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51. 发明专利

DE10133054A1 Catalyst for the gas phase hydrogenation of dicarboxylic acids comprises copper oxide, palladium and/or a palladium compound and an oxide support 未知
公开(公告)号：DE10133054A1
公开(公告)日：2003-01-16
申请号：DE10133054
申请日：2001-07-07
申请人： BASF AG
发明人： SCHLITTER STEPHAN , BORCHERT HOLGER , HESSE MICHAEL , SCHUBERT MARKUS , BOTTKE NILS , FISCHER ROLF-HARTMUTH , ROESCH MARKUS , HEYDRICH GUNNAR , WECK ALEXANDER
IPC分类号： B01J23/89 , B01J37/02 , B01J37/03 , C07D307/08 , C07D307/33 , C07D315/00
摘要： A catalyst (I) for the gas phase hydrogenation of 4C-dicarboxylic acids and/or derivatives, preferably maleic acid anhydride, comprises copper oxide (20-94 wt.%), palladium and/or a palladium compound (0.005-5 wt.%) and an oxide support (2-79.995 wt.%) comprising oxides of Al, Si, Zn, La, Ce, Group IIIa-VIIIa elements and/or Group IA and II elements. Independent claims are also included for: (i) a process for the production of the catalyst (I) by impregnation of an oxide supported copper oxide catalyst with a solution of a soluble palladium compound, drying and optionally calcining; and (ii) a process for the gas phase hydrogenation of 4C-dicarboxylic acids and/or derivatives, preferably maleic acid anhydride in the presence of the catalyst (I).

52. 发明专利

ES2283873T3 PROCEDIMIENTO PARA LA OBTENCION DE ALQUILARILSULFONATOS POR MEDIO DE OLEFINAS MODIFICADAS DIMERIZADAS. 未知
公开(公告)号：ES2283873T3
公开(公告)日：2007-11-01
申请号：ES03799498
申请日：2003-12-22
申请人： BASF AG
发明人： NARBESHUBER THOMAS , STEINBRENNER ULRICH , WIEBELHAUS DAG , BOTTKE NILS
IPC分类号： C07C303/06 , C11D1/22 , C11D11/04
摘要： Procedimiento para la obtención de alquilarilsulfonatos mediante a) reacción de una mezcla de olefinas con 4 átomos de carbono en un catalizador de metátesis para la obtención de una mezcla de olefinas que contiene 2-penteno y/o 3-hexeno, y en caso dado separación de 2-penteno y/o 3-hexeno, b) dimerizado de 2-penteno y/o 3-hexeno obtenido en la etapa a) en presencia de un catalizador de dimerizado para dar una mezcla que contiene olefinas con 10 a 12 átomos de carbono, separación de las olefinas con 10 a 12 átomos de carbono, y separación de un 5 a un 30% en peso, referido a las olefinas separadas con 10 a 12 átomos de carbono, en componentes de bajo punto de ebullición de las olefinas con 10 a 12 átomos de carbono, c) reacción de las mezclas de olefinas con 10 a 12 átomos de carbono obtenidas en la etapa b) con un hidrocarburo aromático en presencia de un catalizador de alquilado para la formación de compuestos alquilaromáticos, pudiéndose añadir antes de la reacción adicionalmente un 0 aun 60% en peso, preferentemente un 0 a un 40% en peso, referido a las mezclas de olefinas con 10 a 12 átomos de carbono, obtenidas en la etapa b), de olefinas lineales, d) sulfonado de compuestos alquilaromáticos obtenidos en la etapa c) y neutralizado para dar alquilarilsulfonatos, pudiéndose añadir antes del sulfonado adicionalmente un 0 a un 60% en peso, preferentemente un 0 a un 50% en peso, referido a los compuestos alquilaromáticos obtenidos en la etapa c), de alquilbencenos lineales, en tanto no se efectúe un mezclado en la etapa c), e) en caso dado mezclado de los alquilarilsulfonatos obtenidos en la etapa d) con un 0 a un 60% en peso, preferentemente un 0 a un 30% en peso, referido a los alquilarilsulfonatos obtenidos en la etapa d), en alquilarilsulfonatos lineales, en tanto no se efectúen mezclados en las etapas c) y d).

53. 发明专利

AT365712T 未知
公开(公告)号：AT365712T
公开(公告)日：2007-07-15
申请号：AT03743348
申请日：2003-02-28
申请人： BASF AG
发明人： FISCHER ROLF-HARTMUTH , ROESCH MARKUS , BOTTKE NILS , WECK ALEXANDER , WINDECKER GUNTHER , HESSE MICHAEL , BORCHERT HOLGER , SCHLITTER STEPHAN
IPC分类号： C07D207/26 , B01J23/72 , B01J23/80 , C07B61/00 , C07D207/267 , C07D307/08
摘要： A process for coproducing alkyl-substituted or unsubstituted THF and pyrrolidones by catalytically hydrogenating C 4 -dicarboxylic acids and/or derivatives thereof in the gas phase in the presence of copper catalysts and reacting GBL with ammonia or primary amines to give pyrrolidones comprises a) hydrogenating C 4 -dicarboxylic acids and/or derivatives thereof in the gas phase at from 200 to 300° C., from 0.1 to 100 bar, catalyst hourly space velocities of from 0.01 to 1 kg of reactant/l of catalyst*hour and reactant/hydrogen molar ratios of from 20 to 800 in the presence of catalysts comprising copper, aluminum and/or zinc to give mixtures of THF and GBL, b) separating the hydrogenation effluent obtained by distillation into a THF/water mixture as the top product and a GBL-containing bottom product, c) separating the THF/water mixture from step b) in a distillation facility consisting of three columns by withdrawing water from the bottom of the first column, recycling water-containing THF from the second into the first column, passing a side stream of the first into the second column, recycling the bottom product of the third column into the first column and withdrawing a distillate at the top of the first column, wherein a side stream of the second column is passed into the third column and the pure THF is obtained as the top product of the third column, d) recovering GBL from the GBL-containing bottom product from step b) by distillation and e) reacting the GBL obtained with ammonia or amines to give corresponding pyrrolidones.

54. 发明专利

AT357430T 未知
公开(公告)号：AT357430T
公开(公告)日：2007-04-15
申请号：AT03799498
申请日：2003-12-22
申请人： BASF AG
发明人： NARBESHUBER THOMAS , STEINBRENNER ULRICH , WIEBELHAUS DAG , BOTTKE NILS
IPC分类号： C11D1/22 , C11D11/04 , C07C303/06
摘要： The invention relates to processes for the preparation of alkylarylsulfonates

55. 发明专利

ZA200505050B Methods for producing alkylaryl sulfonates by using modified dimerized olefins 未知
公开(公告)号：ZA200505050B
公开(公告)日：2006-09-27
申请号：ZA200505050
申请日：2005-06-22
申请人： BASF AG
发明人： NARBESHUBER THOMAS , STEINBRENNER ULRICH , WIEBELHAUS DAG , BOTTKE NILS
IPC分类号： C07C20060101 , C11D20060101 , C11D1/22 , C11D11/04
摘要： The invention relates to processes for the preparation of alkylarylsulfonates

56. 发明专利

DE50302908D1 未知
公开(公告)号：DE50302908D1
公开(公告)日：2006-05-18
申请号：DE50302908
申请日：2003-08-28
申请人： BASF AG
发明人： FISCHER ROLF-HARTMUTH , BOTTKE NILS
IPC分类号： C07C29/136 , C07C213/00 , C07B53/00 , C07B61/00 , C07C29/149 , C07C31/20 , C07C31/22 , C07C215/08
摘要： The invention relates to a process for preparing optically active 2-amino-, 2-chloro-, 2-hydroxy- or 2-alkoxy-1-alcohols by catalytically hydrogenating appropriate optically active 2-amino-, 2-chloro-, 2-hydroxy- and 2-alkoxycarboxylic acids or their acid derivatives in the presence of catalysts comprising palladium and rhenium or platinum and rhenium.

57. 发明专利

DE102004038108A1 未知
公开(公告)号：DE102004038108A1
公开(公告)日：2006-03-16
申请号：DE102004038108
申请日：2004-08-05
申请人： BASF AG
发明人： BOTTKE NILS , TRILLER MICHAEL , MUELLER ULRICH , PINKOS ROLF , HEIDEMANN THOMAS
IPC分类号： C07C2/66 , B01J21/16 , C07B37/02 , C07C15/02 , C07C303/06 , C07C309/31
摘要： The present invention relates to a process for preparing alkylaromatics by reacting aromatic compounds with C1-C14-alkanes in the presence of a heterogeneous catalyst, which comprises using as the catalyst a crystalline, micro- and/or mesoporous solid comprising silicon and at least one father element selected from the group consisting of the transition metals and the main group elements gallium and tin, and activating said catalysts by a reducing pretreatment. Furthermore, the present invention relates to a process for preparing alkylarylsulfonates by sulfonating and neutralizing the alkyl aromatic compounds.

58. 发明专利

AT299872T 未知
公开(公告)号：AT299872T
公开(公告)日：2005-08-15
申请号：AT03709732
申请日：2003-02-28
申请人： BASF AG
发明人： WINDECKER GUNTHER , WECK ALEXANDER , FISCHER ROLF-HARTMUTH , ROESCH MARKUS , BOTTKE NILS , HESSE MICHAEL , SCHLITTER STEPHAN , BORCHERT HOLGER
IPC分类号： B01D3/14 , C07D307/08
摘要： Crude water-containing tetrahydrofuran is purified by passing the crude tetrahydrofuran through three distillation columns, withdrawing water from the bottom of the first column, recycling water-containing tetrahydrofuran from the top of the second column into the first column, passing a sidestream of the first column into the second column, recycling the bottom product of the third column into the first column, and withdrawing a distillate at the top of the first column. Additionally, a sidestream of the second column is passed into the third column and the purified tetrahydrofuran is recovered as the top product of the third column.

59. 发明专利

DE102004003310A1 Producing slightly branched alkylaromatics by alkylating aromatics with olefins comprises reducing the hydroperoxide content of the olefin feed 未知
公开(公告)号：DE102004003310A1
公开(公告)日：2005-08-11
申请号：DE102004003310
申请日：2004-01-22
申请人： BASF AG
发明人： BOSCH MARCO , BOTTKE NILS , BENFER REGINA , NARBESHUBER THOMAS
IPC分类号： B01J29/18 , C07C2/66 , C07C15/107 , C07C303/06 , C07C309/31 , C07C2/58 , C07C6/04 , C07C7/12 , C07C309/30
摘要： Producing slightly branched alkylaromatics by alkylating aromatics with olefins in the presence of an acid catalyst comprises reducing the hydroperoxide content of the olefin feed to less than 1 g per kg of catalyst per hour by treatment with an inorganic hydride. An independent claim is also included for producing alkylaryl sulfonates by contacting a C4 olefin mixture with a metathesis catalyst to produce an olefin mixture containing 2-pentene and/or 3-hexene; optionally separating the 2-pentene and/or 3-hexene; dimerizing the 2-pentene and/or 3-hexene, optionally together with C4 and/or C7 olefins, in the presence of a dimerization catalyst, to give a C8-C14 olefin mixture; optionally separating the C8-C14 olefins and separating 5-30 wt.% of low boilers; reducing the hydroperoxide content of the C8-C14 olefin mixture as above; optionally adding linear olefins in an amount of 0-60 wt.%; reacting the C8-C14 olefin mixture with aromatics in the presence of an acid catalyst to produce alkylaromatics; optionally adding linear alkylbenzenes in an amount of 0-60 wt.%; sulfonating the alkylaromatics and neutralizing the products to give alkylaryl sulfonates; and optionally mixing the alkylaryl sulfonates with 0-60 wt.% (words missing).

60. 发明专利

DE10350333A1 未知
公开(公告)号：DE10350333A1
公开(公告)日：2005-05-25
申请号：DE10350333
申请日：2003-10-29
申请人： BASF AG
发明人： BOTTKE NILS , BENFER REGINA , BOSCH MARCO , NARBESHUBER THOMAS , STEINBRENNER ULRICH , STEPHAN JUERGEN
IPC分类号： C07C2/66 , C11D1/22 , C07C15/107 , C07C2/00
摘要： In a process for preparing alkylaryl compounds by reacting a C10-14-monoolefin mixture with an aromatic hydrocarbon in the presence of an alkylation catalyst to form alkyl aromatic compounds and if appropriate subsequently sulfonating and neutralizing the resulting alkylaryl compounds, in the C10-14-monoolefins, on average, more than 0% and up to 100% of methyl branches are present in the longest carbon chain and fewer than 50% of the methyl branches are in the 2-, 3- and 4-position, calculated starting from the chain ends of the longest carbon chain.

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