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51. 发明申请

US20110028762A1 Process for Producing Cyclohexylbenzene 有权
标题翻译：生产环己基苯的方法
公开(公告)号：US20110028762A1
公开(公告)日：2011-02-03
申请号：US12904215
申请日：2010-10-14
申请人： Tan-Jen CHEN , Jane C. Cheng , Terry E. Helton , John Scott Buchanan
发明人： Tan-Jen CHEN , Jane C. Cheng , Terry E. Helton , John Scott Buchanan
IPC分类号： C07C45/28 , C07C5/10
CPC分类号： C07C2/74 , C07C37/08 , C07C45/53 , C07C2521/04 , C07C2521/06 , C07C2523/06 , C07C2523/14 , C07C2523/44 , C07C2523/46 , C07C2523/75 , C07C2523/755 , C07C2529/70 , C07C2529/74 , C07C2601/14 , Y02P20/52 , C07C13/28 , C07C39/04 , C07C49/403
摘要： In a process for producing cyclohexylbenzene, benzene and hydrogen are fed to at least one reaction zone. The benzene and hydrogen are then contacted in the at least one reaction zone under hydroalkylation conditions with a catalyst system comprising a molecular sieve having an X-ray diffraction pattern including d-spacing maxima at 12.4±0.25, 6.9±0.15, 3.57±0.07 and 3.42±0.07 Angstrom, and at least one hydrogenation metal to produce an effluent containing cyclohexylbenzene. The catalyst system has an acid-to-metal molar ratio of from about 75 to about 750.
摘要翻译：在生产环己基苯的方法中，将苯和氢气进料至至少一个反应区。然后使苯和氢在加氢烷基化条件下在至少一个反应区中与包含分子筛的催化剂体系接触，所述催化剂体系包含具有12.4±0.25,6.9±0.15,3.57±0.07的d间距最大值的X射线衍射图， 3.42±0.07埃，和至少一种氢化金属，以生产含有环己基苯的流出物。催化剂体系具有约75-约750的酸 - 金属摩尔比。

52. 发明申请

US20100179351A1 Process For Producing Cyclohexylbenzene 有权
标题翻译：生产环己基苯的方法
公开(公告)号：US20100179351A1
公开(公告)日：2010-07-15
申请号：US12663303
申请日：2008-08-12
申请人： Tan-Jen Chen , Jane C. Cheng , Terry E. Helton , John Scott Buchanan
发明人： Tan-Jen Chen , Jane C. Cheng , Terry E. Helton , John Scott Buchanan
IPC分类号： C07C2/02 , C07C45/27 , C07C37/08
CPC分类号： C07C2/74 , C07C37/08 , C07C45/53 , C07C2521/04 , C07C2521/06 , C07C2523/06 , C07C2523/14 , C07C2523/44 , C07C2523/46 , C07C2523/75 , C07C2523/755 , C07C2529/70 , C07C2529/74 , C07C2601/14 , Y02P20/52 , C07C13/28 , C07C39/04 , C07C49/403
摘要： In a process for producing cyclohexylbenzene, benzene and hydrogen are fed to at least one reaction zone. The benzene and hydrogen are then contacted in the at least one reaction zone under hydroalkylation conditions with a catalyst system comprising a molecular sieve having an X-ray diffraction pattern including d-spacing maxima at 12.4±0.25, 6.9±0.15, 3.57±0.07 and 3.42±0.07 Angstrom, and at least one hydrogenation metal to produce an effluent containing cyclohexylbenzene. The catalyst system has an acid-to-metal molar ratio of from about 75 to about 750.
摘要翻译：在生产环己基苯的方法中，将苯和氢气进料至至少一个反应区。然后使苯和氢在加氢烷基化条件下在至少一个反应区中与包含分子筛的催化剂体系接触，所述催化剂体系包含具有12.4±0.25,6.9±0.15,3.57±0.07的d间距最大值的X射线衍射图， 3.42±0.07埃，和至少一种氢化金属，以生产含有环己基苯的流出物。催化剂体系具有约75-约750的酸 - 金属摩尔比。

53. 发明申请

US20100040517A1 Process Of Manufacturing Para-Xylene 有权
标题翻译：对二甲苯制造工艺
公开(公告)号：US20100040517A1
公开(公告)日：2010-02-18
申请号：US12603956
申请日：2009-10-22
申请人： Stephen Harold Brown , John Scott Buchanan
发明人： Stephen Harold Brown , John Scott Buchanan
IPC分类号： B01J10/00
CPC分类号： C07C4/04 , C07C1/24 , C07C6/126 , C07C15/08
摘要： This disclosure relates to a process of manufacturing para-xylene, comprising (a) contacting a pygas feedstock and methylating agent with a catalyst under reaction conditions to produce a product having para-xylene, wherein the product has higher para-xylene content than the para-xylene content of the pygas feedstock; and (b) separating the para-xylene from the product of the step (a), wherein the catalyst comprises a molecular sieve having a Diffusion Parameter for 2,2-dimethylbutane of about 0.1-15 sec−1 when measured at a temperature of 120° C. and a 2,2-dimethylbutane pressure of 8 kPa-a and the pygas comprises from about 1 to about 65 wt % benzene and from about 5 to 35 wt % toluene.
摘要翻译：本公开涉及一种制备对二甲苯的方法，其包括（a）在反应条件下使炽热原料和甲基化剂与催化剂接触以产生具有对二甲苯的产物，其中该产物比对位二甲苯具有更高的对二甲苯含量焦炭原料的二甲苯含量; 和（b）从步骤（a）的产物中分离对二甲苯，其中当在下列温度下测量时，催化剂包含具有约0.1-15秒-1的2,2-二甲基丁烷扩散参数的分子筛 120℃，并且2,2-二甲基丁烷压力为8kPa-a，焦煤包含约1至约65重量％的苯和约5至35重量％的甲苯。

54. 发明授权

US07655823B2 Manufacture of xylenes from reformate 有权
标题翻译：从重整产生二甲苯
公开(公告)号：US07655823B2
公开(公告)日：2010-02-02
申请号：US11363831
申请日：2006-02-27
申请人： Gary D. Mohr , John Scott Buchanan , Robert A. Crane , Jihad M. Dakka , Xiaobing Feng , Larry L. Iaccino , Shifang L. Luo
发明人： Gary D. Mohr , John Scott Buchanan , Robert A. Crane , Jihad M. Dakka , Xiaobing Feng , Larry L. Iaccino , Shifang L. Luo
IPC分类号： C07C2/58
CPC分类号： C07C2/86 , C07C2521/02 , C07C2521/06 , C07C2521/08 , C07C2521/18 , C07C2523/02 , C07C2523/10 , C07C2523/18 , C07C2523/34 , C07C2523/40 , C07C2523/74 , C07C2527/14 , C07C2529/40 , C07C2529/65 , C07C2529/70 , C07C2529/85 , C10G2400/30 , C07C15/08
摘要： A process is provided for the production of xylenes from reformate. The process is carried out by methylating the benzene, toluene, or both present in the reformate to produce a resulting product having a higher xylenes content than the reformate. Greater than equilibrium amounts of para-xylene can be produced by the process.
摘要翻译：提供了从重整产生二甲苯的方法。该方法通过甲苯化存在于重整产物中的苯，甲苯或二者进行，以产生具有比重整产物更高的二甲苯含量的所得产物。通过该方法可以产生大于平衡量的对二甲苯。

55. 发明申请

US20090012338A1 Process for Aromatic Alkylation 有权
标题翻译：芳香烷基化方法
公开(公告)号：US20090012338A1
公开(公告)日：2009-01-08
申请号：US12208011
申请日：2008-09-10
申请人： Jihad Mohammed Dakka , John Scott Buchanan , Robert Andrew Crane , Christine Nicole Elia , Xiaobing Feng , Larry Lee Iaccino , Gary David Mohr , Brenda Anne Raich , Jose' Guadalupe Santiesteban , Lei Zhang
发明人： Jihad Mohammed Dakka , John Scott Buchanan , Robert Andrew Crane , Christine Nicole Elia , Xiaobing Feng , Larry Lee Iaccino , Gary David Mohr , Brenda Anne Raich , Jose' Guadalupe Santiesteban , Lei Zhang
IPC分类号： C07C2/64
CPC分类号： C07C2/864 , B01J29/40 , B01J29/44 , B01J2229/12 , B01J2229/32 , B01J2229/42 , C07C2521/10 , C07C2523/42 , C07C2523/46 , C07C2527/14 , C07C2529/40 , Y02P20/52 , Y10S585/906 , C07C15/08 , C07C15/00
摘要： This invention relates to a process for the selective alkylation of toluene and/or benzene with an oxygen-containing alkylation agent. In particular, the process uses a selectivated molecular sieve which has been modified by the addition of a hydrogenation component, wherein at least one of the following conditions is met: (a) the selectivated molecular sieve has an alpha value of less than 100 prior to the addition of the hydrogenation component, or (b) the selectivated and hydrogenated catalyst has an alpha value of less than 100. The process of this invention provides high selectivity for the alkylated product while reducing catalyst degradation.
摘要翻译：本发明涉及用含氧烷基化剂选择性烷基化甲苯和/或苯的方法。特别地，该方法使用已经通过加入氢化组分进行了改性的选择性分子筛，其中符合以下条件中的至少一个：（a）选择性分子筛之前的α值小于100，氢化组分的添加，或（b）选择和氢化的催化剂具有小于100的α值。本发明的方法在减少催化剂降解的同时，对烷基化产物提供高选择性。

56. 发明授权

US07453018B2 Process for aromatic alkylation 有权
标题翻译：芳烃烷基化方法
公开(公告)号：US07453018B2
公开(公告)日：2008-11-18
申请号：US10987324
申请日：2004-11-12
申请人： Jihad Mohammed Dakka , John Scott Buchanan , Robert Andrew Crane , Christine Nicole Elia , Xiaobing Feng , Larry Lee Iaccino , Gary David Mohr , Brenda Anne Raich , Jose′ Guadalupe Santiesteban , Lei Zhang
发明人： Jihad Mohammed Dakka , John Scott Buchanan , Robert Andrew Crane , Christine Nicole Elia , Xiaobing Feng , Larry Lee Iaccino , Gary David Mohr , Brenda Anne Raich , Jose′ Guadalupe Santiesteban , Lei Zhang
IPC分类号： C07C2/66
CPC分类号： C07C2/864 , B01J29/40 , B01J29/44 , B01J2229/12 , B01J2229/32 , B01J2229/42 , C07C2521/10 , C07C2523/42 , C07C2523/46 , C07C2527/14 , C07C2529/40 , Y02P20/52 , Y10S585/906 , C07C15/08 , C07C15/00
摘要： This invention relates to a process for the selective alkylation of toluene and/or benzene with an oxygen-containing alkylation agent. In particular, the process uses a selectivated molecular sieve which has been modified by the addition of a hydrogenation component, wherein at least one of the following conditions is met: (a) the selectivated molecular sieve has an alpha value of less than 100 prior to the addition of the hydrogenation component, or (b) the selectivated and hydrogenated catalyst has an alpha value of less than 100. The process of this invention provides high selectivity for the alkylated product while reducing catalyst degradation.
摘要翻译：本发明涉及用含氧烷基化剂选择性烷基化甲苯和/或苯的方法。特别地，该方法使用已经通过加入氢化组分进行了改性的选择性分子筛，其中符合以下条件中的至少一个：（a）选择性分子筛之前的α值小于100，氢化组分的添加，或（b）选择和氢化的催化剂具有小于100的α值。本发明的方法在减少催化剂降解的同时，对烷基化产物提供高选择性。

57. 发明申请

US20070185361A1 In-line process for generating comonomer 失效
标题翻译：产生共聚单体的在线方法
公开(公告)号：US20070185361A1
公开(公告)日：2007-08-09
申请号：US11518456
申请日：2006-09-08
申请人： John Scott Buchanan , Timothy D. Shaffer , James R. Lattner , John F. Walzer
发明人： John Scott Buchanan , Timothy D. Shaffer , James R. Lattner , John F. Walzer
IPC分类号： C07C2/02
CPC分类号： C07C2/32 , C07C2/36 , C07C2531/22 , C07C2531/24 , Y02P20/52 , C07C11/02
摘要： The present invention relates to an in-line method for generating comonomer from monomer, such as ethylene. The comonomer generated is directly transported, without isolation or storage, to a polyethylene polymerization reactor. The in-line method includes the steps of providing an in-line comonomer synthesis reactor and a downstream gas/liquid phase separator prior to the polymerization reactor; feeding ethylene monomer and a catalyst in a solvent and/or diluent to the comonomer synthesis reactor; reacting the ethylene monomer and the catalyst in solvent and/or diluent under reaction conditions to produce an effluent stream including ethylene monomer and comonomer; passing the effluent stream from the comonomer synthesis reactor to the downstream gas/liquid phase separator to separate a gas stream from a bottom stream, wherein the gas stream is a mixture of ethylene monomer and comonomer; and passing the gas stream to the polymerization reactor to provide the necessary comonomer input
摘要翻译：本发明涉及从单体如乙烯生成共聚单体的在线方法。生成的共聚单体直接输送到聚乙烯聚合反应器中，无需隔离或储存。在线方法包括在聚合反应器之前提供在线共聚单体合成反应器和下游气/液相分离器的步骤; 将乙烯单体和催化剂在溶剂和/或稀释剂中加入到共聚单体合成反应器中; 在反应条件下使乙烯单体和催化剂在溶剂和/或稀释剂中反应以产生包括乙烯单体和共聚单体的流出物流; 将来自共聚单体合成反应器的流出物流输送到下游气/液相分离器以从底部流分离气流，其中气流是乙烯单体和共聚单体的混合物; 并将气流送入聚合反应器以提供所需的共聚单体输入

58. 发明授权

US07176339B2 Manufacture of xylenes using reformate 有权
标题翻译：使用重整产品制造二甲苯
公开(公告)号：US07176339B2
公开(公告)日：2007-02-13
申请号：US10465058
申请日：2003-06-18
申请人： Larry L. Iaccino , Jeevan S. Abichandani , John Scott Buchanan , Robert A. Crane , Jihad M. Dakka , Xiaobing Feng , Shifang L. Luo , Gary D. Mohr
发明人： Larry L. Iaccino , Jeevan S. Abichandani , John Scott Buchanan , Robert A. Crane , Jihad M. Dakka , Xiaobing Feng , Shifang L. Luo , Gary D. Mohr
IPC分类号： C07C2/66
CPC分类号： C10G63/02 , C07C2/66 , C07C2/86 , C07C15/08 , C07C2521/02 , C07C2521/04 , C07C2521/06 , C07C2521/08 , C07C2521/18 , C07C2523/02 , C07C2523/10 , C07C2523/18 , C07C2523/34 , C07C2523/40 , C07C2523/42 , C07C2523/74 , C07C2527/14 , C07C2529/40 , C07C2529/60 , C07C2529/65 , C07C2529/70 , C07C2529/85 , C10G9/00 , C10G11/00 , C10G35/09 , C10G35/095 , C10G2300/1044 , C10G2300/4018 , C10G2400/30 , Y02P20/52
摘要： A process is provided for the production of xylenes from reformate. The process is carried out by methylating under conditions effective for the methylation, the benzene/toluene present in the reformate outside the reforming loop, to produce a resulting product having a higher xylenes content than the reformate. Greater than equilibrium amounts of para-xylene can be produced by the process.
摘要翻译：提供了从重整产生二甲苯的方法。该方法通过在有效甲基化的条件下甲基化进行，在重整循环外的重整产物中存在的苯/甲苯，产生的二甲苯含量高于重整产物。通过该方法可以产生大于平衡量的对二甲苯。

59. 发明授权

US07137622B2 De-entrainment of liquid particles from gas 有权
标题翻译：液体颗粒从气体中夹带
公开(公告)号：US07137622B2
公开(公告)日：2006-11-21
申请号：US10830168
申请日：2004-04-22
申请人： John Scott Buchanan
发明人： John Scott Buchanan
IPC分类号： B01F3/04 , B01D45/08
CPC分类号： B01D45/08 , B01D1/305 , B01D3/20
摘要： A multi-tray distillation unit having a separator for de-entraining liquid particles which are picked up by an upwardly flowing gaseous stream which is flowing countercurrent to a descending liquid flow in the unit. The separator which is placed above the contact plate on which the gas contacts the liquid, comprises vertically spaced tiers of elongated, substantially horizontal open-topped liquid collector channels arrayed in parallel rows transversely to the flow of the gas. The liquid collector channels are vertically staggered to deflect the gas flow from a lower tier level through the gaps between the collection channels of an upper tier and around the channels so as to cause the entrained liquid particles to separate from the gaseous stream by inertia into the channels of the lower tier. The collected liquid is then returned through a liquid downcomer to a contact plate. An improved channel configuration has a rigidly-mounted, horizontally-elongated flow deflector extending downwards from an upper tier channel toward a lower tier channel, this provides gas flow deflection and increased efficiency of liquid particle de-entrainment. The flow deflector may be mounted directly on each upper tier channel. The channels may be formed from a single crimped and perforated metal sheet or the like, and adjacent formed tiers may be stacked to form a de-entrainment zone array. The lower tier channels may be formed from a single metal sheet having a channel bottom and sides, with a foraminous section extending upwardly from one side and a transverse section extending away from the lower channel, and terminating in a flow deflector adjacent to the bottom of a channel of an upper tier.
摘要翻译：一种多托盘蒸馏装置，具有用于去除夹带液体颗粒的分离器，该分离器由向上流动的气流拾取，该气流与该单元中的下降液流逆流流动。放置在气体与液体接触的接触板上方的分离器包括垂直间隔的细长的基本上水平的开放顶部的液体收集器通道，其平行排列成横向于气体流。液体收集器通道垂直交错，以将气流从较低层级穿过上层的收集通道之间的间隙和通道周围的间隙，以使夹带的液体颗粒通过惯性与气流分离成下层渠道。然后将收集的液体通过液体降液管返回到接触板。改进的通道结构具有从上层通道向下层通道向下延伸的刚性安装的水平延伸的导流器，这提供了气体流动偏转和提高液体颗粒去夹带效率。导流板可以直接安装在每个上层通道上。通道可以由单个压接和穿孔的金属板等形成，并且相邻的成形层可以被堆叠以形成去夹带区域阵列。下层通道可以由具有通道底部和侧面的单个金属板形成，具有从一侧向上延伸的多孔部分和从下部通道延伸的横向部分，并且终止于邻近底部的导流器上层通道。

60. 发明授权

US07074739B2 Multi-component molecular sieve catalyst compositions and their use in aromatics reactions 有权
标题翻译：多组分分子筛催化剂组合物及其在芳烃反应中的应用
公开(公告)号：US07074739B2
公开(公告)日：2006-07-11
申请号：US10299170
申请日：2002-11-19
申请人： Jihad Mohammed Dakka , James Clarke Vartuli , John Scott Buchanan , Jose G. Santiesteban , Doron Levin
发明人： Jihad Mohammed Dakka , James Clarke Vartuli , John Scott Buchanan , Jose G. Santiesteban , Doron Levin
IPC分类号： B01J27/182 , B01J29/00
CPC分类号： B01J37/0009 , B01J21/06 , B01J21/066 , B01J23/10 , B01J29/06 , B01J29/40 , B01J29/82 , B01J35/0006 , B01J35/002 , B01J37/03 , B01J2229/20 , B01J2229/32 , B01J2229/36 , B01J2229/42 , C07C2/864 , C07C2521/06 , C07C2523/10 , Y02P20/52 , C07C15/08
摘要： The invention relates to a process for producing alkylated aromatic hydrocarbons, preferably with an oxygen or sulfur containing alkylating agent, in the presence of a multi-component molecular sieve catalyst composition that includes a molecular sieve and an active metal oxide. The invention is also directed to methods of making and formulating the multi-component molecular sieve catalyst composition useful in producing alkylated aromatics.
摘要翻译：本发明涉及在包含分子筛和活性金属氧化物的多组分分子筛催化剂组合物的存在下，优选用含氧或含硫烷基化剂制备烷基化芳烃的方法。本发明还涉及制备和配制用于制备烷基化芳族化合物的多组分分子筛催化剂组合物的方法。

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