 , C08L101/00 , C09D7/12 , C09D109/00 , C09D109/02 , C09D123/22 , C09D133/00 , C09D133/02 , C09D133/06 , C09D133/08 , C09D133/14 , C09D133/24 , C09D157/04 , C09D163/00 , C09D167/00 , C09D175/04 , C09D201/00 , C08F120/54 , C08F120/10
CPC分类号： B05D7/57 , B05D1/007 , B05D3/0209 , B05D3/067 , B05D7/53 , C08F8/00 , C08F210/10 , C08F220/10 , C08F290/046 , C08G18/6229 , C08G18/792 , C08G18/798 , C08G18/8025 , C08G18/807 , C08G18/8074 , C08G2150/20 , C08L33/068 , C09D123/22 , C09D133/062 , C09D133/08 , Y10T428/31504 , Y10T428/31511 , C08F220/00 , C08F220/12 , C08F210/00 , C08L2666/28 , C08L2666/02 , C08F214/18 , C08F2500/03 , C08F2500/02 , C08F212/00 , C08F222/00 , C08F2500/26 , C08L2666/04
摘要： A composition that includes a non-gelled copolymer that includes one or more residues of a first polymerizable ethylenically unsaturated monomer containing a pendant amide, ester or carboxylic acid group. The nearest neighboring monomer residues of the majority of the first monomer residues along the copolymer molecule do not contain pendant carbonyl functional groups. The amide, ester or carboxylic acid group of the residues of the first monomer are the post polymerization transesterification, transamidification or hydrolysis reaction product of a C1-C4 alkyl ester group in the unreacted first monomer with a compound selected from amine functional compounds and hydroxy functional compounds. The reacted copolymer is substantially free of cyclical structures resulting from the transesterification, transamidification or hydrolysis reaction. The compositions may be thermosetting compositions useful in multi-layer composite coatings.
摘要翻译：包含非凝胶共聚物的组合物，其包含含有侧酰胺，酯或羧酸基团的第一可聚合烯属不饱和单体的一个或多个残基。沿着共聚物分子的大部分第一单体残基的最邻近的单体残基不含有羰基官能团。第一单体的残基的酰胺，酯或羧酸基是C 1 -C 4烷基酯基的后聚合酯交换，转酰胺化或水解反应产物在未反应的第一单体中与选自胺官能化合物和羟基官能化合物的化合物反应。反应的共聚物基本上不含由酯交换，酰胺化或水解反应产生的循环结构。组合物可以是可用于多层复合涂层的热固性组合物。

57. 发明授权

US06677422B2 Method of making alternating copolymers of isobutylene type monomers 失效
标题翻译：制备异丁烯型单体的交替共聚物的方法
公开(公告)号：US06677422B2
公开(公告)日：2004-01-13
申请号：US10077559
申请日：2002-02-15
申请人： Simion Coca , Edward R. Coleridge , Gregory J. McCollum , James B. O'Dwyer , James E. Poole , Victoria A. Trettel
发明人： Simion Coca , Edward R. Coleridge , Gregory J. McCollum , James B. O'Dwyer , James E. Poole , Victoria A. Trettel
IPC分类号： C08F1000
CPC分类号： C08F220/12
摘要： A method of making a copolymer composition containing a copolymer, which includes the steps of (a) providing a donor monomer composition that includes an isobutylene type monomer; (b) mixing the donor monomer composition with an ethylenically unsaturated monomer composition that includes one or more ethylenically unsaturated acceptor monomers, and is substantially free of maleate type monomers and fumarate type monomers, and (c) polymerizing the mixture resulting from step (b) in the presence of a free radical polymerization initiator. The polymerization is carried out in the substantial absence of Lewis acids and/or transition metals. The isobutylene type monomer is present at a molar excess of at least 10 mol % based on the molar concentration of monomers in the ethylenically unsaturated monomer composition. The ethylenically unsaturated acceptor monomers are present in an amount of at least 15 mol % of the total monomer composition.
摘要翻译：一种制备含有共聚物的共聚物组合物的方法，其包括以下步骤：（a）提供包含异丁烯型单体的供体单体组合物; （b）将供体单体组合物与包含一种或多种烯键式不饱和受体单体的烯属不饱和单体组合物混合，并且基本上不含马来酸盐型单体和富马酸盐型单体，和（c）将由步骤（b）得到的混合物聚合，在自由基聚合引发剂存在下进行。基本上不存在路易斯酸和/或过渡金属进行聚合。基于烯属不饱和单体组合物中单体的摩尔浓度，异丁烯型单体的摩尔过量为至少10摩尔％。烯属不饱和受体单体的存在量为总单体组合物的至少15摩尔％。

58. 发明授权

US06641707B2 Biodegradation-resistant electrodepositable coating compositions and methods related thereto 失效
标题翻译：耐生物降解电沉积涂料组合物及其相关方法
公开(公告)号：US06641707B2
公开(公告)日：2003-11-04
申请号：US09855975
申请日：2001-05-15
申请人： Alan J. Kaylo , Gregory J. McCollum , Steven R. Zawacky
发明人： Alan J. Kaylo , Gregory J. McCollum , Steven R. Zawacky
IPC分类号： C08F258
CPC分类号： C09D5/4492 , C09D5/4457
摘要： Provided is a biodegradation resistant cationic electrodeposition composition of a resinous phase dispersed in an aqueous medium. The resinous phase includes an electrodepositable resin having cationic onium salt groups which have been at least partially solubilized with an &agr;-alkoxycarboxylic acid of formula (I), where R is C1 to C6 alkyl or aryl and R′ is H or C1 to C2 alkyl. Also provided is a method of electrocoating a conductive substrate serving as a cathode in an electrical circuit where the cathode and an anode are immersed in an aqueous electrodeposition bath containing the biodegradation resistant cationic electrodepositable composition described above, and substrates coated by the method.
摘要翻译：提供了分散在水性介质中的树脂相的抗生物降解性阳离子电沉积组合物。树脂相包括具有阳离子鎓盐基团的电沉积树脂，其已经用式（I）的α-烷氧基羧酸至少部分溶解，其中R是C1-C6烷基或芳基，R'是H或C1-C2烷基。还提供了将电极中的阴极和阴极浸渍在含有上述生物降解性阳离子电沉积组合物的水性电沉积浴中的电路中进行电涂覆的方法，以及通过该方法涂覆的基材。

59. 发明授权

US06423774B1 Cationic aliphatic polyester resins and their electrodeposition 有权
标题翻译：阳离子脂族聚酯树脂及其电沉积
公开(公告)号：US06423774B1
公开(公告)日：2002-07-23
申请号：US09531807
申请日：2000-03-21
申请人： Steven R. Zawacky , Raphael O. Kollah , Craig A. Wilson , Gregory J. McCollum , Robin M. Peffer , Geoffrey R. Webster, Jr. , Venkatachalam Eswarakrishnan , Linda K. Anderson
发明人： Steven R. Zawacky , Raphael O. Kollah , Craig A. Wilson , Gregory J. McCollum , Robin M. Peffer , Geoffrey R. Webster, Jr. , Venkatachalam Eswarakrishnan , Linda K. Anderson
IPC分类号： C08L6703
CPC分类号： C09D5/4423 , Y10S524/901
摘要： The present invention is directed to an electrodepositable composition of a resinous phase dispersed in an aqueous medium. The resinous phase includes an ionic polyester polymer prepared from a) an aromatic and/or cycloaliphatic carboxylic acid compound having at least two aromatic and/or secondary aliphatic carboxyl groups, b) a branched aliphatic, cycloaliphatic or araliphatic compound containing at least two aliphatic hydroxyl groups, the aliphatic hydroxyl groups being either secondary or tertiary hydroxyl groups or primary hydroxyl groups attached to a carbon adjacent to a tertiary or quaternary carbon, c) a compound including an ionic salt group or a group which is converted to an ionic salt group, and d) optionally, at least one hydroxyl substituted carboxylic compound comprising at least one tertiary aliphatic carboxyl group and at least two aliphatic hydroxyl groups. The present invention also includes a method for electrocoating a conductive substrate with the described electrodepositable composition. Lastly, the present invention is directed to a conductive substrate coated according to the described method.
摘要翻译：本发明涉及分散在水性介质中的树脂相的可电沉积组合物。树脂相包括由a）具有至少两个芳族和/或仲脂族羧基的芳族和/或脂环族羧酸化合物制备的离子聚酯聚合物，b）包含至少两个脂族羟基的支链脂族，脂环族或芳脂族化合物基团，脂族羟基是连接到与叔或季碳相邻的碳的仲羟基或叔羟基或伯羟基，c）包含离子盐基团或转化为离子盐基团的基团的化合物，和d）任选地，至少一种含有至少一个叔脂族羧基和至少两个脂族羟基的羟基取代的羧酸化合物。本发明还包括用所述电沉积组合物对导电基材进行电涂覆的方法。最后，本发明涉及根据所述方法涂覆的导电基底。

60. 发明授权

US06355729B1 Electrodepositable coating compositions comprising amine salt group-containing polymers prepared by atom transfer radical polymerization 失效
标题翻译：包含通过原子转移自由基聚合制备的含胺盐基聚合物的电沉积涂料组合物
公开(公告)号：US06355729B1
公开(公告)日：2002-03-12
申请号：US09375018
申请日：1999-08-16
申请人： Gregory J. McCollum , Linda K. Anderson , Simion Coca
发明人： Gregory J. McCollum , Linda K. Anderson , Simion Coca
IPC分类号： C08F892
CPC分类号： C09D5/4488 , C08L57/12 , C08L2666/02
摘要： Disclosed are thermosetting compositions which are comprised of a resinous phase dispersed in an aqueous medium, the resinous phase comprising (a) an ungelled active hydrogen group-containing polymer which contains amine salt groups, the polymer having been prepared by atom transfer radical polymerization in the presence of an initiator having at least one radically transferable group, and (b) a curing agent having at least two functional groups which are reactive with the active hydrogen groups of (a). The active hydrogen group-containing polymers of the thermosetting compositions, which are prepared by atom transfer radical polymerization, have narrow molecular weight distributions and well-defined, specifically tailored polymer architecture which can provide enhanced crosslink density and dispersibility of the thermosetting compositions. Also disclosed is a method of electrocoating a conductive substrate using the thermosetting compositions of the invention, and a substrate coated by this method.
摘要翻译：公开了由分散在水性介质中的树脂相组成的热固性组合物，所述树脂相包含（a）含有胺盐基团的未凝胶化含活性氢基团的聚合物，所述聚合物通过原子转移自由基聚合制备存在具有至少一个可自由基转移基团的引发剂，和（b）具有至少两个与（a）的活性氢基团反应的官能团的固化剂。通过原子转移自由基聚合制备的热固性组合物的含活性氢基团的聚合物具有窄的分子量分布和明确定义的专门定制的聚合物结构，其可以提供增强的热固性组合物的交联密度和分散性。还公开了使用本发明的热固性组合物和通过该方法涂覆的基材的电导涂层的方法。

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