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51. 发明专利

CA2560096A1 HYDROCYANATION METHOD 未知
公开(公告)号：CA2560096A1
公开(公告)日：2005-08-11
申请号：CA2560096
申请日：2005-01-26
申请人： BASF AG
发明人： BAUMANN ROBERT , LUYKEN HERMANN , HADERLEIN GERD , KUNSMANN-KEITEL DAGMAR PASCALE , BARTSCH MICHAEL , JUNGKAMP TIM , SCHEIDEL JENS
IPC分类号： C07C253/10 , C07C255/07
摘要： A process is described for preparing 3-pentenenitrile by hydrocyanating 1,3-butadiene with hydrogen cyanide over at least one catalyst, wherein the 1,3-butadiene and/or hydrogen cyanide is contacted with at least one microporous solid before the reaction.

52. 发明专利

CA2553028A1 METHOD FOR PRODUCING DINITRILES 未知
公开(公告)号：CA2553028A1
公开(公告)日：2005-08-11
申请号：CA2553028
申请日：2005-01-27
申请人： BASF AG
发明人： JUNGKAMP TIM , BAUMANN ROBERT , BARTSCH MICHAEL , LUYKEN HERMANN , HADERLEIN GERD , SCHEIDEL JENS
IPC分类号： C07C253/10 , C07C255/04
摘要： The invention relates to a method for producing adipodinitrile and methylglutar nitrile, said method being characterised by the following steps : (a) an educt flow containing pentenenitriles is reacted with hydrogen cyanid e in the presence of at least one catalyst and at least one promoter to obtain a reaction flow containing pentenenitriles, the at least one catalyst, catalys t breakdown products, the at least one promoter, adipodinitrile and methylglut ar nitrile; (b) the reaction flow is distilled to obtain a bottom product flow (3) that is depleted of pentenenitriles and contains the at least one catalyst, catalyst breakdown products, the at least one promoter, adipodinitrile and methylglutar nitrile, and a top product flow (4) enriched in pentenenitriles; (c) the flow (3) is extracted by an extraction means contained in flow (5) to obtain a top product flow (6) that is enriched with extraction means and contains the catalyst, and a bottom product flow (7) th at is depleted of extraction means and contains catalyst breakdown products, th e at least one promoter, pentenenitriles, adipodinitrile and methylglutar nitrile; (d) the flow (6) is distilled to obtain a bottom product flow (8) containing the catalyst, and a top product flow (9) containing the extractio n means; (e) the flow (7) is distilled to obtain a bottom product flow (10) containing catalyst breakdown products, the at least one promoter, pentene nitriles, adipodinitrile and methylglutarnitrile, and a top product flow (11 ) containing the extraction means; (f) the flow (10) is distilled to obtain a bottom product flow (12) containing catalyst breakdown products, the at leas t one promoter, pentenenitriles, adipodinitrile and methylglutarnitrile, and a top product flow (13) containing pentenenitriles; (g) the flow (12) is distilled to obtain a bottom product flow (14) containing catalyst breakdown products and the at least one promoter, and a top product flow (15) containi ng adipodinitrile and methylglutar nitrile; and (h) the flow (15) is distilled to obtain a bottom product flow (16) containing adipodinitrile, and a top produ ct flow (17) containing methylglutarnitrile.

53. 发明专利

DE10350999A1 未知
公开(公告)号：DE10350999A1
公开(公告)日：2005-06-02
申请号：DE10350999
申请日：2003-10-30
申请人： BASF AG
发明人： BARTSCH MICHAEL , BAUMANN ROBERT , HADERLEIN GERD , FLORES MIGUEL , JUNGKAMP TIM , LUYKEN HERMANN , SCHEIDEL JENS , SIEGEL WOLFGANG
IPC分类号： B01J31/18 , B01J31/24 , C07C253/10 , C07C253/30 , C07C255/07 , C07C255/09 , C07F9/12 , C07F9/48 , C07F9/50 , C07F9/6574 , C07F9/46 , C07F15/04 , C07C253/08 , C07C255/06 , C07C255/04
摘要： The invention relates to phosphinite phosphites I of formula 1, 2, 3, 4, 5 or 6 and mixtures thereof, wherein R1, R2, R4 independently represent an alkyl or alkylene group with 1 to 8 carbon atoms, provided that at least one of the groups R1, R2, R4 is different from H; R5 to R22 independently represent H, an alkyl or alkylene group with 1 to 8 carbon atoms; R3 is H, methyl or ethyl; X is F, Cl or CF3, if n=1 or 2 and X is H, if n=0.

54. 发明专利

DE10351002A1 未知
公开(公告)号：DE10351002A1
公开(公告)日：2005-05-25
申请号：DE10351002
申请日：2003-10-30
申请人： BASF AG
发明人： HADERLEIN GERD , BAUMANN ROBERT , BARTSCH MICHAEL , JUNGKAMP TIM , LUYKEN HERMANN , SCHEIDEL JENS , SCHAEFER HEINZ , SIEGEL WOLFGANG
IPC分类号： B01J31/18 , C01G53/08 , C07F15/04 , B01J31/24 , C07B43/08 , C07B37/08 , C07C253/10 , C07C253/30 , C07C5/22
摘要： A process is described for preparing a nickel(0)-phosphorus ligand complex containing at least one nickel(0)central atom and at least one phosphorus ligand, which comprises reducing a nickel(II) halide dried by azeotropic distillation in the presence of at least one phosphorus ligand.

55. 发明专利

CA2544051A1 USE OF AZEOTROPICALLY DRIED NICKEL(II) HALOGENIDES 未知
公开(公告)号：CA2544051A1
公开(公告)日：2005-05-12
申请号：CA2544051
申请日：2004-10-28
申请人： BASF AG
发明人： HADERLEIN GERD , BAUMANN ROBERT , BARTSCH MICHAEL , LUYKEN HERMANN , SIEGEL WOLFGANG , SCHAEFER HEINZ , SCHEIDEL JENS , JUNGKAMP TIM
IPC分类号： C07F15/04 , B01J31/16 , B01J31/18 , C01G53/00 , C01G53/08
摘要： A process is described for preparing a nickel(0)-phosphorus ligand complex containing at least one nickel(0)central atom and at least one phosphorus ligand, which comprises reducing a nickel(II) halide dried by azeotropic distillation in the presence of at least one phosphorus ligand.

56. 发明专利

DE10323803A1 未知
公开(公告)号：DE10323803A1
公开(公告)日：2004-11-11
申请号：DE10323803
申请日：2003-04-22
申请人： BASF AG
发明人： BARTSCH MICHAEL , BAUMANN ROBERT , HADERLEIN GERD , FLORES MIGUEL , JUNGKAMP TIM , LUYKEN HERMANN , SCHEIDEL JENS , SIEGEL WOLFGANG , KUNSMANN-KEITEL DAGMAR PASCALE
IPC分类号： C07C253/30 , C07C255/07
摘要： A process for isomerizing cis-2-pentenenitrile to trans-3-pentenenitrile in the presence of aluminum oxide as a catalyst, wherein the aluminum oxide has a BET surface area of at least 50 m 2 /g.

57. 发明专利

CA2520571A1 SYSTEM SUITABLE FOR THE HYDROCYANATION OF OLEFINICALLY UNSATURATED COMPOUNDS 未知
公开(公告)号：CA2520571A1
公开(公告)日：2004-10-14
申请号：CA2520571
申请日：2004-03-24
申请人： BASF AG
发明人： JUNGKAMP TIM , FLORES MIGUEL ANGEL , LUYKEN HERMANN , SCHEIDEL JENS , MOLNAR FERENC , BAUMANN ROBERT , HADERLEIN GERD , BARTSCH MICHAEL , SIEGEL WOLFGANG
IPC分类号： B01J23/755 , B01J31/02 , B01J31/14 , B01J31/18 , C07C253/10 , C07C255/04 , B01J27/14 , B01J27/18
摘要： A system suitable for use as a catalyst for the hydrocyanation of olefinical ly unsaturated compounds, containing a) Ni(0), b) Ni(0) as a ligand complex- fixing compound containing trivalent phosphorus, c) a Lewis acid and d) a compound of formula MRn wherein M = AI or Ti, R= identical or different monovalent alkoxyl radicals, wherein several alkoxy radicals can be interbridged, also in the case where M = AI, R = identical or different alky l radicals wherein several alkyl radicals can be interbridged or one or severa l alkyl radicals can be bridged by one or several of the above-mentioned alkox y radicals, n = valency of M. The invention also relates to methods for the hydrocyanation of an olefinically unsaturationed compound in the presence of said system.

58. 发明专利

BR0212965A 未知
公开(公告)号：BR0212965A
公开(公告)日：2004-10-13
申请号：BR0212965
申请日：2002-10-04
申请人： BASF AG
发明人： BARTSCH MICHAEL , BAUMANN ROBERT , KUNSMANN-KEITEL DAGMAR PASCALE , HADERLEIN GERD , JUNGKAMP TIM , ALMAYER MARCO , SIEGEL WOLFGANG , MOLNAR FERENC
IPC分类号： B01J31/22 , B01J31/18 , C07B61/00 , C07C253/10 , C07C253/30 , C07C255/04 , C07C255/07 , C07F9/48
摘要： The invention relates to phosphinites I of formulae (1) or (2), in which R1, R2, R5, R6, R7, R8, R9 independently represent hydrogen, an alkyl or alkylene group having 1 to 8 carbon atoms or an alkoxy group having 1 to 8 carbon atoms; R3 is H or methyl; R4 is i-propyl or t-butyl; X is F, Cl or CF 3 and n is 1 or 2.

59. 发明专利

BR0213108A 未知
公开(公告)号：BR0213108A
公开(公告)日：2004-09-21
申请号：BR0213108
申请日：2002-10-04
申请人： BASF AG
发明人： BARTSCH MICHAEL , BAUMANN ROBERT , KUNSMANN-KEITEL DAGMAR PASCALE , HADERLEIN GERD , JUNGKAMP TIM , ALMAYER MARCO , SIEGEL WOLFGANG , MOLNAR FERENC
IPC分类号： B01J31/22 , B01J31/18 , C07B61/00 , C07C253/10 , C07C253/30 , C07C255/04 , C07C255/07 , C07F9/46 , C07F15/04 , C07F9/50
摘要： Phosphinites I of the formula 1, 2 or 3 where R1, R2, R4 are each, independently of one another, hydrogen, an alkyl or alkylene group having from 1 to 8 carbon atoms or an alkoxy group having from 1 to 8 carbon atoms, with the proviso that at least one of the groups R1, R2, R4 is not H, R3 is H or methyl X is F, Cl or CF 3 n is 0, 1 or 2 can be used as catalysts.

60. 发明专利

BR0211455A 未知
公开(公告)号：BR0211455A
公开(公告)日：2004-08-17
申请号：BR0211455
申请日：2002-07-16
申请人： BASF AG
发明人： BARTSCH MICHAEL , BAUMANN ROBERT , KUNSMANN-KEITEL DAGMAR PASCALE , HADERLEIN GERD , JUNGKAMP TIM , ALMAYER MARCO , SIEGEL WOLFGANG
IPC分类号： B01J31/22 , B01J23/755 , B01J31/18 , B01J31/24 , C07B61/00 , C07C253/10 , C07C255/04
摘要： A system comprising a) Ni(0) b) from 4 to 10 mol per mol of Ni(0) in a) of a compound (I) of the formula P(X1R1)(X2R2)(X3R3) (I) where X1, X2, X3 are each, independently of one another, oxygen or a single bond, R1, R2, R3 are, independently of one another, identical or different organic radicals and c) from 1 to 4 mol per mol of Ni(0) in a) of a compound (II) of the formula where X11, X12, X13 X21, X22, X23 are each, independently of one another, oxygen or a single bond, R11, R12 are identical or different, individual or bridged organic radicals, R21, R22 are identical or different, individual or bridged organic radicals and Y is a bridging group is suitable as catalyst for preparing mixtures of monoolefinic C5 mononitriles having nonconjugated C═C and C═N bonds by hydrocyanation of a 1,3-butadiene-containing hydrocarbon mixture and for preparing a dinitrile by hydrocyanation of a mixture of monoolefinic C5 mononitriles having nonconjugated C═C and C═N bonds.

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