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51. 发明授权

US08962509B2 Preparation of a solid catalyst system 有权
标题翻译：固体催化剂体系的制备
公开(公告)号：US08962509B2
公开(公告)日：2015-02-24
申请号：US13695884
申请日：2011-04-28
申请人： Kalle Kallio , Marja Mustonen , Pertti Elo , Peter Denifl , John Severn
发明人： Kalle Kallio , Marja Mustonen , Pertti Elo , Peter Denifl , John Severn
IPC分类号： C08F4/602 , C08F4/642 , C08F4/6592 , C08F10/00 , C08F4/76 , C07F5/06 , C08F4/52 , B01J31/12 , B01J31/14 , B01J31/22 , B01J31/26
CPC分类号： C08F4/76 , B01J31/124 , B01J31/128 , B01J31/143 , B01J31/2295 , B01J31/26 , B01J2531/46 , B01J2531/48 , B01J2531/49 , B01J2531/90 , B01J2531/94 , C07F5/068 , C08F4/52 , C08F4/6028 , C08F4/6592 , C08F4/65922 , C08F10/00 , C08F2410/01 , Y10S526/943 , C08F4/65912
摘要： Process for the preparation of a solid catalyst system (CS) comprising the steps of preparing a liquid clathrate (LC) comprising (a) a lattice (L) being the reaction product of (i) aluminoxane (A), (ii) an organometallic compound (O) of a transition metal (M) of Group 3 to 10 of the Periodic Table (IUPAC 2007) or of an actinide or lanthanide, and (i) a compound (B) being effective to form with the aluminoxane (A) and the organometallic compound (O) the lattice (L), and (b) a guest (G) being an hydrocarbon compound (HC), and subsequently precipitating said liquid clathrate (LC) obtaining said solid catalyst system (SC).
摘要翻译：制备固体催化剂体系（CS）的方法，包括以下步骤：制备液体包合物（LC），其包含（a）格子（L），其为（i）铝氧烷（A），（ii）有机金属（IUPAC 2007）第3至10族的过渡金属（M）或锕系元素或镧系元素的化合物（O）和（i）与铝氧烷（A）形成有效的化合物（B）和有机金属化合物（O），晶格（L）和（b）作为烃化合物（HC）的客体（G），随后沉淀得到所述固体催化剂体系（SC）的所述液体包合物（LC）。

52. 发明授权

US07341971B2 Production of olefin polymerization catalysts 有权
标题翻译：生产烯烃聚合催化剂
公开(公告)号：US07341971B2
公开(公告)日：2008-03-11
申请号：US10499760
申请日：2002-12-18
申请人： Peter Denifl , Erik Van Praet , Michael Bartke , Marita Oksman , Marja Mustonen , Thomas Garoff , Kari Pesonen
发明人： Peter Denifl , Erik Van Praet , Michael Bartke , Marita Oksman , Marja Mustonen , Thomas Garoff , Kari Pesonen
IPC分类号： B01J37/00 , C08F4/42
CPC分类号： C08F10/00 , C08F4/65925 , C08F4/65927 , C08F10/02 , C08F110/02 , Y10S526/943 , C08F4/65912 , C08F2/22
摘要： The invention provides a process for producing an olefin polymerization catalyst, comprising an organometallic compound of a transition metal or of an actinide or lanthanide, in the form of solid catalyst particles, comprising forming a liquid/liquid emulsion system which comprises a solution of one or more catalyst components dispersed in a solvent immiscible therewith; and solidifying said dispersed phase to convert said droplets to solid particles comprising the catalyst and optionally recovering said particles.
摘要翻译：本发明提供了一种生产烯烃聚合催化剂的方法，其包括过渡金属或锕系元素或镧系元素的有机金属化合物，其为固体催化剂颗粒形式，包括形成液体/液体乳液体系，其包含一种或多种更多的催化剂组分分散在与其不混溶的溶剂中; 并固化所述分散相以将所述液滴转化成包含催化剂的固体颗粒，并任选地回收所述颗粒。

53. 发明授权

US07238637B2 Method for the preparation of olefin polymerization catalysts 有权
标题翻译：烯烃聚合催化剂的制备方法
公开(公告)号：US07238637B2
公开(公告)日：2007-07-03
申请号：US10515997
申请日：2002-12-18
申请人： Thomas Garoff , Kari Pesonen , Päivi Waldvogel , Timo V. Laine , Peter Denifl , Jarmo Lindroos
发明人： Thomas Garoff , Kari Pesonen , Päivi Waldvogel , Timo V. Laine , Peter Denifl , Jarmo Lindroos
IPC分类号： C08F4/642 , C08F4/64 , C08F4/02
CPC分类号： C08F10/00 , C08F4/651 , C08F4/6546 , C08F4/6555
摘要： The invention provides a process for producing an olefin polymerization catalyst comprising a catalyst component formed by contacting at least (a) a compound of Group 1 to 3 of the Periodic Table (IUPAC) with (b) a transition metal compound of Group 4 to 10 of the Periodic Table (IUPAC) or a compound of an actinide or lanthanide, in the form of solid catalyst particles, said process comprising: (1) preparing a solution from said compounds; (2) dispersing said solution to a solvent immiscible therewith and inert in relation to said compounds, to obtain an emulsion in which said solution forms the dispersed phase; and (3) solidifying the catalyst component in the dispersed droplets.
摘要翻译：本发明提供了一种生产烯烃聚合催化剂的方法，其包括通过使（a）元素周期表（IUPAC）中第1至3族的化合物与（b）第4族至第10族的过渡金属化合物的周期表（IUPAC）或者以固体催化剂颗粒的形式的锕系元素或镧系元素的化合物，所述方法包括：（1）制备所述化合物的溶液; （2）将所述溶液分散到与其不混溶的溶剂中，并相对于所述化合物惰性，得到其中所述溶液形成分散相的乳液; 和（3）在分散的液滴中固化催化剂组分。

54. 发明授权

US08828901B2 Preparation of a solid catalyst system 有权
标题翻译：固体催化剂体系的制备
公开(公告)号：US08828901B2
公开(公告)日：2014-09-09
申请号：US13696184
申请日：2011-04-28
申请人： Kalle Kallio , Marja Mustonen , Pertti Elo , John Severn , Peter Denifl
发明人： Kalle Kallio , Marja Mustonen , Pertti Elo , John Severn , Peter Denifl
IPC分类号： C08F4/642 , C08F4/6592
CPC分类号： C08F4/76 , B01J31/0239 , B01J31/0268 , B01J31/124 , B01J31/128 , B01J31/143 , B01J31/2295 , B01J31/26 , B01J2531/90 , C08F4/52 , C08F4/6592 , C08F4/65922 , C08F10/00 , C08F2410/01 , C08F4/65912
摘要： Process for the preparation of a solid catalyst system comprising the steps of generating an emulsion by dispersing a liquid clathrate in a solution wherein (i) the solution constitutes the continuous phase of the emulsion and (ii) the liquid clathrate constitutes in form of droplets the dispersed phase of the emulsion, solidifying said dispersed phase to convert said droplets to solid particles and optionally recovering said particles to obtain said catalyst system, wherein the liquid clathrate comprises a lattice being the reaction product of aluminoxane, an organometallic compound of a transition metal of Group 3 to 10 of the Periodic Table (IUPAC 2007) or of an actinide or lanthanide, and a further compound being effective to form with the aluminoxane and the organometallic compound the lattice, and a guest being an hydrocarbon compound, and the solution comprises a silicon fluid and a hydrocarbon solvent.
摘要翻译：制备固体催化剂体系的方法，包括以下步骤：通过将液体包合物分散在溶液中产生乳液，其中（i）溶液构成乳液的连续相，和（ii）液体包合物以液滴的形式构成分散相，固化所述分散相，将所述液滴转化为固体颗粒，任选地回收所述颗粒以获得所述催化剂体系，其中所述液体包合物包含格子，其为铝氧烷，过渡金属的有机金属化合物周期表第3至10组（IUPAC 2007）或锕系元素或镧系元素，以及有效与铝氧烷和有机金属化合物形成晶格的另外的化合物，以及作为烃化合物的客体，该溶液包含硅液和烃溶剂。

55. 发明授权

US08791042B2 Process for the preparation of an unsupported, solid metallocene catalyst system and its use in polymerization of olefins 有权
标题翻译：制备无载体固体茂金属催化剂体系的方法及其在烯烃聚合中的应用
公开(公告)号：US08791042B2
公开(公告)日：2014-07-29
申请号：US13513450
申请日：2010-12-03
申请人： Nicolas Ronan , Peter Denifl
发明人： Nicolas Ronan , Peter Denifl
IPC分类号： C08F4/649 , C08F4/642 , C08F4/6592
CPC分类号： C08F10/00 , C08F4/65927 , C08F12/20 , C08F12/22 , C08F110/06 , C08F293/005 , C08F2410/01 , C08F2438/01 , C08F4/65912 , C08F2500/12
摘要： Process for the preparation of an unsupported, heterogeneous olefin polymerization catalyst system, comprising an organometallic compound of a transition metal of Group 3 to 10 of the Periodic Table (IUPAC 2007) in the form of solid particles comprising the steps of a) preparing a solution (A) comprising ai) an organometallic compound of a transition metal of Group 3 to 10 of the Periodic Table (IUPAC 2007) or of an actinide or lanthanide, a2) a cocatalyst comprising an element of group 13 of the Periodic Table (IUPAC 2007) and a3) a solvent (A-1), b) preparing a liquid/liquid emulsion system by dispersing the solution (A) in a solvent (B) essentially immiscible with said solution (A) in the presence of a polystyrene-b-fluoro polystyrene copolymer of the formula (I) in which n is a number from 10 to 100, m is a number from 1 to 40, x is a number from 5 to 16, y is a number from 11 to 33, provided that m, n, x and y are selected in a way that the block copolymer is soluble in the solvent B or the solution A in such an extent that a stable emulsion is formed by adding the block copolymer, b1) the solvent (B) constitutes the continuous phase of the emulsion, b2) the solution (A) constitutes in the form of droplets the dispersed phase and b3) the organometallic compound and the cocatalyst are present in the droplets, c) solidifying said dispersed phase to convert said droplets to solid particles and optionally recovering said particles to obtain said catalyst system; an unsupported, heterogeneous olefin polymerization catalyst, obtainable by the process and the use of the catalyst in olefin polymerization.
摘要翻译：制备无支撑的非均相烯烃聚合催化剂体系的方法，其包含固体颗粒形式的元素周期表第3至10族的过渡金属的有机金属化合物（IUPAC 2007），包括以下步骤：a）制备溶液（A）包含ai）周期表第3至10族过渡金属的有机金属化合物（IUPAC 2007）或锕系元素或镧系元素，a2）包含元素周期表第13族元素的助催化剂（IUPAC 2007 ）和a3）溶剂（A-1），b）通过将溶液（A）分散在基本上与所述溶液（A）不混溶的溶剂（B）中，在聚苯乙烯-b的存在下制备液体/液体乳液体系式（I）的氟代聚苯乙烯共聚物，其中n为10至100的数，m为1至40的数，x为5至16的数，y为11至33的数，条件是 m，n，x和y以嵌段共聚物可溶于溶剂中的方式选择 t B或溶液A，通过加入嵌段共聚物形成稳定的乳液，b1）溶剂（B）构成乳液的连续相，b2）溶液（A）以液滴的形式构成分散相和b3）有机金属化合物和助催化剂存在于液滴中，c）固化所述分散相以将所述液滴转化为固体颗粒，并任选地回收所述颗粒以获得所述催化剂体系; 一种无支撑的非均相烯烃聚合催化剂，可通过烯烃聚合中的方法和使用催化剂获得。

56. 发明申请

US20140190723A1 POWER CABLE COMPRISING POLYPROPYLENE 审中-公开
标题翻译：包含聚丙烯的电力电缆
公开(公告)号：US20140190723A1
公开(公告)日：2014-07-10
申请号：US14240552
申请日：2012-08-29
申请人： Torvald Vestberg , Peter Denifl , Per-Ola Hagstrand , Villgot Englund , Ulf Nilsson , Anders Nymark
发明人： Torvald Vestberg , Peter Denifl , Per-Ola Hagstrand , Villgot Englund , Ulf Nilsson , Anders Nymark
IPC分类号： H01B3/30 , H01B9/00
CPC分类号： H01B3/303 , C08F10/06 , C08F110/06 , C08F210/06 , C08L23/0815 , C08L23/10 , C08L23/16 , C08L2314/02 , C08L2314/06 , H01B3/441 , H01B9/00 , C08F4/6555 , C08F4/025 , C08F4/6465 , C08F2/02 , C08F210/16 , C08F2500/12 , C08F2/001
摘要： Power cable comprising a conductor surrounded by at least one layer comprising a polypropylene, wherein the polypropylene comprises nanosized catalyst fragments being evenly distributed in said polypropylene.
摘要翻译：电力电缆包括由包括聚丙烯的至少一层包围的导体，其中所述聚丙烯包括均匀分布在所述聚丙烯中的纳米尺寸的催化剂碎片。

57. 发明申请

US20130245212A1 PREPARATION OF A SOLID CATALYST SYSTEM 有权
标题翻译：固体催化剂体系的制备
公开(公告)号：US20130245212A1
公开(公告)日：2013-09-19
申请号：US13696184
申请日：2011-04-28
申请人： Kalle Kallio , Marja Mustonen , Pertti Elo , John Severn , Peter Denifl
发明人： Kalle Kallio , Marja Mustonen , Pertti Elo , John Severn , Peter Denifl
IPC分类号： C08F4/76 , C08F4/52
CPC分类号： C08F4/76 , B01J31/0239 , B01J31/0268 , B01J31/124 , B01J31/128 , B01J31/143 , B01J31/2295 , B01J31/26 , B01J2531/90 , C08F4/52 , C08F4/6592 , C08F4/65922 , C08F10/00 , C08F2410/01 , C08F4/65912
摘要： Process for the preparation of a solid catalyst system comprising the steps of generating an emulsion by dispersing a liquid clathrate in a solution wherein (i) the solution constitutes the continuous phase of the emulsion and (ii) the liquid clathrate constitutes in form of droplets the dispersed phase of the emulsion, solidifying said dispersed phase to convert said droplets to solid particles and optionally recovering said particles to obtain said catalyst system, wherein the liquid clathrate comprises a lattice being the reaction product of aluminoxane, an organometallic compound of a transition metal of Group 3 to 10 of the Periodic Table (IUPAC 2007) or of an actinide or lanthanide, and a further compound being effective to form with the aluminoxane and the organometallic compound the lattice, and a guest being an hydrocarbon compound, and the solution comprises a silicon fluid and a hydrocarbon solvent.
摘要翻译：制备固体催化剂体系的方法，包括以下步骤：通过将液体包合物分散在溶液中产生乳液，其中（i）溶液构成乳液的连续相，和（ii）液体包合物以液滴的形式构成分散相，固化所述分散相，将所述液滴转化为固体颗粒，任选地回收所述颗粒以获得所述催化剂体系，其中所述液体包合物包含格子，其为铝氧烷，过渡金属的有机金属化合物周期表第3至10组（IUPAC 2007）或锕系元素或镧系元素，以及有效与铝氧烷和有机金属化合物形成晶格的另外的化合物，以及作为烃化合物的客体，该溶液包含硅液和烃溶剂。

58. 发明授权

US08222175B2 Process for the preparation of an olefin polymerisation catalyst 有权
标题翻译：制备烯烃聚合催化剂的方法
公开(公告)号：US08222175B2
公开(公告)日：2012-07-17
申请号：US11794600
申请日：2005-12-22
申请人： Michael Bartke , Peter Denifl
发明人： Michael Bartke , Peter Denifl
IPC分类号： C08F4/602 , C08F4/6592 , B01J31/22
CPC分类号： C08F10/00 , C08F4/65927 , C08F110/06 , Y10S526/943 , C08F4/65912 , C08F4/65908 , C08F2500/18 , C08F2500/24
摘要： This invention relates to a process for the preparation of an olefin polymerization catalyst, to the use of the catalyst in olefin polymerization and to the catalyst and polymers obtained. In particular, the invention relates to the preparation of a catalyst comprising an organometallic compound of a transition metal of Group 3 to 10 of the Periodic Table (IUPAC) by a semi-continuous or continuous process.
摘要翻译：本发明涉及烯烃聚合催化剂的制备方法，烯烃聚合中催化剂的用途以及获得的催化剂和聚合物。特别地，本发明涉及通过半连续或连续方法制备包含周期表（IUPAC）的第3至10族的过渡金属的有机金属化合物的催化剂。

59. 发明申请

US20110213108A1 PROCESS FOR THE PREPARATION OF AN UNSUPPORTED, SOLID METALLOCENE CATALYST SYSTEM AND ITS USE IN POLYMERIZATION OF OLEFINS 有权
标题翻译：制备不需要的固体金属催化剂体系的方法及其在烯烃聚合中的应用
公开(公告)号：US20110213108A1
公开(公告)日：2011-09-01
申请号：US12998627
申请日：2009-11-04
申请人： Pertti Elo , John Severn , Peter Denifl , Soile Rautio , Marja Mustonen , Anu-Leena Hongell
发明人： Pertti Elo , John Severn , Peter Denifl , Soile Rautio , Marja Mustonen , Anu-Leena Hongell
IPC分类号： C08F4/6592 , B01J37/00 , B01J31/22
CPC分类号： C08F10/00 , C08F4/65925 , C08F210/16 , C08F4/65912 , C08F210/14 , C08F2500/18 , C08F2500/03 , C08F2500/12
摘要： Improved process for the preparation of an unsupported, heterogeneous olefin polymerization catalyst system, comprising an organometallic compound of a transition metal of Group 3 to 10 of the Periodic Table (IUPAC) or of an actinide or lanthanide in the form of solid particles comprising the steps of a) preparing a solution of catalyst components, including an aluminoxane, a compound being effective to form stable, liquid clathrates with aluminoxane and an organometallic compound of a transition metal of Group 3 to 10 of the Periodic Table (IUPAC 2007) or of an actinide or lanthanide, in a hydrocarbon solvent, yielding a two phase system with an upper solvent layer, which is separated, b) preparing a liquid/liquid emulsion system comprising a continuous phase in which said solution of the catalyst components forms a dispersed phase in the form of droplets, c) solidifying said dispersed phase to convert said droplets to solid particles and optionally recovering said particles to obtain said catalyst system, the catalysts system itself and its use for olefin polymerization.
摘要翻译：用于制备无支撑的非均相烯烃聚合催化剂体系的改进方法，其包含周期表（IUPAC）的第3至10族的过渡金属或固体颗粒形式的锕系元素或镧系元素的有机金属化合物，其包括步骤 a）制备催化剂组分溶液，包括铝氧烷，有效与铝氧烷和周期表第3至10族过渡金属的有机金属化合物（IUPAC 2007）形成稳定的液体包合物的化合物或锕系元素或镧系元素，在烃溶剂中，产生具有上溶剂层的两相体系，其被分离，b）制备液/液体乳液体系，其包含连续相，其中所述催化剂组分溶液形成分散相液滴的形式，c）固化所述分散相以将所述液滴转化为固体颗粒，并任选地回收所述颗粒以获得所述催化剂体系，催化剂体系本身及其在烯烃聚合中的应用。

60. 发明授权

US07608555B2 Method for the preparation of olefin polymerization catalysts 失效
标题翻译：烯烃聚合催化剂的制备方法
公开(公告)号：US07608555B2
公开(公告)日：2009-10-27
申请号：US11759086
申请日：2007-06-06
申请人： Thomas Garoff , Kari Pesonen , Päivi Waldvogel , Timo V. Laine , Peter Denifl , Jarmo Lindroos
发明人： Thomas Garoff , Kari Pesonen , Päivi Waldvogel , Timo V. Laine , Peter Denifl , Jarmo Lindroos
IPC分类号： C08F4/02 , C08F4/642
CPC分类号： C08F10/00 , C08F4/651 , C08F4/6546 , C08F4/6555
摘要： The present invention relates to a process for the production of catalysts, particularly of Ziegler-Natta type of catalysts for olefin polymerisation, to the catalysts as such, and to their use in polymerising olefins.
摘要翻译：本发明涉及用于生产催化剂，特别是用于烯烃聚合的齐格勒 - 纳塔型催化剂催化剂的方法，以及它们在烯烃聚合中的用途。

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