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41. 发明授权

US07666356B2 Trace sampling 失效
标题翻译：跟踪采样
公开(公告)号：US07666356B2
公开(公告)日：2010-02-23
申请号：US11425313
申请日：2006-06-20
申请人： Daniel O'Donnell , Edward E. A. Bromberg , Paul Crabb , Ravi Konduri , C. Andrew Helm , David H. Fine
发明人： Daniel O'Donnell , Edward E. A. Bromberg , Paul Crabb , Ravi Konduri , C. Andrew Helm , David H. Fine
IPC分类号： G01N1/24 , G01N21/00
CPC分类号： G01N1/2214 , G01N33/0057 , G01N2001/024 , G01N2001/028
摘要： A trace sampling detection system includes a gathering device configured to gather particles through a handle-bar, a gate and an air-stream gatherer. A collection tube is configured to deposit gathered particles from the gathering device onto a portion of a sample media. A carousel wheel that includes the sample media is configured to rotate the sample wheel such that the portion of the sample media including the gathered particles is presented to an exothermic decomposition detector that detects, through an infrared sensor, the decomposition of the gathered particles.
摘要翻译：轨迹采样检测系统包括：收集装置，其被配置成通过手柄条，门和空气流收集器收集颗粒。收集管被配置为将收集的颗粒从收集装置沉积到样品介质的一部分上。包括样品介质的转盘轮被配置为旋转样品轮，使得包含聚集的颗粒的样品介质的部分被呈现给放热分解检测器，其通过红外传感器检测聚集的颗粒的分解。

42. 发明申请

US20080317874A1 Conversion of nitrogen dioxide (NO2) to nitric oxide (NO) 有权
标题翻译：二氧化氮（NO2）转化为一氧化氮（NO）
公开(公告)号：US20080317874A1
公开(公告)日：2008-12-25
申请号：US12076723
申请日：2008-03-21
申请人： David H. Fine , David P. Rounbehler , Greg Vasquez
发明人： David H. Fine , David P. Rounbehler , Greg Vasquez
IPC分类号： A61K33/00 , A61P9/12
CPC分类号： A61M16/10 , A61M2016/1025 , A61M2202/0275 , C01B21/24
摘要： A nitric oxide delivery system, which includes a gas bottle having nitrogen dioxide in air, converts nitrogen dioxide to nitric oxide and employs a surface-active material, such as silica gel, coated with an aqueous solution of antioxidant, such as ascorbic acid. A nitric oxide delivery system may be used to generate therapeutic gas including nitric oxide for use in delivering the therapeutic gas to a mammal.
摘要翻译：包括在空气中具有二氧化氮的气瓶的一氧化氮输送系统将二氧化氮转化为一氧化氮，并使用涂覆有抗氧化剂水溶液如抗坏血酸的表面活性物质如硅胶。一氧化氮递送系统可用于产生治疗气体，包括用于将治疗气体递送至哺乳动物的一氧化氮。

43. 发明授权

US07204125B2 Pressure activated sampling system 失效
标题翻译：压力激活采样系统
公开(公告)号：US07204125B2
公开(公告)日：2007-04-17
申请号：US11087818
申请日：2005-03-24
申请人： David H. Fine , Freeman W. Fraim
发明人： David H. Fine , Freeman W. Fraim
IPC分类号： G01N30/72 , G01N33/22 , G01N35/10 , B01D15/08
CPC分类号： G01N1/2202 , G01N2001/022 , G01N2001/024 , Y10S436/901 , Y10T436/141111 , Y10T436/163333 , Y10T436/170769 , Y10T436/173845
摘要： Screening of items for the presence of contaminants, such as explosives residue, is accomplished by subjecting an item loaded into a pressure chamber to a pressure substantially in excess of atmospheric pressure conditions and rapidly decompressing the item to the ambient atmospheric pressure. The rapid decompression serves to scavenge vapors and particles from the exterior and interior of the item and any objects it contains. A sample of the vapors and particles removed from the item by the rapid decompression is sampled and is tested to determine whether a predetermined contaminant is present in the sample. Depending on the types of contaminants for which the sample is tested, it is possible to detect whether explosives, biological or chemical agents, and/or narcotics residues are present on or in the item being screened.
摘要翻译：通过对装载到压力室中的物品施加基本上超过大气压力条件的压力并将物品快速减压至环境大气压来实现污染物（例如爆炸物残渣）的存在的筛选。快速减压用于清除物品的外部和内部以及其包含的任何物体的蒸气和颗粒。对通过快速减压从物品中除去的蒸气和颗粒的样品进行采样，并进行测试以确定样品中是否存在预定的污染物。根据测试样品的污染物类型，可以检测爆炸物，生物或化学物质和/或麻醉剂残留物是否存在于待筛选的物品上。

44. 发明授权

US5808178A High speed gas chromatography 失效
标题翻译：高速气相色谱
公开(公告)号：US5808178A
公开(公告)日：1998-09-15
申请号：US731573
申请日：1996-10-16
申请人： David P. Rounbehler , Eugene K. Achter , David H. Fine , George B. Jarvis , Stephen J. MacDonald , David B. Wheeler , Clayton D. Wood
发明人： David P. Rounbehler , Eugene K. Achter , David H. Fine , George B. Jarvis , Stephen J. MacDonald , David B. Wheeler , Clayton D. Wood
IPC分类号： G01N30/02 , G01N30/06 , G01N30/12 , G01N30/16 , G01N30/20 , G01N30/30 , G01N30/40 , G01N30/46 , G01N30/60 , G01N30/84 , G01N30/54
CPC分类号： G01N30/30 , G01N2030/025 , G01N2030/062 , G01N2030/121 , G01N2030/122 , G01N2030/123 , G01N2030/3015 , G01N2030/303 , G01N2030/3038 , G01N2030/3046 , G01N2030/3061 , G01N2030/3069 , G01N2030/3076 , G01N2030/3084 , G01N2030/402 , G01N2030/405 , G01N2030/8405 , G01N30/06 , G01N30/16 , G01N30/461 , G01N30/466 , G01N30/6047
摘要： A high speed gas chromatography system includes a heated isothermal region and a gas chromatography column located externally to the isothermal region. The system also includes a detector and a flow path between the column and the detector. At least a portion of the flow path is positioned in the isothermal region.
摘要翻译：高速气相色谱系统包括加热的等温区域和位于等温区域外部的气相色谱柱。该系统还包括检测器和柱与检测器之间的流动路径。流路的至少一部分位于等温区域中。

45. 发明授权

US5688693A Method and system for sampling and determining the presence of contaminants in recyclable plastic materials 失效
标题翻译：用于取样和确定可回收塑料材料中污染物存在的方法和系统
公开(公告)号：US5688693A
公开(公告)日：1997-11-18
申请号：US639757
申请日：1996-04-29
申请人： David H. Fine , Freeman W. Fraim , Stephen J. MacDonald , Alex Malaspina , Forrest Lee Bayer , Dirck vanBuren Myers
发明人： David H. Fine , Freeman W. Fraim , Stephen J. MacDonald , Alex Malaspina , Forrest Lee Bayer , Dirck vanBuren Myers
IPC分类号： G01N1/28 , B07C5/34 , B08B9/46 , B09B5/00 , B29B17/00 , B29B17/02 , B29B17/04 , G01N1/00 , G01N1/22 , G01N1/24 , G01N21/64 , G01N21/76 , G01N21/90 , G01N33/00 , G01N33/44 , G01N35/02
CPC分类号： G01N33/442 , B07C5/34 , B08B9/46 , B29B17/00 , B29B17/02 , G01N1/2226 , G01N21/64 , G01N21/766 , G01N21/9018 , G01N21/9081 , B08B2203/005 , B29B2017/0203 , B29B2017/0275 , B29K2067/00 , B29K2105/065 , B29L2031/7158 , G01N1/2202 , G01N1/24 , G01N2001/2223 , G01N2001/2229 , G01N2033/0081 , G01N21/76 , Y02W30/62 , Y02W30/622 , Y10S241/38 , Y10T436/11 , Y10T436/115831 , Y10T436/25375 , Y10T436/25875
摘要： An inspection system for sampling and determining the presence of residues of contaminants within plastic materials to be recycled from used plastic materials such as plastic beverage bottles or plastic food containers includes a chemical sniffing apparatus, or alternatively an optical scanner, for detecting the contaminants as the plastic materials are rapidly moved along a conveyor past a series of stations. Recycled food or beverage bottles are fed through a shredder in-line with the conveyor and the shredded plastic material from the bottles is fed to a washer. The bottles and shredded material may be tested for contaminants at any location in an in-line process. In one exemplary system first the bottles are tested prior to entry into the shredder in order to remove bottles containing gross contaminants. Second the shredded material emerging from the shredder is immediately tested for contaminants at an elevated temperature caused by the shredding process and contaminated materials are separated or sorted out from the uncontaminated material. Third, the materials are again tested for contaminants as they emerge from the washer once again taking advantage of the elevated temperature of the materials which is conducive to the emission of vapors of the contaminants. Contaminated materials are again sorted from the uncontaminated supply of materials to be used for the fabrication of new plastic food or beverage bottles.
摘要翻译：用于取样和确定塑料材料中残留物的存在的检查系统将从塑料饮料瓶或塑料食品容器等塑料材料中回收使用，包括用于检测污染物的化学嗅探装置或光学扫描仪，塑料材料沿着传送带快速移动通过一系列的站。回收的食品或饮料瓶通过与输送机成线的粉碎机进料，并且来自瓶子的切碎的塑料材料被供给到洗衣机。瓶子和切碎的材料可以在在线过程中的任何位置测试污染物。在一个示例性系统中，首先在进入粉碎机之前测试瓶子，以便去除含有大量污染物的瓶子。第二，从切碎机出来的切碎的材料立即在高温下测试污染物，并且被污染的材料从未污染的材料中分离或分离出来。第三，再次利用材料的高温有利于污染物蒸气的排放，再次从洗衣机中出来的污染物被测试。受污染的材料再次从用于制造新的塑料食品或饮料瓶的未受污染的材料供应分类。

46. 发明授权

US5092218A Selective detection of explosives vapors 失效
标题翻译：炸药蒸气的选择性检测
公开(公告)号：US5092218A
公开(公告)日：1992-03-03
申请号：US81919
申请日：1987-07-08
申请人： David H. Fine , David P. Rounbehler
发明人： David H. Fine , David P. Rounbehler
IPC分类号： G01N1/00 , G01N1/02 , G01N1/22 , G01N1/28 , G01N1/40 , G01N21/76 , G01N27/417 , G01N30/02 , G01N30/06 , G01N30/08 , G01N30/12 , G01N30/14 , G01N30/16 , G01N30/30 , G01N30/40 , G01N30/46 , G01N30/62 , G01N30/64 , G01N30/72 , G01N30/84 , G01N31/12 , G01N33/00 , G01N33/22 , G01V9/00
CPC分类号： G01N30/461 , G01N1/02 , G01N30/08 , G01N30/12 , G01N30/84 , G01N33/0057 , G01V9/007 , G01N1/2214 , G01N1/2226 , G01N1/28 , G01N1/40 , G01N2001/022 , G01N2001/028 , G01N2030/025 , G01N2030/065 , G01N2030/085 , G01N2030/121 , G01N2030/122 , G01N2030/123 , G01N2030/125 , G01N2030/126 , G01N2030/143 , G01N2030/167 , G01N2030/3007 , G01N2030/3046 , G01N2030/3053 , G01N2030/3061 , G01N2030/3069 , G01N2030/3076 , G01N2030/3084 , G01N2030/626 , G01N2030/642 , G01N2030/8405 , G01N21/76 , G01N30/14 , G01N30/40 , G01N30/62 , G01N30/72
摘要： A highly selective, sensitive, fast detection system and method are disclosed for detecting vapors of specific compounds in air. Vapors emanating from compounds such as explosives, or stripped from surfaces using heat and suction from a hand-held sample gun, are collected on surfaces coated with gas chromatograph (GC) material which trap explosives vapors but repel nitric oxide, then are desorbed and concentrated in one or more cold spot concentrators. A high speed gas chromatograph (GC) separates the vapors, after which specific vapors are decomposed in two pyrolyzers arranged in parallel and the resulting nitric oxide is detected. A low temperature pyrolyzer with silver produces NO from nitramines or nitrite esters; a high temperature pyrolyzer decomposes all explosives vapors to permit detection of the remaining explosives. Also disclosed is a series arrangement of pyrolyzers and gas chromatographs and an NO detector to time-shift detection of certain vapors and facilitate very fast GC analyses. The use of hydrogen as a carrier gas, plus unique collectors and concentrators, high speed heaters, NO detectors, and very fast, temperature-programmable GC's enhance selectivity, sensitivity and speed of detection.
摘要翻译：公开了一种高选择性，灵敏，快速的检测系统和方法，用于检测空气中特定化合物的蒸气。从化合物如爆炸物或从手持式样品枪吸取热量从表面剥离的蒸气被收集在涂有气相色谱（GC）材料的表面上，该气相色谱（GC）材料捕获爆炸物蒸气但排斥一氧化氮，然后被解吸和浓缩在一个或多个冷点浓缩器中。高速气相色谱仪（GC）分离蒸汽，之后特定的蒸汽在平行排列的两个热解器中分解，并检测到所产生的一氧化氮。含有银的低温热解器由硝胺或亚硝酸酯产生NO; 高温热解器分解所有炸药蒸气，以便检测剩余的炸药。还公开了热解器和气相色谱仪的串联布置和用于某些蒸气的时移检测的NO检测器，并且促进非常快速的GC分析。使用氢气作为载气，加上独特的收集器和浓缩器，高速加热器，NO检测器和非常快速的温度可编程GC增强了选择性，灵敏度和检测速度。

47. 发明授权

US4066411A N-nitroso compound analyzer with sample atomization 失效
标题翻译：具有样品原型的N-NITROSO化合物分析仪
公开(公告)号：US4066411A
公开(公告)日：1978-01-03
申请号：US760603
申请日：1977-01-19
申请人： David H. Fine , John J. Fronduto , David P. Rounbehler
发明人： David H. Fine , John J. Fronduto , David P. Rounbehler
IPC分类号： G01N30/84 , G01N33/00 , G01N31/08
CPC分类号： G01N30/84 , G01N2030/8405 , G01N2030/8476 , Y10T436/170769 , Y10T436/179228
摘要： A liquid-gas interface is provided between a heated reaction chamber of an N-nitroso compound detection system and a liquid chromatograph. The liquid-gas interface atomizes liquid chromatograph effluent, including the N-nitroso compounds to be measured, with a stream of carrier gas, into the reaction chamber. In the heated reaction chamber, the effluent from the interface is vaporized. Condensation of non-volatile N-nitroso compounds is avoided by preheating the liquid effluent prior to atomization.

48. 发明授权

US3996004A Detection system with liquid chromatograph 失效
标题翻译：液相色谱检测系统
公开(公告)号：US3996004A
公开(公告)日：1976-12-07
申请号：US614287
申请日：1975-09-17
申请人： David H. Fine , David P. Rounbehler
发明人： David H. Fine , David P. Rounbehler
IPC分类号： G01N30/84 , G01N31/00 , G01N31/08
CPC分类号： G01N30/84 , G01N31/00 , Y10T436/173076
摘要： Apparatus for detecting the amount of a specific compound in a sample dissolved in a liquid solvent. The apparatus comprises, in combination, a high pressure liquid chromatograph, means to transform the chromatograph effluent to the gaseous state, a cold trap and a specific gas detector. The cold trap includes means to cool the gas injected therein at a predetermined temperature, and means to maintain a predetermined pressure therein, whereby the solvent is condensed and the gaseous effluent from the trap substantially consists of the specific gas.
摘要翻译：用于检测溶解在液体溶剂中的样品中特定化合物的量的装置。该装置组合包括高压液相色谱仪，将色谱流出物转化为气态的装置，冷阱和特定气体检测器。冷阱包括在预定温度下冷却注入其中的气体的装置，以及在其中保持预定压力的装置，由此使溶剂冷凝，并且来自捕集阱的气态流出物基本上由特定气体组成。

49. 发明授权

US3996003A Specific compound detection system with liquid chromatograph 失效
标题翻译：具有液相色谱的具体化合物检测系统
公开(公告)号：US3996003A
公开(公告)日：1976-12-07
申请号：US614286
申请日：1975-09-17
申请人： David H. Fine , David P. Rounbehler
发明人： David H. Fine , David P. Rounbehler
IPC分类号： G01N30/84 , G01N31/08
CPC分类号： G01N30/84 , Y10T436/170769 , Y10T436/171538 , Y10T436/173845
摘要： Apparatus for detecting the amount of a specific compound in a sample dissolved in a liquid solvent. The apparatus comprises, in combination, a high pressure liquid chromatograph, means to transform the chromatograph effluent to the gaseous state, a cold trap and a specific gas detector. The cold trap includes means to cool the gas injected therein at a predetermined temperature, and means to maintain a predetermined pressure therein, whereby the solvent is condensed and the gaseous effluent from the trap substantially consists of the specific gas.
摘要翻译：用于检测溶解在液体溶剂中的样品中特定化合物的量的装置。该装置组合包括高压液相色谱仪，将色谱流出物转化为气态的装置，冷阱和特定气体检测器。冷阱包括在预定温度下冷却注入其中的气体的装置，以及在其中保持预定压力的装置，由此使溶剂冷凝，并且来自捕集阱的气态流出物基本上由特定气体组成。

50. 发明授权

US3996002A Method and apparatus for measuring the n-nitroso compound content of a sample 失效
标题翻译：用于测量样品的n-亚硝基化合物含量的方法和装置
公开(公告)号：US3996002A
公开(公告)日：1976-12-07
申请号：US614101
申请日：1975-09-17
申请人： David H. Fine
发明人： David H. Fine
IPC分类号： G01N31/00 , G01N21/52 , G01N31/10
CPC分类号： G01N31/00 , Y10T436/170769
摘要： The N-nitroso compound content of a sample is measured by selectively breaking the N-NO bond in the N-nitroso compound molecule by non-catalytic pyrolyzation at temperatures in the range 300.degree. C to 500.degree. C, thereby liberating nitric oxide (NO), and by the subsequent measurement of the amount of nitric oxide liberated. The apparatus comprises a chromatograph and an NO detector together with a non-catalytic pyrolyzer. The pyrolyzer includes a chemically inert material configured to provide a cylindrical cross-section flow path for the chromatograph effluent. The pyrolyzer further includes the temperature control means for adding thermal energy at a controlled rate so that the flow path is characterized by temperatures in the range of 300.degree. C to 500.degree. C.
摘要翻译：样品的N-亚硝基化合物含量通过在300℃〜500℃的温度范围内的非催化热解选择性地破坏N-亚硝基化合物分子中的N-NO键来测定，从而释放出一氧化氮），并随后测量释放的一氧化氮的量。该装置包括色谱仪和NO检测器以及非催化热解器。热解器包括化学惰性材料，其被配置为提供色谱流出物的圆柱形横截面流动路径。热解器还包括用于以受控速率加入热能的温度控制装置，使得流动路径的特征在于300℃至500℃范围内的温度。

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