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51. 发明授权

US06777514B2 Geminally disubstituted olefin-carbon monoxide-ethylene polymer useful as a polyvinyl chloride plasticizer and a method of making same 失效
公开(公告)号：US06777514B2
公开(公告)日：2004-08-17
申请号：US10228755
申请日：2002-08-27
申请人： Abhimanyu O. Patil , Nicholas V. Smith , Jose G. Santiesteban , Allen D. Godwin , Steven P. Rucker , Stephen Zushma
发明人： Abhimanyu O. Patil , Nicholas V. Smith , Jose G. Santiesteban , Allen D. Godwin , Steven P. Rucker , Stephen Zushma
IPC分类号： C08F428
CPC分类号： C08G67/02 , C08L27/06 , C08L73/00 , C08L2666/14
摘要： The invention is related to a geminally disubstituted olefin-carbon monoxide-ethylene polymer. The invention is also related to a method for preparing geminally disubstituted olefin-carbon monoxide-ethylene polymers by reacting a geminally disubstituted olefin feed, a carbon monoxide feed and an ethylene feed under free radical polymerization conditions. The invention is further related to a geminally disubstituted olefin-carbon monoxide-ethylene-X polymer, where monomer X is a free radical polymerizable monomer. The invention is also directed to a method for preparing geminally disubstituted olefin-carbon monoxide-ethylene-X polymers by reacting a geminally disubstituted olefin feed, a carbon monoxide feed, an ethylene feed and a feed containing monomer X under free radical polymerization conditions. The polymers of the invention are useful as polyvinyl chloride plasticizers.

52. 发明授权

US06573396B2 Co-production of dialkyl carbonates and diols with treatment of hydroxy alkyl carbonate 失效
标题翻译：与碳酸二烷基酯和二醇共同生产碳酸羟基烷基酯
公开(公告)号：US06573396B2
公开(公告)日：2003-06-03
申请号：US09976608
申请日：2001-10-12
申请人： J. Scott Buchanan , Jose G. Santiesteban , Zhaozhong Jiang
发明人： J. Scott Buchanan , Jose G. Santiesteban , Zhaozhong Jiang
IPC分类号： C07C6996
CPC分类号： C07C68/065 , Y02P20/127 , C07C69/96
摘要： A process for the production of a dialkyl carbonate and a diol from a cyclic carbonate and an aliphatic monohydric alcohol wherein the cyclic carbonate and aliphatic monohydric alcohol are reacted in the presence of a transesterification catalyst to form a crude product stream which contains a dialkyl carbonate, a diol, a hydroxy alkyl carbonate, which is formed as an intermediate of the two step transesterification reaction, unreacted aliphatic monohydric alcohol and unreacted cyclic carbonate. The dialkyl carbonate and unreacted aliphatic monohydric alcohol are separated from the crude product stream and then the hydroxy alkyl carbonate is diminished, reduced or eliminated from the crude product stream, prior to the separation and purification steps needed to recover the diol, resulting in improved yields and product purity.
摘要翻译：一种由环状碳酸酯和脂族一元醇生产碳酸二烷基酯和二醇的方法，其中环状碳酸酯和脂肪族一元醇在酯交换催化剂的存在下反应，形成含有碳酸二烷基酯的粗产物流，作为两步酯交换反应的中间体形成的二醇，羟基烷基碳酸酯，未反应的脂肪族一元醇和未反应的环状碳酸酯。将碳酸二烷基酯和未反应的脂肪族一元醇与粗产物流分离，然后在回收二醇所需的分离和纯化步骤之前，从粗产物流中减少，还原或消除羟基烷基碳酸酯，从而提高产率和产品纯度。

53. 发明申请

US20080128329A1 Process for decreasing bromine-reactive contaminants in hydrocarbon feeds 失效
标题翻译：降低碳氢化合物进料中溴反应性污染物的方法
公开(公告)号：US20080128329A1
公开(公告)日：2008-06-05
申请号：US11633971
申请日：2006-12-05
申请人： Stephen H. Brown , Jose G. Santiesteban , Bryson J. Sundberg , Terry E. Helton , Daria N. Lissy , Jean W. Beeckman , Arthur P. Werner
发明人： Stephen H. Brown , Jose G. Santiesteban , Bryson J. Sundberg , Terry E. Helton , Daria N. Lissy , Jean W. Beeckman , Arthur P. Werner
IPC分类号： C10G25/03
CPC分类号： C10G29/02 , B01J29/7007 , B01J29/7038 , B01J35/023 , B01J35/026 , C10G2300/1096 , C10G2300/4018
摘要： A process for reducing the Bromine Index of a hydrocarbon feed containing bromine-reactive contaminants that has improved cycle length and utilizes a crystalline molecular sieve catalyst. The process is carried out by contacting the hydrocarbon feed under conversion conditions with a catalyst shaped in the form of an elongated aggregate comprising a crystalline molecular sieve having a MWW or *BEA framework type. The shortest cross-sectional dimension of the elongated aggregate is less about 1/10 inch (2.54 millimeters).
摘要翻译：一种降低含溴反应性污染物的烃进料的溴指数的方法，其具有改善的循环长度并且使用结晶分子筛催化剂。该方法通过在转化条件下使烃进料与包含具有MWW或* BEA骨架类型的结晶分子筛的细长骨料形式的催化剂接触来进行。细长骨料的最短横截面尺寸较小约为1/10英寸（2.54毫米）。

54. 发明授权

US06730142B2 Separation of propylene from hydrocarbon mixtures 有权
标题翻译：丙烯与烃混合物的分离
公开(公告)号：US06730142B2
公开(公告)日：2004-05-04
申请号：US10100978
申请日：2002-03-19
申请人： Sebastian C. Reyes , Venkatesan V. Krishnan , Gregory J. DeMartin , John H. Sinfelt , Karl G. Strohmaier , Jose G. Santiesteban
发明人： Sebastian C. Reyes , Venkatesan V. Krishnan , Gregory J. DeMartin , John H. Sinfelt , Karl G. Strohmaier , Jose G. Santiesteban
IPC分类号： B01D5304
CPC分类号： B01D53/04 , B01D53/02 , B01D53/0462 , B01D53/047 , B01D2253/30 , B01D2256/24 , B01D2257/702 , B01D2259/40083 , Y10S95/902
摘要： In a process for separating propylene from a mixture comprising propylene and propane, the mixture is passed through a bed of an adsorbent comprising a porous crystalline material having (i) a diffusion time constant for propylene of at least 0.1 sec−1, when measured at a temperature of 373° K and a propylene partial pressure of 8 kPa, and (ii) a diffusion time constant for propane, when measured at a temperature of 373° K and a propane partial pressure of 8 kPa, less than 0.02 of said diffusion time constant for propylene. The bed preferentially adsorbs propylene from the mixture. The adsorbed propylene is then desorbed from the bed either by lowering the pressure or raising the temperature of the bed.
摘要翻译：在从包含丙烯和丙烷的混合物中分离丙烯的方法中，将混合物通过包含多孔结晶材料的吸附剂床，该多孔结晶材料的床（i）丙烯的扩散时间常数至少为0.1秒-1，当在373°K的温度和8kPa的丙烯分压下测量，和（ii）丙烷的扩散时间常数，当在373°K的温度和8kPa的丙烷分压下测量时，小于0.02的所述丙烯的扩散时间常数。床优先从混合物中吸附丙烯。然后通过降低压力或提高床的温度，将吸附的丙烯从床中解吸。

55. 发明授权

US06548709B2 Method for the production of arylsulfides and compositions made therefrom 有权
公开(公告)号：US06548709B2
公开(公告)日：2003-04-15
申请号：US09973606
申请日：2001-10-09
申请人： Margaret M. Wu , Philip Trotto , Shifang Luo , Jose G. Santiesteban , Hye Kyung C. Timken , Sandeep S. Dhingra , Simon C. Weston , Richard T. Spissell
发明人： Margaret M. Wu , Philip Trotto , Shifang Luo , Jose G. Santiesteban , Hye Kyung C. Timken , Sandeep S. Dhingra , Simon C. Weston , Richard T. Spissell
IPC分类号： C07C31900
CPC分类号： C10M135/28 , C07C319/14 , C07C321/30
摘要： The present invention relates to methods for production of arylsulfides wherein an aromatic compound is reacted with elemental sulfur in the presence of solid acid catalyst. The solid acid catalyst can be a zeolite. The methods are useful for producing alkylated diphenylsulfides from aromatic compounds and elemental sulfur.

56. 发明授权

US06500996B1 Process for BTX purification 失效
标题翻译： BTX纯化方法
公开(公告)号：US06500996B1
公开(公告)日：2002-12-31
申请号：US09428762
申请日：1999-10-28
申请人： Stephen H. Brown , Tarun K. Chaudhuri , Jose G. Santiesteban
发明人： Stephen H. Brown , Tarun K. Chaudhuri , Jose G. Santiesteban
IPC分类号： C07C266
CPC分类号： C10G69/08 , C10G59/02 , C10G61/02
摘要： A process for the removal of hydrocarbon contaminants, such as dienes and olefins, from an aromatics reformate by contacting an aromatics reformate stream with a hydrotreating catalyst and/or a molecular sieve. The hydrotreating catalyst substantially converts all dienes to oligomers and partially converts olefins to alkylaromatics. The molecular sieve converts the olefins to alkylaromatics. The process provides an olefin depleted product which can be passed through a clay treater to substantially convert the remaining olefins to alkylaromatics. The hydrotreating catalyst has a metal component of nickel, cobalt, chromium, vanadium, molybdenum, tungsten, nickel-molybdenum, cobalt-nickel-molybdenum, nickel-tungsten, cobalt-molybdenum or nickel-tungsten-titanium, with a nickel molybdenum/alumina catalyst being preferred. The molecular sieve is an intermediate pore size zeolite, preferably MCM-22. The clay treatment can be carried out with any clay suitable for treating hydrocarbons.
摘要翻译：通过使芳族化合物重整产物流与加氢处理催化剂和/或分子筛接触，从芳族化合物重整产物中除去烃类污染物如二烯和烯烃的方法。加氢处理催化剂基本上将所有二烯转化为低聚物并将烯烃部分转化为烷基芳族化合物。分子筛将烯烃转化为烷基芳族化合物。该方法提供烯烃消耗产物，其可以通过粘土处理器以将剩余的烯烃基本上转化为烷基芳族化合物。加氢处理催化剂具有镍，钴，铬，钒，钼，钨，镍 - 钼，钴 - 镍 - 钼，镍 - 钨，钴 - 钼或镍 - 钨 - 钛的金属组分和镍钼/氧化铝催化剂是优选的。分子筛是中等孔径的沸石，优选MCM-22。粘土处理可以用适合于处理碳氢化合物的任何粘土进行。

57. 发明授权

US06489529B1 Production of monocycloalkyl aromatic compounds 有权
标题翻译：单环烷基芳族化合物的生产
公开(公告)号：US06489529B1
公开(公告)日：2002-12-03
申请号：US09490435
申请日：2000-01-24
申请人： Jane C. Cheng , Jose G. Santiesteban , Michael A. Steckel , James C. Vartuli
发明人： Jane C. Cheng , Jose G. Santiesteban , Michael A. Steckel , James C. Vartuli
IPC分类号： C07C1512
CPC分类号： C07C6/126 , C07C2521/06 , C07C2523/30 , C07C2529/70
摘要： There is described a process for the transalkylation of a polycycloalkyl aromatic compound, particularly the transalkylation of dicyclohexylbenzene to produce monocyclohexylbenzene. The process comprises contacting the polycycloalkyl aromatic compound with benzene in the presence of a catalyst selected from the group consisting of an acidic solid comprising a Group IVB metal oxide modified with an oxyanion of a Group VIBA metal oxide, TEA-mordenite, zeolite beta and a porous crystalline material having an X-ray diffraction pattern including d-spacing maxima at 12.4±0.25, 6.9±0.15, 3.57±0.07 and 3.42±0.07 Angstrom. Preferably the catalyst is a WOx/ZrO2 material.
摘要翻译：描述了多环烷基芳族化合物的烷基转移，特别是二环己基苯的烷基转移以产生单环己基苯的方法。该方法包括在选自以下的催化剂的存在下使多环烷基芳族化合物与苯接触，所述催化剂选自包含用VIBA族金属氧化物的氧阴离子改性的IVB族金属氧化物，TEA-丝光沸石，β沸石和具有12.4±0.25,6.9±0.15,3.57±0.07和3.42±0.07埃的d间距最大值的X射线衍射图的多孔结晶材料。优选地，催化剂是WO x / ZrO 2材料。

58. 发明授权

US06410804B1 Production of phenol using reactive distillation 失效
标题翻译：使用反应蒸馏生产苯酚
公开(公告)号：US06410804B1
公开(公告)日：2002-06-25
申请号：US09468465
申请日：1999-12-21
申请人： Doron Levin , Jose G. Santiesteban
发明人： Doron Levin , Jose G. Santiesteban
IPC分类号： C07C3708
CPC分类号： C07C37/08 , C07C45/53 , Y02P20/127 , Y10S203/06 , C07C49/08 , C07C39/04
摘要： A process for producing phenol and acetone from cumene hydroperoxide comprises: i) introducing a cumene hydroperoxide feed into a reactive distillation column comprising at its upper portion a distillation column and at its lower portion a catalyst bed, at a point above said catalyst bed; ii) mixing a diluting portion of acetone with said cumene hydroperoxide to provide a diluted cumene hydroperoxide; iii) directing said diluted cumene hydroperoxide through said catalyst bed under conditions sufficient to effect the exothermic decomposition of said cumene hydroperoxide to a product comprising a heavy fraction comprising phenol and a vaporized light fraction comprising acetone; iv) withdrawing said heavy fraction as bottoms from said column; v) flowing said vaporized light fraction upwards through the catalyst bed and at least a portion of the reactive distillation column; vi) condensing said light fraction to provide at least a portion of said diluting portion of acetone for subsequent mixing with said cumene hydroperoxide feed; vii) optionally withdrawing a portion of said light fraction as overhead from said column; and viii) repeating steps i) through vii). An apparatus for carrying out the process is also provided.
摘要翻译：从氢过氧化枯烯生产苯酚和丙酮的方法包括：i）将氢过氧化枯烯进料引入反应性蒸馏塔，反应蒸馏塔在其上部包含蒸馏塔，其下部在催化剂床的上方加入催化剂床; ii 将丙酮的稀释部分与所述异丙基氢过氧化物混合以提供稀释的氢过氧化枯烯; iii）在足以使所述异丙基氢过氧化氢发生放热分解的产物的条件下将所述稀释的氢过氧化枯烯引导通过所述催化剂床，所述产物包含含有苯酚以及包含丙酮的气化轻馏分; iv）从所述塔中抽出所述重馏分作为塔底物; v）使所述蒸发的轻馏分向上通过催化剂床和至少一部分反应蒸馏塔; vi）将所述轻馏分冷凝至提供所述丙稀稀释部分的至少一部分用于随后的混合物 g用所述异丙基氢过氧化物进料; vii）任选地将所述轻馏分的一部分从塔中取出; 和viii）重复步骤i）至vii）。还提供了一种用于执行该过程的装置。

59. 发明授权

US06207850B1 Process for co-production of dialkyl carbonate and alkanediol 有权
标题翻译：共同生产碳酸二烷基酯和链烷二醇的方法
公开(公告)号：US06207850B1
公开(公告)日：2001-03-27
申请号：US09433362
申请日：1999-11-03
申请人： Zhaozhong Jiang , Rene B. LaPierre , Jose G. Santiesteban , Hye Kyung Cho Timken , William A. Weber
发明人： Zhaozhong Jiang , Rene B. LaPierre , Jose G. Santiesteban , Hye Kyung Cho Timken , William A. Weber
IPC分类号： C07C6806
CPC分类号： C07C29/1285 , C07C68/065 , C07C69/96 , C07C31/202
摘要： A method is provided for co-producing dialkyl carbonate and alkanediol by reacting alkylene carbonate with alkanol in the presence of a IIIA metal oxide catalyst, preferably alumina.
摘要翻译：提供了一种通过在IIIA金属氧化物催化剂，优选氧化铝的存在下使碳酸亚烷基酯与链烷醇反应来共同生产碳酸二烷基酯和链烷二醇的方法。

60. 发明授权

US06169216A Production of phenol 有权
标题翻译：生产苯酚
公开(公告)号：US06169216A
公开(公告)日：2001-01-02
申请号：US09296852
申请日：1999-04-22
申请人： Doron Levin , Jose G. Santiesteban , James C. Vartuli
发明人： Doron Levin , Jose G. Santiesteban , James C. Vartuli
IPC分类号： C07C3708
CPC分类号： C07C37/08 , B01J27/053 , C07C45/53 , Y02P20/52 , C07C49/08 , C07C39/04
摘要： A process for producing phenol and acetone from cumene hydroperoxide is described in which the cumene hydroperoxide is contacted with a solid-acid catalyst comprising a sulfated transition metal oxide, preferably sulfated zirconia.
摘要翻译：描述了由氢过氧化枯烯生产苯酚和丙酮的方法，其中氢过氧化枯烯与包含硫酸化过渡金属氧化物，优选硫酸化氧化锆的固体酸催化剂接触。

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