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41. 发明申请

WO9849130A3 HYDROXYNAPHTHOIC ACIDS AND DERIVATIVES 审中-公开
标题翻译：羟基磷酸和衍生物
公开(公告)号：WO9849130A3
公开(公告)日：1999-01-28
申请号：PCT/US9808544
申请日：1998-04-28
申请人： UNIV NEW MEXICO
发明人： VANDER JAGT DAVID L , DECK LORRAINE M , ROYER ROBERT E
IPC分类号： C07C51/29 , C07C51/377 , C07C65/11 , C07C67/343 , C07C235/66 , C07C69/76 , C07C63/34 , C07C233/00
CPC分类号： C07C235/66 , C07C51/29 , C07C51/377 , C07C65/11 , C07C67/343 , C07C65/24 , C07C63/36 , C07C69/734
摘要： In one embodiment, the present invention provides a compound comprising formula (I), wherein A = H or OH, X = OH, a halogen, OR, NHR, NR', R'' where R, R', and R'' = H, C1-8alkyl, C2-8alkenyl, or C2-8alkynyl, cycloalkyl, cycloalkenyl, aryl, aralkyl or heterocyclic, substituted or unsubstituted; and R1,R2,R3,R4,R5 = H, C1-8alkyl, C2-8alkenyl, or C2-8alkynyl, cycloalkyl, cycloalkenyl, aryl or heterocyclic, substituted or unsubstituted, wherein R1 includes at least one methylene spacer through which R1 is attached to said compound. The present invention also provides methods for making hydroxynaphthoic acids.

42. 发明申请

WO2016101517A1 制备氯甲酰基取代苯的清洁工艺审中-公开
公开(公告)号：WO2016101517A1
公开(公告)日：2016-06-30
申请号：PCT/CN2015/079272
申请日：2015-05-19
申请人：上海方纶新材料科技有限公司
发明人：王农跃 , 瞿雄伟 , 李国华 , 邵建明 , 赵全忠 , 闻国强
IPC分类号： C07C51/64 , C07C63/34 , C07C63/30 , C07C63/70 , C07C63/10 , C07C63/307
CPC分类号： C07C51/64 , C07C63/10 , C07C63/30 , C07C63/307 , C07C63/34 , C07C63/70
摘要：本发明属于化工技术领域，涉及一种制备氯甲酰基取代苯的清洁工艺。本发明的工艺通过氧化氯化反应和酰氯化反应的尾气氯化氢，并将所获得的氧化产物氯气回用到氯化反应中。本发明是一种制备聚合级氯甲酰基取代苯的清洁工艺。

43. 发明申请

WO2007082639A1 VERWENDUNG VON ESTERN MIT VERZWEIGTEN ALKYLGRUPPEN ALS SCHMIERMITTEL 审中-公开
标题翻译：酯的使用支链烷基ALS GREASE
公开(公告)号：WO2007082639A1
公开(公告)日：2007-07-26
申请号：PCT/EP2007/000034
申请日：2007-01-04
申请人： COGNIS IP MANAGEMENT GMBH , SCHERER, Markus , RETTEMEYER, Dirk
发明人： SCHERER, Markus , RETTEMEYER, Dirk
IPC分类号： C10M105/34 , C10M105/36 , C10M129/70 , C10M129/72 , C07C69/003 , C07C69/24 , C07C63/34 , C07C69/36 , C07C69/38 , C07C69/40 , C07C69/42 , C07C69/44 , C07C69/46 , C07C69/48 , C07C69/50
CPC分类号： C10M105/36 , C10M105/34 , C10M129/70 , C10M129/72 , C10M2207/281 , C10M2207/2815 , C10M2207/282 , C10M2207/2825 , C10N2220/025 , C10N2220/028 , C10N2230/10 , C10N2230/36 , C10N2230/64 , C10N2240/04 , C10N2240/08 , C10N2240/10 , C10N2240/14 , C10N2240/30 , C10N2240/40
摘要： Vorgeschlagen wird die Verwendung von Estern mit verzweigten Alkylgruppen, welche Reaktionsprodukte darstellen von Alkoholen der allgemeinen Formel (I) R 1 OH, in der R 1 für einen verzweigten Alkylrest mit 10 bis 40 C-Atomen steht mit: a) aliphatischen Dicarbonsäuren der allgemeinen Formel (II) HOOC-R 2 -COOH, in der R 2 für einen verzweigten oder unverzweigten, gesättigten Alkylrest mit 0 bis 34 C-Atomen steht, oder b) gesättigten Monocarbonsäuren der allgemeinen Formel (III) R 3 -COOH, in der R 3 für einen verzweigten Alkylrest aus 3 bis 39 C-Atomen steht, oder c) gesättigte Monocarbonsäuren der allgemeinen Formel (III) in der R 3 für einen linearen Alkylrest aus 3 bis 29 C-Atomen steht, oder d) einer Mischung aus mindestens zwei der genannten Säuregruppe a)-c) als Schmiermittel mit der Maßgabe, dass die Ester mit verzweigten Alkylgruppen eine Oxidationsstabilität von größer oder gleich 1000 Stunden in einem Test auf Oxidationsstabilität (beispielsweise nach DIN EN ISO 4263-3) aufweisen und eine Verträglichkeit gegenüber Dichtungsmaterialien (beispielsweise nach ASTM D 471), zeigen. Des Weiteren werden Schmiermittel vorgeschlagen, enthaltend die genannten Ester mit verzweigten Alkylgruppen in Mengen von 0,1 bis 99,5 Gew.-%, bezogen auf die Gesamtmenge an Schmiermittel.
摘要翻译：提出了使用具有支链烷基酯，其是通式（I）R的醇的反应产物的^{1 OH，R ^{1 是具有10的支链烷基 40个碳原子，具有：a）将通式脂族二羧酸（II）HOOC-R ^{2 -COOH，其中R ^{2 是一个支链或无支链的，饱和烷基是0至34个碳原子，或b）饱和通式单羧酸（III）R ^{3 -COOH，其中R ^{3 是一个支链的烷基的3〜是39个C原子，或c）饱和通式单羧酸（III），其中R ^{3 是直链烷基3至29个碳原子的，或d）中的至少两种的混合物酸基团的）-c）称为与具有支链的酯的烷基基团具有大于或氧化稳定性等于1000小时条件的润滑剂包括用于氧化稳定性的试验（例如，根据DIN EN ISO 4263-3），并用密封材料兼容性（例如，根据ASTM D 471）显示。具有支链含有所述的酯。此外，提出了润滑剂的烷基中的0.1的量至99.5重量％，基于润滑剂的总量。}}}}}}}

46. 发明专利

JPH0395139A PRODUCTION OF AROMATIC CARBOXYLIC ACID 失效
公开(公告)号：JPH0395139A
公开(公告)日：1991-04-19
申请号：JP23429589
申请日：1989-09-08
申请人： OSAKA GAS CO LTD
发明人： NOMURA MASAKATSU
IPC分类号： C07D307/91 , C07C51/285 , C07C63/06 , C07C63/331 , C07C63/34 , C07C63/42 , C07C66/02
摘要： PURPOSE:To directly and efficiently obtain the title compound useful as a raw material for polymer fiber, plastic, etc., by using a solvent soluble component of coal liquefied oil as a raw material and subjecting the component to direct oxidation reaction without using the component for hydrogenating decomposition reaction. CONSTITUTION:A solvent-soluble component from coal liquefied oil formed in a large amount in liquefying coal is subjected to direct oxidation reaction to give the objective compound. An aliphatic hydrocarbon such as hexane, heptane or octane, alicyclic hydrocarbon such as cyclohexane or an aromatic hydrocarbon such as benzene is used as a solvent to extract the solvent-soluble component. Oxidation reaction with an oxidizing agent such as potassium dichromate or air oxidation reaction in the presence of a catalyst (e.g. V2O5) is used as the oxidation reaction. In case of using the oxidizing agent, the temperature is 200-300 deg.C and in case of using the catalyst, the temperature is 300-500 deg.C.

47. 发明专利

JPH02252613A SEPARATING AND RECOVERING METHOD OF CERIUM COMPOUND 失效
公开(公告)号：JPH02252613A
公开(公告)日：1990-10-11
申请号：JP7127089
申请日：1989-03-23
申请人： SUMIKIN CHEMICAL
发明人： DOUKO YOSHIHARU , MAEDA KAZUHIKO , SUGIURA KAZUKI
IPC分类号： B01J38/60 , C01F17/00 , C07C51/47 , C07C63/34
摘要： PURPOSE:To recover cerium in high yield by adding aqueous solution of sulfuric acid to a mixture containing naphthalenecarboxylic acid and Ce compound, separating insoluble naphthalenecarboxylic acid and adding alkaline aqueous solution. CONSTITUTION:An aqueous solution of sulfuric acid is added to a mixture containing naphthalenecarboxylic acid and cerium compound to dissolve the cerium compound in the aqueous solution of sulfuric acid. Next, insoluble naphthalenecarboxylic acid is separated from said aqueous solution and an alkaline aqueous solution is added to the aqueous solution of sulfuric acid, then the cerium compound is separated and recovered as a solid to separate and recover cerium compound. Naphthoic acid, naphthalenedicarboxylic acid, naphthalenetricarboxylic acid or naphthalenetetracarboxylic acid is utilized as naphthalenecarboxylic acid. On the other hand, aqueous solution of sodium hydroxide, potassium hydroxide, calcium hydroxide, sodium carbonate, potassium carbonate, sodium bicarbonate or potassium bicarbonate is used as alkaline aqueous solution.

48. 发明专利

JPH02250849A PURIFICATION OF NAPHTHALENECARBOXYLIC ACID 失效
公开(公告)号：JPH02250849A
公开(公告)日：1990-10-08
申请号：JP7126789
申请日：1989-03-23
申请人： SUMIKIN CHEMICAL
发明人： YAMADA TERUAKI , MAEDA KAZUHIKO , SUGIURA KAZUKI , NAMEKATA TAKESHI
IPC分类号： C07C51/487 , C07C63/34
摘要： PURPOSE:To obtain a purified naphthalenecarboxylic acid free from discoloration in high purity by a simple operation by oxidizing a substituted naphthalene to give a crude naphthalenecarboxylic acid and additionally oxidizing the crude naphthalenecarboxylic acid with O2 in the presence of an alkali metal compound in a solvent. CONSTITUTION:A substituted naphthalene is oxidized to give a crude naphthalenecarboxylic acid(NCA), which is oxidized with molecular oxygen in the presence of an alkali metal compound in a solvent, preferably dissolved in an alkali aqueous solution, almost all oxidation intermediates of impurities are converted into carboxylic acids to give a purified naphthalenecarboxylic acid. Further the amount of colored components is reduced and hue is extremely improved by the oxidation treatment. The oxidation treatment is used together with decoloring treatment with a solid adsorbent to provide a high-quality product. Further, after the oxidation of the NCA with O2, a NCA alkali salt is precipitated by introducing CO2 or SO3 into the aqueous solution or the NCA alkali salt is precipitated by cooling or concentration to give NCA having more excellent purity and hue.

49. 发明专利

JPH0272170A NAPHTHOIC ACID LACTONE DERIVATIVE 失效
公开(公告)号：JPH0272170A
公开(公告)日：1990-03-12
申请号：JP31035488
申请日：1988-12-08
申请人： TANABE SEIYAKU CO
发明人： IWASAKI TAMEO , TAKASHIMA KOKI
IPC分类号： A61K31/085 , A61K31/235 , A61K31/265 , A61K31/34 , A61K31/343 , A61K31/357 , A61K31/36 , A61K31/365 , A61P3/06 , A61P9/10 , C07C43/315 , C07C45/00 , C07C45/71 , C07C47/57 , C07C51/38 , C07C63/34 , C07C65/24 , C07C67/00 , C07C67/08 , C07C67/347 , C07C69/94 , C07D307/87 , C07D307/88 , C07D307/92 , C07D317/68 , C07D317/70 , C07D493/04
摘要： NEW MATERIAL:A naphthoic acid lactone derivative expressed by formula I [either of R and R is H or alkoxy and the other is alkoxy; A is benzene ring (which may be substituted by alkyl, alkoxy, phenyl-alkoxy, OH or halogen), provided that either of R and R is H or >=2C alkoxy when A is formula II or III] or pharmaceutically acceptable salts thereof. EXAMPLE:1-(3,4-Dimethoxyphenyl)-3-hydroxymethyl-4-hydroxy-2-naphthoic acid lactone. USE:A medicine composition antilipemic action. PREPARATION:A 2,3-bislower alkoxycarbonylnaphthalene derivative expressed by formula IV (R and R are lower alkyl) or salt thereof is subjected to reduc tive lactonization reaction to afford the naphthoic acid lactone derivative expressed by formula I.

50. 发明专利

JPH0272136A NAPHTHALENE DERIVATIVE, PRODUCTION AND SYNTHETIC INTERMEDIATE THEREOF 失效
公开(公告)号：JPH0272136A
公开(公告)日：1990-03-12
申请号：JP31035388
申请日：1988-12-08
申请人： TANABE SEIYAKU CO
发明人： IWASAKI TAMEO , TAKASHIMA KOKI
IPC分类号： A61K31/085 , A61K31/235 , A61K31/265 , A61K31/34 , A61K31/343 , A61K31/357 , A61K31/36 , A61K31/365 , A61P3/06 , A61P9/10 , C07C43/315 , C07C45/00 , C07C45/71 , C07C47/57 , C07C51/38 , C07C63/34 , C07C65/24 , C07C67/00 , C07C67/08 , C07C67/347 , C07C69/94 , C07D307/87 , C07D307/88 , C07D307/92 , C07D317/68 , C07D317/70 , C07D493/04
摘要： NEW MATERIAL:A naphthalene derivative expressed by formula I or salt of said compound [R is H or alkoxycarbonyl; R is alkoxycarbonyl; one of R and R is H or alkoxy and th other is alkoxy; A is benzene ring (allowed of substitution by alkyl, etc.), benzene ring substituted by alkylene dioxy, with a proviso that in a case of R and R are simultaneously methoxycarbonyl, A is formula II or R is H, R is ethoxycarbonyl and A is formula III, one of R and R is H or >=2C alkoxy]. EXAMPLE:1-(3,4-dimethoxyphenyl)-2,3-bis(methoxycarbonyl)-4-hydro-xynap htalene. USE:Medicine having anti-lipemia action. PREPARATION:An acetylene compound expressed by formula IV is reacted with novel aldehyde compound expressed by formula V, lower alkyl acetal of said compound or salt of said compound to obtain the aimed compound expressed by formula I.

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