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51. 发明授权

US08057769B2 Method for making phosphate-based electrode active materials 失效
标题翻译：制造磷酸盐电极活性物质的方法
公开(公告)号：US08057769B2
公开(公告)日：2011-11-15
申请号：US12135271
申请日：2008-06-09
申请人： Jeremy Barker , M. Yazid Saidi
发明人： Jeremy Barker , M. Yazid Saidi
IPC分类号： C01B25/45 , H01M4/139
CPC分类号： H01M4/136 , C01B25/455 , H01M4/5825 , H01M4/587 , H01M4/623 , H01M10/0525
摘要： The invention is directed to synthesizing a phosphate-based electrode active material. The method includes the step of reacting two or more starting materials collectively containing at least a PO33− anion, an alkali metal and a metal which is redox active in the final reaction product, at a temperature and for a time sufficient to form the phosphate-based electrode active material.
摘要翻译：本发明涉及合成磷酸盐类电极活性物质。该方法包括在最终反应产物中，在足以形成磷酸盐化合物的温度和时间下将两种或多种起始原料共同含有至少含有PO33-阴离子，碱金属和至少为氧化还原活性的金属的步骤，基电极活性物质。

52. 发明授权

US07960059B2 Product and method for the processing of precursors for lithium phosphate active materials 有权
标题翻译：用于处理磷酸锂活性物质前体的产品和方法
公开(公告)号：US07960059B2
公开(公告)日：2011-06-14
申请号：US12046942
申请日：2008-03-12
申请人： George Adamson , Jeremy Barker , Allan Dirilo , Titus Faulkner , M. Yazid Saidi , Jeffrey Swoyer
发明人： George Adamson , Jeremy Barker , Allan Dirilo , Titus Faulkner , M. Yazid Saidi , Jeffrey Swoyer
IPC分类号： H01M4/58 , C01B25/45
CPC分类号： H01M4/5825 , H01M4/582 , H01M10/052
摘要： Methods for producing an electrode active material precursor, comprising; a) producing a mixture comprising particles of lithium hydrogen phosphate, having a first average particle size, and a metal hydroxide, having a second average particle size; and b) grinding said mixture in a jet mill for a period of time suitable to produce a generally homogeneous mixture of particles having a third average size smaller than said first average size. The precursor may be used as a starting material for making electrode active materials for use in a battery, comprising lithium, a transition metal, and phosphate or a similar anion.
摘要翻译：电极活性物质前体的制造方法， a）制备具有第一平均粒径的磷酸氢锂颗粒和具有第二平均粒径的金属氢氧化物的混合物; 以及b）在喷射式研磨机中研磨所述混合物一段适当的时间，以生产具有比所述第一平均尺寸小的第三平均尺寸的颗粒的均匀混合物。前体可以用作用于制造用于电池的电极活性材料的起始材料，其包括锂，过渡金属和磷酸盐或类似的阴离子。

53. 发明授权

US07901810B2 Battery active materials and methods for synthesis 有权
标题翻译：电池活性物质和合成方法
公开(公告)号：US07901810B2
公开(公告)日：2011-03-08
申请号：US10848452
申请日：2004-05-17
申请人： Jeremy Barker , M. Yazid Saidi , Jeffrey Swoyer
发明人： Jeremy Barker , M. Yazid Saidi , Jeffrey Swoyer
IPC分类号： H01M4/58 , H01M4/88 , H01M4/00
CPC分类号： C01B25/37 , H01M4/5825 , H01M10/0525
摘要： Active materials for rechargeable batteries have a general formula Aa(MO)bM′cXO4 where A represents an alkali metal or mixture of alkali metals, a is greater than about 0.1 and less than or equal to about 2; MO is an ion containing a transition metal M not in its highest oxidation state, M′ represents a metal, or mixture of metals, and b is greater than 0 and less than or equal to about 1, c is less than 1 wherein a, b and c are selected so as to maintain the electroneutrality of the compound, and X is phosphorus, arsenic, or sulfur, or mixtures thereof. Preferred active materials are alkali metal vanadyl metal phosphates of general formula Aa(VO)bM′cPO4 where a and b are both greater than 0 and c may be zero or greater. New synthetic routes are provided to alkali metal mixed metal phosphates where at least one of the starting materials is a metal-oxo group (MO)3+, where M represents a metal in a +5 oxidation state. Reductive methods are provided for reacting a metal-oxo phosphate with an alkali metal compound in the presence of reducing carbon. The carbothermal reduction step can for example result in the reduction of a +5 metal to a +4 state or lower.
摘要翻译：用于可再充电电池的活性材料具有通式Aa（MO）bM'cXO4，其中A表示碱金属或碱金属的混合物，a大于约0.1且小于或等于约2; MO是含有不处于其最高氧化态的过渡金属M的离子，M'表示金属或金属的混合物，b大于0且小于或等于约1，c小于1，其中a，选择b和c以保持化合物的电中性，X是磷，砷或硫，或其混合物。优选的活性物质是通式为Aa（VO）bM'cPO4的碱金属氧钒基金属磷酸盐，其中a和b都大于0，c可以为零或更大。向碱金属混合金属磷酸盐提供新的合成路线，其中至少一种原料是金属 - 氧代基（MO）3+，其中M表示+5氧化态的金属。提供还原方法，用于在还原性碳存在下使金属 - 氧代磷酸酯与碱金属化合物反应。碳热还原步骤可以例如将+5金属还原成+4状态或更低。

54. 发明申请

US20100330426A1 Electrode Active Material and Method of Making The Same 审中-公开
标题翻译：电极活性材料及其制作方法
公开(公告)号：US20100330426A1
公开(公告)日：2010-12-30
申请号：US12872904
申请日：2010-08-31
申请人： George W. Adamson , Jeremy Barker , Gerbrand Ceder , Ming Dong , Dane Morgan , M. Yazid Saidi
发明人： George W. Adamson , Jeremy Barker , Gerbrand Ceder , Ming Dong , Dane Morgan , M. Yazid Saidi
IPC分类号： H01M4/58
CPC分类号： H01M4/58 , C01P2002/72 , C04B35/447 , C04B2235/3203 , C04B2235/3206 , C04B2235/3239 , C04B2235/3244 , C04B2235/3251 , C04B2235/3262 , C04B2235/3272 , C04B2235/3277 , C04B2235/441 , C04B2235/449 , H01M4/136 , H01M4/382 , H01M4/582 , H01M4/5825 , H01M10/052 , H01M2300/0037
摘要： The invention provides an electrochemical cell which includes a first electrode and a second electrode which is a counter electrode to said first electrode, and an electrolyte material interposed there between. The first electrode includes an alkali metal phosphorous compound doped with an element having a valence state greater than that of the alkali metal.
摘要翻译：本发明提供了一种电化学电池，其包括第一电极和第二电极，第二电极是与所述第一电极对置的电极，以及介于其间的电解质材料。第一电极包括掺杂有具有大于碱金属的价态的元素的碱金属磷化合物。

55. 发明授权

US07270915B2 Alkali/transition metal HALO-and hydroxy-phosphates and related electrode active materials 有权
标题翻译：碱/过渡金属HALO和羟基磷酸盐及相关电极活性物质
公开(公告)号：US07270915B2
公开(公告)日：2007-09-18
申请号：US11223082
申请日：2005-09-09
申请人： Jeremy Barker , M. Yazid Saidi , Jeffrey Swoyer
发明人： Jeremy Barker , M. Yazid Saidi , Jeffrey Swoyer
IPC分类号： H01M4/58
CPC分类号： H01M4/485 , C01B25/455 , H01M4/136 , H01M4/505 , H01M4/525 , H01M4/58 , H01M4/5805 , H01M4/582 , H01M4/5825 , H01M4/583 , H01M10/052 , H01M10/0525 , H01M2004/028
摘要： The present invention relates to novel battery having a first electrode comprising an electrode active material represented by the general formula AaMb(XY4)2Zd, a second electrode which is a counter-electrode to the first electrode; and an electrolyte.
摘要翻译：本发明涉及具有第一电极的新型电池，所述第一电极包括由通式A表示的电极活性材料（XY 4）第二电极，其是与第一电极相对的电极;第二电极，其是与第一电极相对的电极; 和电解质。

56. 发明授权

US07060206B2 Synthesis of metal compounds under carbothermal conditions 有权
公开(公告)号：US07060206B2
公开(公告)日：2006-06-13
申请号：US10150343
申请日：2002-05-17
申请人： Jeremy Barker , M. Yazid Saidi , Jeffrey Swoyer , Ming Dong
发明人： Jeremy Barker , M. Yazid Saidi , Jeffrey Swoyer , Ming Dong
IPC分类号： H01M4/48 , H01M4/52 , C01B25/30 , C01D1/02
CPC分类号： H01M4/5825 , C01B25/37 , C01B25/45 , C01G21/00 , C01G31/00 , C01G39/00 , C01P2006/40 , H01M4/13 , H01M4/131 , H01M4/136 , H01M4/1391 , H01M4/1397 , H01M4/485 , H01M4/505 , H01M4/525 , H01M4/582 , H01M6/40 , H01M10/052 , H01M10/0525 , H01M10/0566 , Y10T29/10 , Y10T156/1002
摘要： Active materials of the invention contain at least one alkali metal and at least one other metal capable of being oxidized to a higher oxidation state. Preferred other metals are accordingly selected from the group consisting of transition metals (defined as Groups 4–11 of the periodic table), as well as certain other non-transition metals such as tin, bismuth, and lead. The active materials may be synthesized in single step reactions or in multi-step reactions. In at least one of the steps of the synthesis reaction, reducing carbon is used as a starting material. In one aspect, the reducing carbon is provided by elemental carbon, preferably in particulate form such as graphites, amorphous carbon, carbon blacks and the like. In another aspect, reducing carbon may also be provided by an organic precursor material, or by a mixture of elemental carbon and organic precursor material.

57. 发明授权

US07008566B2 Oligo phosphate-based electrode active materials and methods of making same 有权
标题翻译：磷酸磷酸酯基电极活性材料及其制备方法
公开(公告)号：US07008566B2
公开(公告)日：2006-03-07
申请号：US10409849
申请日：2003-04-08
申请人： Jeremy Barker , M. Yazid Saidi
发明人： Jeremy Barker , M. Yazid Saidi
IPC分类号： H01M4/58 , C01B25/37 , C01B25/26
CPC分类号： H01M4/5825 , H01B1/08
摘要： The invention provides an electrochemical cell which includes a first electrode and a second electrode which is a counter electrode to said first electrode, and an electrolyte material interposed there between. The first electrode includes an active material having an alkali metal-containing oligo phosphate-based electrode active material.
摘要翻译：本发明提供了一种电化学电池，其包括第一电极和第二电极，第二电极是与所述第一电极对置的电极，以及介于其间的电解质材料。第一电极包括具有含碱金属的磷酸酯类磷酸酯类电极活性物质的活性物质。

58. 发明授权

US06716372B2 Lithium-containing materials 有权
标题翻译：含锂材料
公开(公告)号：US06716372B2
公开(公告)日：2004-04-06
申请号：US10001376
申请日：2001-10-19
申请人： Jeremy Barker , M. Yazid Saidi , Jeffrey Swoyer
发明人： Jeremy Barker , M. Yazid Saidi , Jeffrey Swoyer
IPC分类号： C01B2537
CPC分类号： H01M4/5825 , C01B25/37 , C01B25/45 , C01G21/00 , C01G31/00 , C01G39/00 , C01P2006/40 , H01M4/13 , H01M4/131 , H01M4/136 , H01M4/1391 , H01M4/1397 , H01M4/485 , H01M4/505 , H01M4/525 , H01M4/582 , H01M6/40 , H01M10/052 , H01M10/0525 , H01M10/0566 , Y10T29/10 , Y10T156/1002
摘要： The invention provides novel lithium-mixed metal materials which, upon electrochemical interaction, release lithium ions, and are capable of reversibly cycling lithium ions. The invention provides a rechargeable lithium battery which comprises an electrode formed from the novel lithium-mixed metal materials. Methods for making the novel lithium-mixed metal materials and methods for using such lithium-mixed metal materials in electrochemical cells are also provided. The lithium-mixed metal materials comprise lithium and at least one other metal besides lithium. Preferred materials are lithium-mixed metal phosphates which contain lithium and two other metals besides lithium.
摘要翻译：本发明提供新的锂混合金属材料，其在电化学相互作用时释放锂离子，并且能够可逆地循环锂离子。本发明提供一种可再充电锂电池，其包括由新型锂混合金属材料形成的电极。还提供了制备新的锂复合金属材料的方法和在电化学电池中使用这种锂混合金属材料的方法。锂混合金属材料除锂之外还包含锂和至少一种其它金属。优选的材料是除了锂之外还含有锂和另外两种金属的锂混合金属磷酸盐。

59. 发明授权

US06447951B1 Lithium based phosphates, method of preparation, and uses thereof 有权
标题翻译：锂基磷酸盐，制备方法及其用途
公开(公告)号：US06447951B1
公开(公告)日：2002-09-10
申请号：US09195961
申请日：1998-11-19
申请人： Jeremy Barker , M. Yazid Saidi
发明人： Jeremy Barker , M. Yazid Saidi
IPC分类号： H01M458
CPC分类号： H01M10/052 , H01M4/136 , H01M4/1397 , H01M4/5825
摘要： The invention provides an electrochemical cell which comprises an electrode having a lithium metal phosphorous compound.
摘要翻译：本发明提供一种电化学电池，其包括具有锂金属磷化合物的电极。

60. 发明授权

US06869547B2 Stabilized electrochemical cell active material 失效
标题翻译：稳定的电化学电池活性材料
公开(公告)号：US06869547B2
公开(公告)日：2005-03-22
申请号：US09974043
申请日：2001-10-09
申请人： Jeremy Barker , M. Yazid Saldi , Jeffrey L. Swoyer
发明人： Jeremy Barker , M. Yazid Saldi , Jeffrey L. Swoyer
IPC分类号： C01G45/00 , C01G45/12 , H01M4/50 , H01M4/505 , H01M4/62 , H01M10/0525 , H01M10/0567 , H01M10/36 , H01M4/02
CPC分类号： H01M4/505 , C01G45/1242 , C01G45/125 , C01G45/1257 , C01P2002/32 , C01P2002/72 , C01P2002/77 , C01P2004/80 , C01P2004/84 , C01P2006/12 , C01P2006/40 , H01M4/62 , H01M10/0525 , H01M10/0567
摘要： Stabilized lithiated manganese oxide (LMO) is prepared by reacting cubic spinel lithium manganese oxide particles and particles of an alkali metal compound in air for a time and at a temperature sufficient to decompose at least a portion of the alkali metal compound, providing a treated lithium manganese oxide. The reaction product is characterized as particles having a core or bulk structure of cubic spinel lithium manganese oxide and a surface region which is enriched in Mn+4 relative to the bulk. X-ray diffraction data and x-ray photoelectron spectroscopy data are consistent with the structure of the stabilized LMO being a central bulk of cubic spinel lithium manganese oxide with a surface layer or region comprising A2MnO3, where A is an alkali metal. Electrochemical cells containing the stabilized LMO of the invention have improved charging and discharging characteristics and maintain integrity over a prolonged life cycle. The electrochemical cells are stabilized against decomposition of cell components, including electrode and electrolyte components.
摘要翻译：通过使立方尖晶石锂锰氧化物颗粒和碱金属化合物颗粒在空气中反应一段时间并在足以分解至少一部分碱金属化合物的温度下制备稳定的锂化锰氧化物（LMO），从而提供处理过的锂氧化锰。反应产物的特征在于具有立方尖晶石锂锰氧化物的核心或体积结构的颗粒和相对于体积富含Mn +4的表面区域。 X射线衍射数据和X射线光电子能谱数据与稳定的LMO的结构一致，稳定的LMO是具有包含A2MnO3的表面层或区域的立方尖晶石锂锰氧化物的中心体，其中A是碱金属。包含本发明的稳定的LMO的电化学电池具有改善的充电和放电特性并且在延长的寿命周期内保持完整性。电化学电池被稳定以防止细胞成分的分解，包括电极和电解质组分。

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