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41. 发明授权

US3047482A Production of oximes 失效
标题翻译：生产肟
公开(公告)号：US3047482A
公开(公告)日：1962-07-31
申请号：US83074359
申请日：1959-07-31
申请人： ALLIED CHEM
发明人： CHAO-SHING CHENG , BERNARD TAUB
IPC分类号： B01J31/02 , C07C249/06 , C07C251/44
CPC分类号： B01J31/0231 , B01J31/0202 , B01J31/0207 , B01J31/0208 , B01J31/04 , C07C249/06 , Y10S204/903 , Y10S204/911 , Y10S204/912 , Y10S204/913 , Y10S204/914 , C07C251/44

42. 发明授权

US09932296B2 Method of producing cycloalkanone oxime 有权
公开(公告)号：US09932296B2
公开(公告)日：2018-04-03
申请号：US14409299
申请日：2013-03-29
申请人： Toray Industries, Inc.
发明人： Toru Takahashi , Yasuyoshi Nishikawa , Shoji Morita
IPC分类号： B01J19/12 , C07C249/06
CPC分类号： C07C249/06 , B01J19/122 , B01J2219/1203 , C07C251/44
摘要： A method of producing a cycloalkanone oxime by a photochemical reaction of a cycloalkane with a photo nitrosating agent in a liquid by light irradiation includes irradiating the liquid with a light source configured to emit light satisfying conditions that, in an emission energy distribution with respect to wavelength of light, a wavelength providing a maximum value of emission energy is 550 nm to 700 nm and a continuous wavelength range including the wavelength providing the maximum value and outputting energy of or over 5% of the maximum value is equal to or less than 150 nm, wherein a ratio ηE/V of a light irradiation energy ηE out of electric power E input into the light source to a reaction volume V which is a volume of a space for the photochemical reaction of the cycloalkane with the photo nitrosating agent is equal to or greater than 5.5 w/L.

43. 发明申请

US20150175531A1 METHOD OF PRODUCING CYCLOALKANONE OXIME 有权
标题翻译：生产环烷酮氧化物的方法
公开(公告)号：US20150175531A1
公开(公告)日：2015-06-25
申请号：US14409299
申请日：2013-03-29
申请人： Toray Industries, Inc.
发明人： Toru Takahashi , Yasuyoshi Nishikawa , Shoji Morita
IPC分类号： C07C249/06 , B01J19/12
CPC分类号： C07C249/06 , B01J19/122 , B01J2219/1203 , C07C251/44
摘要： A method of producing a cycloalkanone oxime by a photochemical reaction of a cycloalkane with a photo nitrosating agent in a liquid by light irradiation includes irradiating the liquid with a light source configured to emit light satisfying conditions that, in an emission energy distribution with respect to wavelength of light, a wavelength providing a maximum value of emission energy is 550 nm to 700 nm and a continuous wavelength range including the wavelength providing the maximum value and outputting energy of or over 5% of the maximum value is equal to or less than 150 nm, wherein a ratio ηE/V of a light irradiation energy ηE out of electric power E input into the light source to a reaction volume V which is a volume of a space for the photochemical reaction of the cycloalkane with the photo nitrosating agent is equal to or greater than 5.5 w/L.
摘要翻译：通过光照射在液体中通过环烷烃与光亚硝化剂的光化学反应制备环烷酮肟的方法包括用配置成发射满足以下条件的光源照射液体：在相对于波长的发射能量分布中提供发射能量的最大值的波长为550nm至700nm，并且包括提供最大值并输出最大值的5％以上的能量的波长的连续波长范围等于或小于150nm ，其中将光入射到光源的光功率E的光照射能量E E与E反映成反应体积V，反应体积V是环烷烃与光亚硝化的光化学反应的空间体积试剂等于或大于5.5w / L。

44. 发明申请

US20110152535A1 PREPARATION OF ISOXAZOLIN-3-YLACYLBENZENES 有权
标题翻译： ISOXAZOLIN-3-YLACYBENZENES的制备
公开(公告)号：US20110152535A1
公开(公告)日：2011-06-23
申请号：US13039137
申请日：2011-03-02
申请人： Joachim Rheinheimer , Wolfgang von Deyn , Joachim Gebhardt , Michael Rack , Rene Lochtman , Norbert Götz , Michael Keil , Matthias Witschel , Helmut Hagen , Ulf Mißlitz , Ernst Baumann
发明人： Joachim Rheinheimer , Wolfgang von Deyn , Joachim Gebhardt , Michael Rack , Rene Lochtman , Norbert Götz , Michael Keil , Matthias Witschel , Helmut Hagen , Ulf Mißlitz , Ernst Baumann
IPC分类号： C07D261/04
CPC分类号： C07C249/06 , C07C201/10 , C07C201/12 , C07C205/44 , C07C209/62 , C07C251/48 , C07C253/00 , C07C255/50 , C07C315/04 , C07C319/14 , C07D261/04 , C07D413/10 , C07C323/09 , C07C317/24 , C07C317/32 , C07C205/06 , C07C211/52
摘要： A process is described for preparing isoxazoles of the formula I where the substituents are as defined below: R1 is hydrogen, C1-C6-alkyl, R2 is C1-C6-alkyl, R3, R4, R5 are hydrogen, C1-C6-alkyl, or R4 and R5 together form a bond, R6 is a heterocyclic ring, n is 0, 1 or 2; which comprises preparing an intermediate of the formula VI where R1, R3, R4 and R5 are as defined above, followed by halogenation, thiomethylation, oxidation and acylation to give compounds of the formula I. Also novel intermediates for preparing the compounds of the formula I and novel processes for preparing the intermediates are described.
摘要翻译：描述了制备式I的异恶唑的方法，其中取代基如下所定义：R 1是氢，C 1 -C 6烷基，R 2是C 1 -C 6烷基，R 3，R 4，R 5是氢，C 1 -C 6 - 烷基，或R4和R5一起形成键，R6是杂环，n是0,1或2; 其包括制备式VI的中间体，其中R 1，R 3，R 4和R 5如上定义，然后进行卤化，硫甲基化，氧化和酰化，得到式I化合物。还有用于制备式I化合物的中间体并描述了制备中间体的新方法。

45. 发明授权

US06768023B2 Process for producing organic compounds using nitrites 失效
标题翻译：使用亚硝酸盐生产有机化合物的方法
公开(公告)号：US06768023B2
公开(公告)日：2004-07-27
申请号：US10379600
申请日：2003-03-06
申请人： Yasutaka Ishii , Tatsuya Nakano , Takahiro Iwahama
发明人： Yasutaka Ishii , Tatsuya Nakano , Takahiro Iwahama
IPC分类号： C07C24906
CPC分类号： C07C201/00 , C07B47/00 , C07C249/06 , C07C2601/08 , C07C2601/14 , C07C2601/18 , C07C2601/20 , Y02P20/55 , C07C251/44 , C07C251/48 , C07C207/02
摘要： A process produces an organic compound by allowing (A) a compound capable of generating a free radical to react with (B) at least one of esters and salts of nitrous acid in the presence of a nitrogen-containing cyclic compound constitutively having a skeleton represented by following Formula (i) in its ring: wherein X is an oxygen atom or an —OR group, and wherein R is a hydrogen atom or a hydroxyl-protecting group. Examples of the nitrogen-containing cyclic compound are cyclic imide compounds having a cyclic imide skeleton represented by following Formula (I): wherein n is 0 or 1; X is an oxygen atom or an —OR group, and wherein R is a hydrogen atom or a hydroxyl-protecting group.
摘要翻译：一种方法通过使（A）能够产生自由基的化合物在（B）至少一种亚硝酸的酯和盐的存在下，使组成性地具有骨架的含氮环状化合物其中X为氧原子或-OR基团，其中R为氢原子或羟基保护基团。含氮环状化合物的实例是具有由下式（I）表示的环状酰亚胺骨架的环状酰亚胺化合物：其中n为0或1; X是氧原子或-OR基团，其中R是氢原子或羟基保护基团。

46. 发明申请

US20030171618A1 Process for producing organic compounds using nitrites 失效
标题翻译：使用亚硝酸盐生产有机化合物的方法
公开(公告)号：US20030171618A1
公开(公告)日：2003-09-11
申请号：US10379600
申请日：2003-03-06
发明人： Yasutaka Ishii , Tatsuya Nakano , Takahiro Iwahama
IPC分类号： C07C249/06
CPC分类号： C07C201/00 , C07B47/00 , C07C249/06 , C07C2601/08 , C07C2601/14 , C07C2601/18 , C07C2601/20 , Y02P20/55 , C07C251/44 , C07C251/48 , C07C207/02
摘要： A process produces an organic compound by allowing (A) a compound capable of generating a free radical to react with (B) at least one of esters and salts of nitrous acid in the presence of a nitrogen-containing cyclic compound constitutively having a skeleton represented by following Formula (i) in its ring: 1 wherein X is an oxygen atom or an nullOR group, and wherein R is a hydrogen atom or a hydroxyl-protecting group. Examples of the nitrogen-containing cyclic compound are cyclic imide compounds having a cyclic imide skeleton represented by following Formula (I): 2 wherein n is 0 or 1; X is an oxygen atom or an nullOR group, and wherein R is a hydrogen atom or a hydroxyl-protecting group.
摘要翻译：一种方法通过使（A）能够产生自由基的化合物在（B）至少一种亚硝酸的酯和盐的存在下，使组成性地具有骨架的含氮环状化合物其中X为氧原子或-OR基团，其中R为氢原子或羟基保护基团。含氮环状化合物的实例是具有由下式（I）表示的环状酰亚胺骨架的环状酰亚胺化合物：其中n为0或1; X是氧原子或-OR基团，其中R是氢原子或羟基保护基团。

47. 发明授权

US06525204B1 Method for producing isoxazoline-3-yl-acyl benzene 有权
标题翻译：异恶唑啉-3-基 - 酰基苯的制备方法
公开(公告)号：US06525204B1
公开(公告)日：2003-02-25
申请号：US09674535
申请日：2000-11-02
申请人： Joachim Rheinheimer , Wolfgang von Deyn , Joachim Gebhardt , Michael Rack , Rene Lochtman , Norbert Götz , Michael Keil , Matthias Witschel , Helmut Hagen , Ulf Misslitz , Ernst Baumann
发明人： Joachim Rheinheimer , Wolfgang von Deyn , Joachim Gebhardt , Michael Rack , Rene Lochtman , Norbert Götz , Michael Keil , Matthias Witschel , Helmut Hagen , Ulf Misslitz , Ernst Baumann
IPC分类号： C07D26104
CPC分类号： C07C249/06 , C07C201/10 , C07C201/12 , C07C205/44 , C07C209/62 , C07C251/48 , C07C253/00 , C07C255/50 , C07C315/04 , C07C319/14 , C07D261/04 , C07D413/10 , C07C323/09 , C07C317/24 , C07C317/32 , C07C205/06 , C07C211/52
摘要： A process is described for preparing isoxazol-3-ylacylbenzenes. Also, novel intermediates for preparing isoxazol-3-ylacylbenzenes and novel processes for preparing the intermediates are described.
摘要翻译：描述了制备异恶唑-3-基酰基苯的方法。另外还描述了用于制备异恶唑-3-基酰基苯的新型中间体和制备中间体的新方法。

48. 发明授权

US3090739A Method of producing nitroso compounds or oximes 失效
标题翻译：生产亚硝基化合物或肟的方法
公开(公告)号：US3090739A
公开(公告)日：1963-05-21
申请号：US4344060
申请日：1960-07-18
申请人： TOYO RAYON CO LTD
发明人： YOSHIKAZU ITO
IPC分类号： B01J19/12 , C07C201/00 , C07C207/02
CPC分类号： B01J19/122 , C07C201/00 , C07C249/06 , C07C207/02 , C07C251/44 , C07C251/38

49. 发明授权

US11697646B2 Triazole N-linked carbamoyl cyclohexyl acids as LPA antagonists 有权
公开(公告)号：US11697646B2
公开(公告)日：2023-07-11
申请号：US17224161
申请日：2021-04-07
申请人： BRISTOL-MYERS SQUIBB COMPANY
发明人： Yan Shi , Peter Tai Wah Cheng , Ying Wang , Jun Shi , Shiwei Tao , Jun Li , Lawrence J. Kennedy , Robert F. Kaltenbach, III , Hao Zhang , James R. Corte
IPC分类号： C07D401/04 , C07D403/04 , C07D249/06 , A61P35/00 , A61P1/16 , A61P19/10 , A61P13/12 , A61P11/00 , C07C249/06 , C07C403/04
CPC分类号： C07D401/04 , A61P35/00 , C07C249/06 , C07C403/04 , C07D249/06 , C07D403/04 , A61P1/16 , A61P11/00 , A61P13/12 , A61P19/10
摘要： The present invention provides compounds of Formula (I):

or a stereoisomer, tautomer, or pharmaceutically acceptable salt or solvate thereof, wherein all the variables are as defined herein. These compounds are selective LPA receptor inhibitors.

50. 发明申请

US20170298015A1 PHOTOCHEMICAL REACTION DEVICE, PHOTOCHEMICAL REACTION METHOD USING SAME, AND LACTAM PRODUCTION METHOD USING SAID METHOD 审中-公开
公开(公告)号：US20170298015A1
公开(公告)日：2017-10-19
申请号：US15517424
申请日：2015-09-17
申请人： TORAY INDUSTRIES, INC.
发明人： Takenori Sugimoto , Toru Takahashi , Kazuki Sugawara
IPC分类号： C07D201/04 , B01J19/12 , C07C249/06
CPC分类号： C07D201/04 , B01J19/12 , B01J19/127 , B01J2219/0801 , B01J2219/0877 , B01J2219/1203 , C07B61/00 , C07C249/04 , C07C249/06 , C07C251/44
摘要： Provided is a photochemical reaction device wherein two partitions formed from an optically transparent material are arranged apart from each other between a light source and a reaction liquid, and an optically transparent fluid introduction/discharge means for introducing an optically transparent fluid between the partitions and discharging the fluid and a state change detection means for detecting a change in the state of the optically transparent fluid at the discharge side of the optically transparent fluid introduction/discharge means are provided. Also provided are a photochemical reaction method that uses the photochemical reaction device and a lactam production method that uses the photochemical reaction method. The present invention prevents decreases in the performance of the light source even when the optically transparent material in the photochemical reaction device is damaged, and makes it possible to reliably prevent ignition even if the reaction liquid is a flammable liquid.

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